IP Library Granted Patent US 8,835,377
Granted Patent B2
US 8,835,377 · App. 13/219,132 · Granted Sep 16, 2014

Oral delivery of peptide pharmaceutical compositions

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Quick Facts
Patent No.
US 8,835,377
App. No.
13/219,132
Granted
Sep 16, 2014
Kind
B2
Abstract

Bioavailability of peptide active agents to be administered orally is enhanced by a pharmaceutical composition providing targeted release of the peptide to the intestine by combining the composition with an absorption enhancer. Bioavailability is further significantly increased by administering the composition in an acid-resistant protective vehicle which transports components of the invention through the stomach. The composition may optionally further include a sufficient amount of a pH-lowering agent to lower local intestinal pH. All components are released together into the intestine with the peptide.

Claims (30)

1. A solid oral single dosage form comprising:

a peptide comprising a 2,6-dimethyltyrosine (Dmt)

residue or a prodrug thereof; and

at least one pharmaceutically acceptable pH-lowering agent comprising a carboxylic acid, wherein the pH-lowering agent is present in the single dosage form in a quantity which, if added to 10 milliliters of 0.1M aqueous sodium bicarbonate solution, would be sufficient to lower the pH of the solution to no higher than 5.5.

2. The single dosage form of claim 1 wherein the peptide further comprises an arginine residue, a phenylalanine residue, and a lysine residue.

3. The single dosage form of claim 1 wherein the pH-lowering agent is citric acid.

4. The single dosage form of claim 1 further comprising at least one absorption enhancer.

5. The single dosage form of claim 4 wherein the absorption enhancer is an acylcarnitine.

6. The single dosage form of claim 5 wherein the acylcarnitine is lauroyl carnitine.

7. The single dosage form of claim 1 further comprising an enteric coating.

8. The single dosage form of claim 7 wherein the enteric coating is present at a weight which is no more than 20% of the weight of the remainder of the single dosage form excluding the enteric coating.

9. The single dosage form of claim 7 wherein the enteric coating is present at a weight which is no more than 5-15% of the weight of the remainder of the single dosage form excluding said enteric coating.

10. The single dosage form of claim 1 wherein the pH-lowering agent is present in the single dosage form in a quantity which, if added to 10 milliliters of 0.1M aqueous sodium bicarbonate solution, would be sufficient to lower the pH of the solution to no higher than 3.5.

11. The single dosage form of claim 1 formulated as a capsule.

12. A solid oral single dosage form comprising:

a deltorphin analog or a prodrug thereof comprising

a dimethylphenylalanine residue; and

at least one pharmaceutically acceptable pH-lowering agent comprising a carboxylic acid, wherein the pH-lowering agent is present in the single dosage form in a quantity which, if added to 10 milliliters of 0.1M aqueous sodium bicarbonate solution, would be sufficient to lower the pH of the solution to no higher than 5.5.

13. The single dosage form of claim 12 wherein the deltorphin analog is Tyrosine-D-alanine-Xaa-Glutamic Acid-Valine-Valine-Glycine-NH 2 , wherein Xaa is L-or D-dimethylphenylalanine

14. The single dosage form of claim 12 wherein the pH-lowering agent is citric acid.

15. The single dosage form of claim 12 further comprising an absorption enhancer.

16. The single dosage form of claim 15 wherein the absorption enhancer is lauroyl carnitine.

17. The single dosage form of claim 12 further comprising an enteric coating that is present at a weight which is no more than 20% of the weight of the remainder of the single dosage form excluding the enteric coating.

18. The single dosage form of claim 12 further comprising an enteric coating that is present at a weight which is no more than 5-15% of the weight of the remainder of the single dosage form excluding said enteric coating.

19. The single dosage form of claim 12 wherein the pH-lowering agent is present in the single dosage form in a quantity which, if added to 10 milliliters of 0.1M aqueous sodium bicarbonate solution, would be sufficient to lower the pH of the solution to no higher than 3.5.

20. The single dosage form of claim 12 formulated as a capsule.

21. The single dosage form of claim 1 comprising a therapeutically-effective amount of the peptide comprising the 2,6-dimethyltyrosine (Dmt) residue or prodrug thereof to achieve analgesia.

22. The single dosage form of claim 12 comprising a therapeutically-effective amount of the deltorphin analog or prodrug thereof comprising the dimethylphenylalanine residue to achieve analgesia.

23. A method for relieving pain comprising administering to a subject in need thereof a therapeutically-effective amount of the single dosage form of claim 1 .

24. A method for relieving pain comprising administering to a subject in need thereof a therapeutically-effective amount of the single dosage form of claim 12 .

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Jun 28, 2023
From: CADENCE BANK, A MISSISSIPPI BANK AND SUCCESSOR BY MERGER TO CADENCE BANK, N.A., A NATIONAL BANKING ASSOCIATION, AS AGENT
To: ENTERIS BIOPHARMA, INC.
Reel/Frame 064149/0741 →
SECURITY INTEREST Recorded Aug 26, 2019
From: ENTERIS BIOPHARMA, INC.
To: CADENCE BANK, N.A.
Reel/Frame 050174/0428 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NATURE OF CONVEYANCE PREVIOUSLY RECORDED ON REEL 039184 FRAME 0797. ASSIGNOR(S) HEREBY CONFIRMS THE NUNC PRO TUNC ASSIGNMENT EFFECTIVE 02/01/2016. Recorded Aug 15, 2016
From: UGP THERAPEUTICS, INC.
To: ENTERIS BIOPHARMA, INC.
Reel/Frame 039682/0212 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 19, 2016
From: UGP THERAPEUTICS, INC.
To: ENTERIS BIOPHARMA, INC.
Reel/Frame 039184/0797 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 23, 2013
From: UNIGENE LABORATORIES, INC.
To: UGP THERAPEUTICS, INC.
Reel/Frame 030856/0340 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 7, 2012
From: MEHTA, NOZER M.; STERN, WILLIAM; GILLIGAN, JAMES P.
To: UNIGENE LABORATORIES INC.
Reel/Frame 028913/0511 →