IP Library Granted Patent US 9,089,480
Granted Patent B2
US 9,089,480 · App. 13/203,756 · Granted Jul 28, 2015

Anionic oil-in-water emulsions containing prostaglandins and uses thereof

Inventors: Frederic Lallemand (Fresnes, FR); Betty Phillips (Antony, FR); Jean-Sebastien Garrigue (Verrieres le Buisson, FR)
Assignee: SANTEN SAS
A61K9/0048A61K31/5575A61K47/10A61K47/26A61K47/44
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Quick Facts
Patent No.
US 9,089,480
App. No.
13/203,756
Granted
Jul 28, 2015
Kind
B2
Abstract

A colloidal anionic oil-in-water emulsion includes a prostaglandin, an oil having a iodine value ≦2, a surfactant and water, provided the anionic oil-in-water emulsion does not contain polyvinyl alcohol. The use of the anionic oil-in-water emulsions for enhancing the stability of the prostaglandins, for the treatment of ocular hypertension and/or glaucoma, for promoting growth of eyelashes and/or for treating eyelash hypotrichosis is also described.

Claims (30)

1. A colloidal oil-in-water emulsion comprising

a prostaglandin F 2alpha

an oil having a iodine value ≦2,

a non-ionic surfactant selected from the group consisting of poloxamers, tyloxapol, polysorbates, sorbitan esters, polyoxyl stearates and mixtures thereof, and

water,

wherein the non-ionic surfactant, the amount of which is comprised between 0.0005 and 1% in weight by weight of said emulsion, releases negative charges during the manufacturing process of the emulsion, said emulsion having a negative zeta potential lower than −10 mV, said emulsion not containing polyvinyl alcohol, and said emulsion being free of cationic surfactant.

2. The colloidal oil-in-water emulsion according to claim 1 , wherein the prostaglandin F 2alpha is selected from the group consisting of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; an ester or an amide prodrug of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; and mixtures thereof.

3. The colloidal oil-in-water emulsion according to claim 1 , wherein the oil is selected from the group consisting of oily fatty acids, oily fatty alcohols, fatty acids esters, vegetable oils, animal oils, mineral oils, liquid paraffin, semi-synthetic oils and mixtures thereof.

4. The colloidal oil-in-water emulsion according to claim 3 , wherein the oil is medium chain triglycerides (MCT).

5. The colloidal oil-in-water emulsion according to claim 1 , wherein the amount of prostaglandin F 2alpha relative to the total weight of the emulsion is comprised between 0.001 to 1% w/w.

6. The colloidal oil-in-water emulsion according to claim 1 , wherein the amount of the oil relative to the total weight of the emulsion is not higher than 7% w/w.

7. The colloidal oil-in-water emulsion according to claim 1 , wherein the emulsion is free of any buffer.

8. A method for treating ocular hypertension and/or glaucoma comprising administering to a subject in need thereof a colloidal oil-in-water emulsion comprising

a prostaglandin F 2alpha

an oil having a iodine value ≦2,

a non-ionic surfactant selected from the group consisting of poloxamers, tyloxapol, polysorbates, sorbitan esters, polyoxyl stearates and mixtures thereof, and

water,

wherein the non-ionic surfactant, the amount of which is comprised between 0.0005 and 1% in weight by weight of said emulsion, releases negative charges during the manufacturing process of the emulsion, said emulsion having a negative zeta potential lower than −10 mV, said emulsion not containing polyvinyl alcohol, and said emulsion being free of cationic surfactant.

9. The method according to claim 8 , wherein the prostaglandin F 2alpha is selected from the group consisting of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; an ester or an amide prodrug of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; and mixtures thereof.

10. The method according to claim 8 , wherein the oil is selected from the group consisting of oily fatty acids, oily fatty alcohols, fatty acids esters, vegetable oils, animal oils, mineral oils, liquid paraffin, semi-synthetic oils and mixtures thereof.

11. The method according to claim 10 , wherein the oil is medium chain triglycerides (MCT).

12. A delivery device comprising a colloidal oil-in-water emulsion comprising

a prostaglandin F 2alpha

an oil having a iodine value ≦2,

a non-ionic surfactant selected from the group consisting of poloxamers, tyloxapol, polysorbates, sorbitan esters, polyoxyl stearates and mixtures thereof, and

water,

wherein the non-ionic surfactant, the amount of which is comprised between 0.0005 and 1% in weight by weight of said emulsion, releases negative charges during the manufacturing process of the emulsion, said emulsion having a negative zeta potential lower than −10 mV, said emulsion not containing polyvinyl alcohol, and said emulsion being free of cationic agent.

13. The delivery device according to claim 12 , wherein the prostaglandin prostaglandin F 2alpha is selected from the group consisting of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; an ester or an amide prodrug of latanoprost, isopropyl unoprostone, travoprost, bimatoprost, tafluprost ; and mixtures thereof.

14. The colloidal oil-in-water emulsion according to claim 1 , wherein the amount of the surfactant relative to the total weight of the emulsion is between 0.001 and 0.5% w/w.

15. The colloidal oil-in-water emulsion according to claim 14 , wherein the amount of the surfactant relative to the total weight of the emulsion is between 0.01 and 0.5% w/w.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 19, 2013
From: NOVAGALI PHARMA SA
To: SANTEN SAS
Reel/Frame 031667/0321 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 6, 2011
From: LALLEMAND, FREDERIC; PHILIPS, BETTY; GARRIGUE, JEAN-SEBASTIEN
To: NOVAGALI PHARMA SA
Reel/Frame 027026/0498 →
Priority Claims (1)
EP 09305203 · Mar 4, 2009 · regional
Continuity (2)
Provisional Application 61157347 · Mar 4, 2009
Related Publication 20110319488A1 · Dec 29, 2011