IP Library Granted Patent US 9,643,144
Granted Patent B2
US 9,643,144 · App. 13/224,443 · Granted May 9, 2017

Method to generate and disperse nanostructures in a composite material

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Quick Facts
Patent No.
US 9,643,144
App. No.
13/224,443
Granted
May 9, 2017
Kind
B2
Abstract

A method of making a nanostructure-reinforced composite comprises providing matrix particles in a reactor; fluidizing the matrix particles; introducing a nanostructure material into the reactor; homogeneously dispersing the nanostructure material; uniformly depositing the nanostructure material on the matrix particles to form a composite powder; generating a nanostructure on the matrix particles from the nanostructure material; and processing the composite powder to form the nanostructure-reinforced composite having a matrix formed from the matrix particles. The nanostructures are evenly distributed in the matrix of the nanostructure-reinforced composite.

Claims (21)

1. A method of making a nanostructure-reinforced composite comprising:

providing matrix particles in a reactor, the matrix particles comprising a metal selected from magnesium, aluminum, titanium, manganese, iron, cobalt, nickel, copper, molybdenum, tungsten, palladium, chromium, ruthenium, gold, silver, zinc, zirconium, vanadium, silicon, or a combination thereof;

fluidizing the matrix particles;

introducing a nanostructure material into the reactor;

homogeneously dispersing the nanostructure material;

uniformly depositing the nanostructure material on the matrix particles to form a composite powder;

mechanically alloying the composite powder to generate a nanostructure on the matrix particles from the nanostructure material; and

processing the composite powder to form the nanostructure-reinforced composite having a matrix formed from the matrix particles,

wherein the nano structures are evenly distributed in the matrix of the nanostructure-reinforced composite.

2. The method of claim 1 , wherein the matrix particles are about 0.5 μm to about 500 μm.

3. The method of claim 1 , wherein the amount of the nanostructure material on the matrix particles is about 0.001 wt. % to about 50 wt. % based on the weight of the composite powder.

4. The method of claim 1 , wherein uniformly depositing the nanostructure material on the matrix particles is a chemical process.

5. The method of claim 1 , wherein uniformly depositing the nanostructure material on the matrix particles is a physical process.

6. The method of claim 1 , wherein processing the composite powder comprises mechanical alloying, sintering, hot pressing, spark plasma sintering, extrusion, curing, molding, or a combination thereof.

7. The method of claim 1 , wherein processing the composite powder comprises

mechanical alloying the composite powder using a ball mill; and

sintering the composite powder to form the nanostructure-reinforced composite.

8. The method of claim 1 , wherein the nanostructure material comprises nanoparticles, nanotubes, fullerenes, nanowires, nanodots, nanorods, sheets, graphene, nanographite, C1-C4 alkane, C1-C4 alkene, C1-C4 alkyne, benzene, metal, metal oxide, nanodiamonds, polysilsesquioxanes, inorganic nanoparticles, nanoclays, metal nanoparticles, or combinations thereof.

9. The method of claim 1 , wherein the matrix particles fragment into smaller particles during mechanical alloying.

10. The method of claim 1 , wherein additional nanostructure material is added to the composite powder during mechanical alloying.

11. The method of claim 1 , wherein the matrix and nanostructures form a monolith with substantially all of the matrix particles being integrated into the matrix.

Assignments (3)
CHANGE OF NAME Recorded Apr 5, 2022
From: BAKER HUGHES, A GE COMPANY, LLC
To: BAKER HUGHES HOLDINGS LLC
Reel/Frame 059596/0405 →
CHANGE OF NAME Recorded Mar 23, 2022
From: BAKER HUGHES INCORPORATED
To: BAKER HUGHES, A GE COMPANY, LLC
Reel/Frame 059485/0502 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2011
From: XU, ZHIYUE; AGRAWAL, GAURAV
To: BAKER HUGHES INCORPORATED
Reel/Frame 027275/0667 →