IP Library Granted Patent US 9,125,824
Granted Patent B1
US 9,125,824 · App. 13/173,927 · Granted Sep 8, 2015

Methods and systems for processing organic trans-resveratrol as dietary supplements

Inventors: Naomi Balcombe (Gainesville, FL); Robert Maru (Livingston, NJ); Surendra Vallabhaneni (Flemington, NJ)
Assignee: InnoVitamin Organics, LLC
A61K9/2054A61K9/1682
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,125,824
App. No.
13/173,927
Granted
Sep 8, 2015
Kind
B1
Abstract

Methods and systems for processing organic trans-resveratrol for use in dietary supplements is disclosed. The process begins with harvesting grapes, stems and leaves, placing them in a cloth sack and delivering the grapes, stems and leaves to a nearby processing facility within less than 25 minutes. Thereafter, grapes are pressed to extract the juice and the residual pomace of skin, seeds and stems is removed from the pressing cylinder, ground to a fine mesh powder (approximately 50 mesh size), mixed with a bioflavanoid compound and polygonum cuspidatum , handled in controlled temperatures between approximately 10.0° C. (50 degrees F.) to approximately 30° C. (86 degrees F.) and with humidity of the storage area at less than 35%. The process results in a high quality and high quantity yield of a stable, organic trans-resveratrol for use in dietary supplements that are bioavailable and easily absorbed by the consumer of the dietary supplement.

Claims (40)

1. A method of processing trans-resveratrol for use in dietary supplements consisting essentially of the steps of:

solely harvesting organically grown grapes, vines and leaves;

placing the harvested organically grown grapes, the vines and the leaves in a cloth sack;

transporting the harvested organically grown grapes and the vines to a separating location in a time period between approximately 4 minutes to approximately 25 minutes after harvesting;

separating the organically grown grapes from the vines and the leaves;

pressing the organically grown grapes until a pomace of grape skin, grape seeds and grape stems is left in a container;

removing the pomace from the container;

adding the vines and the leaves to the pomace;

shipping the pomace to an extraction location with vines and leaves;

storing the pomace, the vines and the leaves at the extraction location;

grinding the pomace, the vines and the leaves into a fine powder;

shipping the fine powder to manufacturing location;

mixing the fine powder with bioflavanoid nutrients and polygonum into a mixture;

processing the mixture in a granulator to form a granulated mixture;

coating the granulated mixture with a cellulose barrier coating to protect the granulated mixture from heat, humidity and UV light in atmospheric conditions;

storing the granulated mixture with the cellulose bather coating in a vacuum sealed UV light protected container;

shipping the vacuum sealed container to the manufacturing location;

preparing a dietary supplement product in the form of at least one of capsules, liquids and tablets from the granulated mixture with the cellulose bather coating;

placing prepared capsules, liquids and tablets into a closed container; and

shipping the closed container to final destination, wherein the dietary supplements contains approximately 97 to 99 percent stable organic trans-resveratrol to approximately 1 to 3% cis-resveratrol with low levels of impurities and low levels of microbial grown.

2. The method of claim 1 , wherein the organically grown grapes and the vines are selected from organically grown French Muscadine grapes, American Muscadine grapes and mixtures thereof.

3. The method of claim 1 , wherein the transporting to a separating facility is a time period of from approximately five minutes to approximately ten minutes of harvesting.

4. The method of claim 1 , wherein the pomace of grape skin, grape seeds and grape stems is mixed with the vines and the stems, and is ground to a fine powder, wherein the powder has a mesh size in a range between approximately 40 mesh to approximately 80 mesh.

5. The method of claim 1 , wherein the fine powder is mixed with the bioflavanoid nutrients into a compound, the bioflavanoid nutrients is selected from at least one of quercetin dihydrate, hesperidin complex, and rose hips concentrate.

6. The method of claim 5 , wherein the bioflavanoid compound is quercetin dihydrate.

7. The method of claim 1 , wherein the controlled environment for storage of the fine powder and bioflavanoid mixture includes a temperature range of between 10.0° C. (50 degrees F.) to approximately 30° C. (86 degrees F.) and a humidity level in the storage area of less than 35% water vapor in the air.

8. The method of claim 1 , wherein the granulated mixture is dried at approximately 26.6° C. (80° F.) to reduce the moisture content of the mixture to a range between 0.1 weight % to approximately 10 wt. %.

9. The method of claim 8 , wherein the moisture content of the granulated mixture is approximately 1% by weight.

10. The method of claim 9 further consisting of the step of preparing dietary supplements in the form of at least one of capsules, liquids and tablets.

11. The method of claim 10 , wherein the shipping step includes storing the capsules, liquids and tablets in dark containers for shipment.

12. A method of processing trans-resveratrol for use in dietary supplements consisting of the steps of:

solely harvesting organically grown grapes, vines and leaves;

separating the organically grown grapes from the vines and the leaves;

pressing the organically grown grapes until a pomace of grape skin, seeds and stems is left;

adding the vines and the leaves to the pomace;

grinding the pomace, the vines and the leaves into a fine powder;

mixing the powder with bioflavanoid nutrients and polygonum into a mixture;

processing the mixture in a granulator to form a granulated mixture;

coating the granulated mixture with a cellulose barrier coating to protect the granulated mixture from heat, humidity and UV light in atmospheric conditions; and

preparing a dietary supplement product in the form of at least one of capsules, liquids and tablets from the granulated mixture with the cellulose barrier coating, wherein the dietary supplements contains approximately 97 to 99 percent stable organic trans-resveratrol to approximately 1 to 3% cis-resveratrol with low levels of impurities and low levels of microbial grown.

Assignments (6)
CORRECTIVE ASSIGNMENT TO CORRECT THE CORRESPONDENCE/ASSIGNMENTS PREVIOUSLY RECORDED ON REEL 048534 FRAME 0920. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT OF SECURITY INTEREST. Recorded Mar 15, 2019
From: MIDCAP FUNDING X TRUST
To: MIDCAP FUNDING IV TRUST
Reel/Frame 049091/0524 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2019
From: MIDCAP FUNDING X TRUST
To: MIDCAP FUNDING IV TRUST
Reel/Frame 048534/0920 →
SECURITY INTEREST Recorded Mar 9, 2017
From: PENTA MEZZANINE SBIC FUND I, L.P.
To: GOLISANO HOLDINGS, LLC
Reel/Frame 041525/0896 →
SECURITY INTEREST Recorded Nov 13, 2015
From: INNOVITAMIN ORGANICS, LLC
To: PENTA MEZZANINE SBIC FUND I, L.P.
Reel/Frame 037031/0870 →
SECURITY AGREEMENT Recorded Nov 2, 2015
From: INNOVITAMIN ORGANICS, LLC, A DELAWARE LIMITED LIABILITY COMPANY
To: MIDCAP FUNDING X TRUST, AS AGENT
Reel/Frame 037020/0762 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2011
From: BALCOMBE, NAOMI; MARU, ROBERT; VALLABHANENI, SURENDRA
To: INNOVITAMIN ORGANICS, LLC
Reel/Frame 026531/0332 →
Continuity (1)
Provisional Application 61390366 · Oct 6, 2010