IP Library Granted Patent US 9,242,211
Granted Patent B2
US 9,242,211 · App. 13/190,105 · Granted Jan 26, 2016

Catalysts possessing an improved resistance to poisoning

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Quick Facts
Patent No.
US 9,242,211
App. No.
13/190,105
Granted
Jan 26, 2016
Kind
B2
Abstract

The present invention relates generally to the field of catalysts for use in connection with one or more types of emissions control (e.g., emissions control associated with the combustion of one or more types of fossil fuel) and, in particular to catalyst compositions that possess an improved resistance to at least one type of poisoning. In another embodiment, the catalysts of the present invention are designed to be utilized in conjunction with an SCR and possess an improved resistance to phosphorus poisoning.

Claims (67)

1. A poison-resistant SCR catalyst composition comprising:

(i) at least one vanadium compound or metal;

(ii) at least one tungsten compound or metal;

(iii) at least one titanium compound or metal; and

(iv) at least one additional compound selected from one or more cobalt compounds or metal, one or more niobium compounds or metal, or mixtures of two or more thereof,

wherein poison-resistance in the SCR catalyst is achieved due to the molar ratio of the metal portion of component (iv) to the metal portion of component (i) falling in the range of about 10:1 to about 1:10.

2. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 9:1 to about 1:9.

3. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 8:1 to about 1:8.

4. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 7:1 to about 1:7.

5. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 4:1 to about 1:4.

6. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 3:1 to about 1:3.

7. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 2:1 to about 1:2.

8. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is about 2:1.

9. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (ii) is in the range of about 3:1 to about 1:35.

10. The catalyst composition of claim 1 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (iii) is in the range of about 1:1 to about 1:2000.

11. The catalyst composition of claim 1 , wherein the catalyst composition contains less than about 5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

12. The catalyst composition of claim 1 , wherein the catalyst composition contains less than about 2.5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

13. The catalyst composition of claim 1 , wherein the catalyst composition contains less than about 1 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

14. The catalyst composition of claim 1 , wherein the catalyst composition contains less than about 0.5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

15. The catalyst composition of claim 1 , wherein the catalyst composition is free of any one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

16. The catalyst composition of claim 1 , wherein the catalyst composition has an SO 2 to SO 3 conversion, or oxidation, rate that is about 2 percent or less.

17. The catalyst composition of claim 1 , wherein the catalyst composition is resistant to phosphorus poisoning.

18. A poison-resistant SCR catalyst composition comprising:

(i) at least one vanadium compound or metal;

(ii) at least one tungsten compound or metal;

(iii) at least one titanium compound or metal; and

(iv) at least one additional compound selected from one or more cobalt compounds or metal, one or more niobium compounds or metal, or mixtures of two or more thereof,

wherein poison-resistance in the SCR catalyst is achieved due to: (a) the molar ratio of the metal portion of component (iv) to the metal portion of component (i) falling in the range of about 10:1 to about 1:10; (b) the molar ratio of the metal portion of component (iv) to the metal portion of component (ii) falling in the range of about 3:1 to about 1:35; and (c) the molar ratio of the metal portion of component (iv) to the metal portion of component (iii) falling in the range of about 1:1 to about 1:2000.

19. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 9:1 to about 1:9.

20. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 8:1 to about 1:8.

21. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 7:1 to about 1:7.

22. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 4:1 to about 1:4.

23. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 3:1 to about 1:3.

24. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 2:1 to about 1:2.

25. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is about 2:1.

26. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (ii) is in the range of about 2.5:1 to about 1:32.5.

27. The catalyst composition of claim 18 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (iii) is in the range of about 1:1.5 to about 1:1750.

28. The catalyst composition of claim 18 , wherein the catalyst composition contains less than about 5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

29. The catalyst composition of claim 18 , wherein the catalyst composition contains less than about 2.5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

30. The catalyst composition of claim 18 , wherein the catalyst composition contains less than about 1 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

31. The catalyst composition of claim 18 , wherein the catalyst composition contains less than about 0.5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

32. The catalyst composition of claim 18 , wherein the catalyst composition is free of any one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

33. The catalyst composition of claim 18 , wherein the catalyst composition has an SO 2 to SO 3 conversion, or oxidation, rate that is about 2 percent or less.

34. The catalyst composition of claim 18 , wherein the catalyst composition is resistant to phosphorus poisoning.

35. A method for increasing the active life of a catalyst and/or preventing, reducing, mitigating and/or controlling phosphorus poisoning in an SCR catalyst, the method comprising the steps of:

(a) providing at least one SCR catalyst composition, the SCR catalyst composition comprising:

(i) at least one vanadium compound or metal;

(ii) at least one tungsten compound or metal;

(iii) at least one titanium compound or metal; and

(iv) at least one additional compound selected from one or more cobalt compounds or metal, one or more niobium compounds or metal, or mixtures of two or more thereof,

wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 10:1 to about 1:10; and

(b) supplying a NO x -containing gas to the catalyst and at least one other compound to permit the catalyst to control NO x by the conversion of NO x into another nitrogen compound or nitrogen (N 2 ) gas,

wherein the catalyst composition is resistant to phosphorus poisoning due to at least the molar ratio of component (iv) to component (i).

36. The method of claim 35 , wherein the at least one other compound is ammonia and the catalyst composition is an SCR catalyst.

37. The method of claim 35 , wherein the method is applied to combustion, waste or flue gasses of a combustion process selected from a fossil fuel powered mobile, or stationary, combustion process, a biomass combustion process, or a waste combustion process.

38. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 9:1 to about 1:9.

39. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 8:1 to about 1:8.

40. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 7:1 to about 1:7.

41. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 4:1 to about 1:4.

42. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 3:1 to about 1:3.

43. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is in the range of about 2:1 to about 1:2.

44. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (i) is about 2:1.

45. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (ii) is in the range of about 3:1 to about 1:35.

46. The method of claim 35 , wherein the molar ratio of the metal portion of component (iv) to the metal portion of component (iii) is in the range of about 1:1 to about 1:2000.

47. The method of claim 35 , wherein the catalyst composition contains less than about 5 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

48. The method of claim 35 , wherein the catalyst composition contains less than about 1 weight percent of one or more binary metal oxides, or ternary metal oxides, formed from any suitable combination of one or two of Co and/or Nb in combination with either one or both of V and W.

49. The method of claim 35 , wherein the catalyst composition has an SO 2 to SO 3 conversion, or oxidation, rate that is about 2 percent or less.

Assignments (14)
SECURITY INTEREST Recorded Jul 18, 2025
From: BABCOCK & WILCOX ENTERPRISES, INC.; THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX CANADA CORP.; BABCOCK & WILCOX FPS INC.
To: B. RILEY FINANCIAL, INC.
Reel/Frame 072053/0943 →
SECURITY INTEREST Recorded May 23, 2025
From: BABCOCK & WILCOX ENTERPRISES, INC.; THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX CANADA CORP.; BABCOCK & WILCOX FPS INC.
To: GLAS TRUST COMPANY LLC
Reel/Frame 071371/0835 →
SECURITY INTEREST Recorded Mar 3, 2025
From: BABCOCK & WILCOX ENTERPRISES, INC.; THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX CANADA CORP.; BABCOCK & WILCOX FPS INC.
To: PENSION BENEFIT GUARANTY CORPORATION
Reel/Frame 070380/0647 →
RELEASE OF SECURITY INTEREST Recorded Sep 13, 2024
From: MSD PCOF PARTNERS XLV, LLC
To: THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; AMERICON LLC
Reel/Frame 069017/0362 →
SECURITY INTEREST Recorded Jan 19, 2024
From: BABCOCK & WILCOX ENTERPRISES, INC.; THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX CANADA CORP.; BABCOCK & WILCOX FPS INC.
To: AXOS BANK, AS ADMINISTRATIVE AGENT
Reel/Frame 066354/0765 →
SECURITY INTEREST Recorded Jul 22, 2021
From: THE BABCOCK & WILCOX COMPANY (F/K/A BABCOCK & WILCOX POWER GENERATION GROUP, INC.); BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX TECHNOLOGY, LLC; DIAMOND POWER INTERNATIONAL, LLC (F/K/A DIAMOND POWER INTERNATIONAL, INC.)
To: MSD PCOF PARTNERS XLV, LLC, AS AGENT
Reel/Frame 056962/0486 →
RELEASE OF SECURITY INTEREST Recorded Jul 1, 2021
From: BANK OF AMERICA, N.A.
To: DIAMOND POWER INTERNATIONAL, LLC (F/K/A DIAMOND POWER INTERNATIONAL, INC.); MEGTEC TURBOSONIC TECHNOLOGIES, INC.; THE BABCOCK & WILCOX COMPANY (F/K/A BABCOCK & WILCOX POWER GENERATION GROUP, INC.); BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX TECHNOLOGY, LLC (F/K/A MCDERMOTT TECHNOLOGY, INC.); SOFCO-EFS HOLDINGS LLC; BABCOCK & WILCOX MEGTEC, LLC
Reel/Frame 057337/0823 →
RELEASE OF SECURITY INTEREST Recorded May 17, 2018
From: LIGHTSHIP CAPITAL LLC
To: BABCOCK & WILCOX ENTERPRISES, INC.; THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX MEGTEC, LLC; MEGTEC TURBOSONIC TECHNOLOGIES, INC.; BABCOCK & WILCOX UNIVERSAL, INC.; BABCOCK & WILCOX TECHNOLOGY, LLC
Reel/Frame 046182/0829 →
SECURITY INTEREST Recorded Aug 10, 2017
From: THE BABCOCK & WILCOX COMPANY; DIAMOND POWER INTERNATIONAL, LLC; BABCOCK & WILCOX MEGTEC, LLC; MEGTEC TURBOSONIC TECHNOLOGIES, INC.; BABCOCK & WILCOX UNIVERSAL, INC.; BABCOCK & WILCOX TECHNOLOGY, LLC
To: LIGHTSHIP CAPITAL LLC
Reel/Frame 043515/0001 →
CHANGE OF NAME Recorded Sep 24, 2015
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
To: THE BABCOCK & WILCOX COMPANY
Reel/Frame 036675/0434 →
SECURITY INTEREST Recorded Jul 28, 2015
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC. (TO BE RENAMED THE BABCOCK AND WILCOX COMPANY)
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036201/0598 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jun 27, 2012
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 028456/0706 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2012
From: GUO, XIAOYU
To: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
Reel/Frame 028316/0751 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 9, 2011
From: GUO, XIAOYU
To: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
Reel/Frame 026720/0222 →