IP Library Granted Patent US 9,688,631
Granted Patent B2
US 9,688,631 · App. 13/203,759 · Granted Jun 27, 2017

Thermosetting ring-opening metathesis polymerization materials with thermally degradable linkages

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Quick Facts
Patent No.
US 9,688,631
App. No.
13/203,759
Granted
Jun 27, 2017
Kind
B2
Abstract

The present invention provides a new class of thermosetting ring-opening metathesis polymerization materials based on norbornene and oxanorbornene dicarboximide moieties containing at least one acetal ester group linkage. The acetal ester group is degradable when subjected to heat or acidic aqueous hydrolysis. The polymerization materials can be used in reworkable thermosetting compositions. R1-Rs, X, and n are defined herein.

Claims (12)

1. A compound represented by the following structure:

wherein X is independently CH 2 or O; R 1 is selected from the group consisting of unsubstituted or substituted alkyl, cycloalkyl, alkenyl, and aryl groups, wherein any of the before mentioned groups may be present with or without heteroatoms; R 2 is n-propyl and n is 1 to 3.

2. The compound according to claim 1 , wherein X is CH 2 ; R 1 selected from the group consisting of C 1 -C 8 alkyl and alkenyl groups, cyclopentane, cyclohexane, and cycloheptane groups, wherein any of the before mentioned groups may be present with or without heteroatoms; and n is 1 to 3.

3. A compound represented by the following structure:

4. A compound represented by the following general structure:

wherein X is independently CH 2 or O; R 1 , and R 3 are independently selected from the group consisting of unsubstituted or substituted alkyl, cycloalkyl, alkenyl, and aryl groups, wherein any of the before mentioned groups may be present with or without heteroatoms; wherein each R 1 group is further independently selected from any of the before mentioned groups.

5. The compound according to claim 4 , wherein X is CH 2 ; R 1 and R 3 are independently selected from the group consisting of C 1 -C 8 alkyl and alkenyl groups, cyclopentane, cyclohexane, and cycloheptane groups, wherein any of the before mentioned groups may be present with or without heteroatoms.

6. The compound according to claim 5 , wherein the compound is represented by the following structure:

7. An adhesive, coating, encapsulation, personal care, oilfield, membrane, agricultural, or cleaning composition comprising a compound represented by the following structure:

wherein X is independently CH 2 or O; R 1 is selected from the group consisting of unsubstituted or substituted alkyl, cycloalkyl, alkenyl, and aryl groups, wherein any of the before mentioned groups may be present with or without heteroatoms; R 2 is n-propyl, and n is 1 to 3.

8. An adhesive, coating, encapsulation, personal care, oilfield, membrane, agricultural, or cleaning composition comprising a compound represented by the following general structure:

wherein X is independently CH 2 or O; R 1 , and R 3 are independently selected from the group consisting of unsubstituted or substituted alkyl, cycloalkyl, alkenyl, and aryl groups, wherein any of the before mentioned groups may be present with or without heteroatoms; wherein each R 1 group is further independently selected from any of the before mentioned groups.

Assignments (8)
RELEASE OF SECURITY INTEREST Recorded Jan 10, 2020
From: THE BANK OF NOVA SCOTIA
To: AVOCA LLC; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES LLC
Reel/Frame 051557/0504 →
SECURITY AGREEMENT Recorded Jul 3, 2017
From: AVOCA, INC.; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES, INC.
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 043084/0753 →
CHANGE OF NAME Recorded May 24, 2017
From: ISP INVESTMENTS INC.
To: ISP INVESTMENTS LLC
Reel/Frame 042560/0842 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 8, 2017
From: KHOSRAVI, EZAT; MUSA, OSAMA M.
To: ISP INVESTMENTS INC.
Reel/Frame 042273/0922 →
CHANGE OF NAME Recorded May 8, 2017
From: ISP INVESTMENTS INC.
To: ISP INVESTMENTS LLC
Reel/Frame 042419/0987 →
RELEASE OF SECURITY AGREEMENT Recorded Aug 28, 2013
From: THE BANK OF NOVA SCOTIA
To: ASHLAND INC.; HERCULES INCORPORATED; ISP INVESTMENTS INC.; ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC
Reel/Frame 031106/0682 →
SECURITY AGREEMENT Recorded Oct 6, 2011
From: ISP INVESTMENTS INC.
To: ASHLAND INC.
Reel/Frame 027023/0500 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY DATA ADDRESS CHANGE EMAIL ADDRESS PREVIOUSLY RECORDED ON REEL 027023 FRAME 0500. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY AGREEMENT. Recorded Oct 6, 2011
From: ISP INVESTMENTS INC.
To: THE BANK OF NOVA SCOTIA, GWS LOAN OPERATIONS
Reel/Frame 027027/0526 →