IP Library Granted Patent US 8,603,267
Granted Patent B2
US 8,603,267 · App. 13/169,204 · Granted Dec 10, 2013

Extrusion of glassy aluminum-based alloys

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Quick Facts
Patent No.
US 8,603,267
App. No.
13/169,204
Granted
Dec 10, 2013
Kind
B2
Abstract

A method of extruding a glassy aluminum-based alloy billet, by soaking the billet for sufficient time to heat the billet to an extrusion starting temperature of from about 300° F. to about 600° F. and extruding the billet in a streamline die having an extrusion ratio to keep the adiabatic temperature below the starting temperature while maintaining the streamline die at a temperature of about 400° F. to about 600° F. at a ram speed less than that which would raise the streamline die temperature within this range.

Claims (17)

1. A method of extruding an aluminum-based alloy, comprising the steps of:

selecting an aluminum-based alloy billet, wherein the aluminum based alloy is selected from the group consisting of a devitrified alloy having a nanocrystalline microstructure and a glassy aluminum alloy having substantially no devitrification;

soaking the billet for sufficient time to heat the billet to an extrusion starting temperature of from about 450° F. to about 550° F. (232.2° C. to 287.9° C.), wherein a time for the soaking is from about 10 minutes to about 72 hours;

extruding the billet in a streamline die having an extrusion ratio sufficient to keep the adiabatic temperature below the starting temperature while maintaining the streamline die at a temperature of about 400° F. to about 600° F. (204.4° C. to 315.6° C.) at a ram speed less than that which would raise the streamline die temperature within this range; and

removing the extruded billet from the die.

2. The method of claim 1 , wherein the aluminum based alloy is an aluminum based alloy containing from 3 to 18.5 atomic percent nickel and 3 to 14.0 atomic percent yttrium.

3. The method of claim 1 , wherein the streamline die is maintained at a temperature ranging from about 400° F. to about 575° F. (204.4° C. to 301.7° C.) at a ram speed of from about 0.1 to 100 inches per minute.

4. The method of claim 1 , wherein the streamline die is maintained at a temperature ranging from about 475° F. to about 525° F. (246.1° C. to 273.9° C.) at a ram speed of from about 0.1 to 5 inches per minute.

5. The method of claim 1 , wherein the streamline die has an extrusion ratio of from about 1 to about 10, and has a length ranging from about 4 inches to 6 inches (10.16 cm. to 15.24 cm.).

6. A method of extruding a devitrified aluminum-based alloy, comprising the steps of:

selecting a devitrified aluminum-based alloy billet having a nanocrystalline microstructure;

soaking the billet having a nanocrystalline microstructure for sufficient time to heat the billet to an extrusion starting temperature of from about 450° F. to about 550° F. (232.2° C. to 287.9° C.), wherein a time for the soaking is from about 10 minutes to about 72 hours;

extruding the billet in a streamline die having an extrusion ratio sufficient to keep the adiabatic temperature below the starting temperature while maintaining the streamline die at a temperature of about 400° F. to about 600° F. (204.4° C. to 315.6° C.) at a ram speed less than that which would raise the streamline die temperature within this range; and

removing the extruded billet from the die.

7. The method of claim 6 , wherein the devitrified aluminum based alloy is an aluminum based alloy containing from 3 to 18.5 atomic percent nickel and 3 to 14.0 atomic percent yttrium.

8. The method of claim 7 , wherein the streamline die is maintained at a temperature ranging from about 400° F. to about 575° F. (204.4° C. to 301.7° C.) at a ram speed of from about 0.1 to 100 inches per minute.

9. The method of claim 6 , wherein the streamline die has an extrusion ratio of from about 1 to about 10, and has a length ranging from about 4 inches to 6 inches (10.16 cm. to 15.24 cm.).

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
CONFIRMATORY LICENSE Recorded Sep 10, 2013
From: UNITED TECHNOLOGIES CORPORATION
To: DARPA
Reel/Frame 031200/0360 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 27, 2011
From: WATSON, THOMAS J.
To: UNITED TECHNOLOGIES CORPORATION
Reel/Frame 026504/0497 →