IP Library Granted Patent US 8,679,224
Granted Patent B2
US 8,679,224 · App. 13/222,002 · Granted Mar 25, 2014

Hydrogen, lithium, and lithium hydride production

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Quick Facts
Patent No.
US 8,679,224
App. No.
13/222,002
Granted
Mar 25, 2014
Kind
B2
Abstract

A method of producing high purity lithium metal is provided, where gaseous-phase lithium metal is extracted from lithium hydride and condensed to form solid high purity lithium metal. The high purity lithium metal may be hydrided to provide high purity lithium hydride.

Claims (13)

1. A method of producing hydrogen and lithium comprising:

heating lithium hydride to form liquid-phase lithium hydride;

reducing an ambient pressure over the liquid-phase lithium hydride;

extracting hydrogen and gaseous-phase lithium metal from the liquid-phase lithium hydride;

condensing the gaseous-phase lithium metal as purified solid-phase lithium metal; and

melting the solid-phase lithium metal to form refined liquid-phase lithium metal.

2. The method of claim 1 further comprising hydriding the refined liquid-phase lithium metal.

3. The method of claim 1 further comprising:

hydriding the refined liquid-phase lithium metal to form re-charged lithium hydride; and

again performing the steps of claim 1 at least one time using the re-charged lithium hydride as the lithium material.

4. The method of claim 1 further comprising retarding a formation of a barrier crust adjacent the liquid-phase lithium hydride.

5. The method of claim 4 wherein the step of retarding the formation of the barrier crust comprises sparging the liquid-phase lithium hydride with an inert gas.

6. The method of claim 4 wherein the step of retarding the formation of the barrier crust comprises agitating the liquid lithium hydride with an energy having a periodic waveform.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2014
From: BABCOCK & WILCOX TECHNICAL SERVICES Y-12, LLC
To: CONSOLIDATED NUCLEAR SECURITY, LLC
Reel/Frame 033756/0649 →
CONFIRMATORY LICENSE Recorded Jun 18, 2012
From: B&W Y-12, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 028391/0288 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 1, 2011
From: BROWN, SAM W.; SPENCER, LARRY S.; PHILLIPS, MICHAEL R.; POWELL, G. LOUIS; CAMPBELL, PEGGY J.
To: BABCOCK & WILCOX TECHNICAL SERVICES Y-12, LLC
Reel/Frame 026846/0388 →