IP Library Granted Patent US 9,012,668
Granted Patent B2
US 9,012,668 · App. 13/185,841 · Granted Apr 21, 2015

Method and systems for enhancing oil recovery from ethanol production byproducts

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Quick Facts
Patent No.
US 9,012,668
App. No.
13/185,841
Granted
Apr 21, 2015
Kind
B2
Abstract

Methods and related systems efficiently and effectively recover a significant amount of valuable, useable oil from byproducts formed during a dry milling process used for producing ethanol. The method may include forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct using a multi-stage evaporator, as well as recovering the oil before the final stage of the evaporator. Further, the step of recovering oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects include related methods and subsystems for recovering oil.

Claims (22)

1. A method for recovering oil in a dry milling process for producing ethanol from corn, the method comprising:

separating a whole stillage byproduct of the dry milling process with a separator into a distillers wet grains fraction, a thin stillage fraction, and an oily fraction;

combining the oily and thin stillage fractions;

evaporating the combined fractions of the oily fraction and the thin stillage fraction to remove moisture and form a concentrate of the oily and thin stillage fractions;

recovering oil from the concentrate with an additional separator;

evaporating the concentrate to further reduce the moisture content of the concentrate and form an evaporated concentrate; and

mixing the evaporated concentrate with the further reduced moisture content with the distillers wet grains fraction.

2. The method of claim 1 , further comprising adding a chemical additive during the step of recovering the oil from the concentrate.

3. The method of claim 2 , wherein adding the chemical additive comprises adjusting a pH of the concentrate.

4. The method of claim 2 , wherein adding the chemical additive comprises adding enzymes.

5. The method of claim 1 , wherein recovering oil from the concentrate with the additional separator further recovers an additional distillers wet grains fraction and an additional thin stillage concentrate fraction.

6. The method of claim 5 , wherein recovering oil from the concentrate with the additional separator comprises recovering the oil with a horizontal centrifugal three phase decanter.

7. The method of claim 5 , wherein recovering oil from the concentrate with the additional separator comprises recovering the oil with disc stack centrifuge.

8. The method of claim 5 , further comprising evaporating the additional distillers wet grains fraction and the additional thin stillage concentrate fraction to further reduce the moisture content therein.

9. A method for recovering oil in a dry milling process for producing ethanol from corn, the method comprising:

evaporating a thin stillage fraction to form a thin stillage concentrate with a reduced moisture content relative to the thin stillage fraction;

recovering oil from the thin stillage concentrate with a horizontal centrifugal three phase decanter;

evaporating the thin stillage concentrate to further reduce the moisture content of the thin stillage concentrate and form an evaporated thin stillage concentrate; and

mixing the evaporated thin stillage concentrate with a distillers wet grains fraction.

10. The method of claim 9 , further comprising adding a chemical additive during the step of recovering the oil from the concentrate.

11. The method of claim 10 , wherein adding the chemical additive comprises adjusting a pH of the concentrate.

12. The method of claim 10 , wherein adding the chemical additive comprises adding enzymes.

Assignments (4)
SECURITY AGREEMENT Recorded Feb 9, 2016
From: GREENSHIFT CORPORATION; VIRIDIUS CAPITAL LLC; GS CLEANTECH CORPORATION; GS COES (YORKVILLE I), LLC; GS DESIGN, INC.; GS RENTALS, LLC; GREENSHIFT ENGINEERING, INC.; GS AGRILFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS GLOBAL BIODIESEL, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC; GENAREX LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 037752/0763 →
SECURITY AGREEMENT Recorded Jan 8, 2013
From: ECOSYSTEM TECHNOLOGIES, LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS AGRIFUELS CORPORATION; GS BIG MANAGEMENT, LLC; GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS COES (ADRIAN I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS GLOBAL BIODIESEL, LLC; GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS TECHNOLOGY, LLC; GREENSHIFT ENGINEERING, INC. (F/K/A GS CARBON DIOXIDE TECHNOLOGIES, INC.); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL, INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; VIRIDIS CAPITAL LLC
To: YA GLOBAL INVESTMENTS, L.P., AS COLLATERAL AGENT
Reel/Frame 029588/0092 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 20, 2011
From: DAVID J. WINSNESS
To: GS ETHANOL TECHNOLOGIES, INC.
Reel/Frame 026618/0483 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 20, 2011
From: GS ETHANOL TECHNOLOGIES, INC.
To: GS CLEANTECH CORPORATION
Reel/Frame 026618/0510 →