IP Library Granted Patent US 9,115,467
Granted Patent B2
US 9,115,467 · App. 13/195,721 · Granted Aug 25, 2015

Methods and systems for solvent purification

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Quick Facts
Patent No.
US 9,115,467
App. No.
13/195,721
Granted
Aug 25, 2015
Kind
B2
Abstract

A method including: (a) contacting lime with an extract including an S1 solvent carrying a contaminant load to form a lime treated extract; and (b) reducing the contaminant load by removing solids.

Claims (12)

1. A method comprising:

(a) contacting lime with an extract carrying a contaminant load comprising an S1 solvent, to form a lime treated extract and solids;

(b) reducing said contaminant load by removing at least a portion of said solids from said lime treated extract and solids;

(c) carbonating said removed solids or said lime with CO 2 gas to form a slurry comprising calcium carbonate; and

(d) contacting said slurry comprising calcium carbonate with additional lime.

2. The method of claim 1 , wherein said contaminant load is reduced by more than 20% (wt/wt).

3. The method of claim 1 , wherein the method further comprises prior to step (a) contacting an extractant comprising said S1 solvent with an acid hydrolyzate of a lignocellulosic substrate to produce an acid-carrying extract; and de-acidifying said acid-carrying extract to produce said extract carrying a contaminant load.

4. A method comprising:

(a) cyclically contacting a first portion of an extractant comprising Si solvent with an acid hydrolyzate of a lignocellulosic substrate to produce an acid-reduced hydrolyzate and an extract comprising acid and S1 solvent carrying a contaminant load;

(b) de-acidifying said extract to form a de-acidified extract with S1 solvent carrying the contaminant load; and

(c) cyclically routing a second portion of said extractant comprising S1 solvent carrying a contaminant load to a decontamination module which applies a contaminant reduction process to said second portion to produce an extractant with a reduced contaminant load.

5. The method of claim 4 , wherein said contaminant reduction process comprises treatment of said second portion of said extractant with lime.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2024
From: VIRDIA LLC
To: INTERNATIONAL N&H DENMARK APS
Reel/Frame 069873/0615 →
CHANGE OF NAME Recorded Mar 18, 2021
From: VIRDIA, INC.
To: VIRDIA, LLC
Reel/Frame 055633/0305 →
RELEASE OF SECURITY INTEREST Recorded Mar 12, 2021
From: TRIPLEPOINT CAPITAL LLC
To: VIRDIA, INC.
Reel/Frame 055599/0793 →
SECURITY AGREEMENT Recorded Nov 1, 2013
From: VIRDIA, INC.
To: TRIPLEPOINT CAPITAL LLC
Reel/Frame 031536/0844 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 29, 2013
From: VIRDIA LTD
To: VIRDIA, INC.
Reel/Frame 031510/0052 →