Method for removing contaminants from boron powder
View Patent ↗Methods for removing an organic contaminant from contaminated boron powder are provided. One method includes providing a contaminated boron powder, the boron powder being comingled with an organic contaminant. The method also includes placing the contaminated boron powder and the organic contaminant comingled therewith onto an inert container. The method includes placing the inert container, the contaminated boron powder, and the organic contaminant comingled therewith, into an enclosed space. A heat source is provided in the enclosed space. The method also includes heating the contaminated boron powder and the organic contaminant comingled therewith to an elevated temperature. The method includes altering the organic contaminant so as to reduce the amount of the organic contaminant comingled with the boron powder. Another method includes reducing the amount of the organic contaminant comingled with the boron powder to not more than about 0.1 weight percent of soluble residue.
1. A method of removing a contaminant from contaminated boron powder, the method including:
providing a contaminated boron powder, the boron powder being comingled with an organic contaminant;
placing the contaminated boron powder and the contaminant comingled therewith onto an inert container;
placing the inert container, the contaminated boron powder, and the contaminant comingled therewith, into an enclosed space;
providing a heat source for the enclosed space;
heating the contaminated boron powder and the contaminant comingled therewith to an elevated temperature, wherein the elevated temperature is about 500° C.; and
altering the contaminant so as to reduce an amount of the organic contaminant.
2. The method according to claim 1 , wherein the step of altering the contaminant is breaking down a carbon chain forming the organic contaminant.
3. The method according to claim 1 , wherein the step of altering the contaminant is vaporizing the organic contaminant.
4. The method according to claim 1 , wherein the method further includes providing a special selected qas atmosphere within the enclosed space.
5. The method according to claim 1 , further including the step of cooling the boron powder to less than about 100° C. prior to removal of the boron powder from the enclosed space.
6. A method of removing a contaminant from contaminated boron powder, the method including:
providing a contaminated boron powder, the boron powder being comingled with an organic contaminant;
placing the contaminated boron powder and the contaminant comingled therewith onto an inert container;
placing the inert container, the contaminated boron powder, and the contaminant comingled therewith, into an enclosed space;
providing a heat source for the enclosed space;
heating the contaminated boron powder and the contaminant comingled therewith to an elevated temperature; and
altering the contaminant so as to reduce an amount of the organic contaminant;
wherein the method further includes providing a selected qas atmosphere within the enclosed space and the special selected qas atmosphere is hydrogen.
7. A method of removing a contaminant from contaminated boron powder, the method including:
providing a contaminated boron powder, the boron powder being comingled with an organic contaminant;
placing the contaminated boron powder and the contaminant comingled therewith onto an inert container;
placing the inert container, the contaminated boron powder, and the contaminant comingled therewith, into an enclosed space;
providing a heat source for the enclosed space;
heating the contaminated boron powder and the contaminant comingled therewith to an elevated temperature, wherein the elevated temperature is about 500° C.; and
altering the contaminant so that the amount of the organic contaminant in the boron powder after a processing cycle is not more than about 0.1 weight percent of soluble residue.
8. The method according to claim 7 , wherein the step of altering the contaminant is breaking down a carbon chain forming the organic contaminant.
9. The method according to claim 7 , wherein the step of altering the contaminant is vaporizing the organic contaminant.
10. The method according to claim 7 , wherein the method further includes providing a special selected gas atmosphere within the enclosed space.
11. The method according to claim 10 , wherein the special selected gas atmosphere is hydrogen.
12. The method according to claim 7 , further including the step of cooling the boron powder to less than about 100° C. prior to removal of the boron powder from the enclosed space.