Heater and related methods therefor
View Patent ↗The invention relates generally to heaters and methods of using the heaters. In certain embodiments, a heater includes a pressure shell having a cylindrical heating cavity, an annular heat shield disposed within the cylindrical heating cavity, and at least one heating element disposed within an interior volume of the annular heat shield. In another embodiment, a method of preparing a trichlorosilane includes introducing a reactant stream comprising silicon tetrachloride into a heater, passing electrical current through a heating element to heat the reactant stream, and introducing the heated reactant stream into a reactor.
1. A method of facilitating trichlorosilane production, comprising:
introducing a reactant stream containing at least one of silicon tetrachloride and hydrogen into an inlet of a heater having:
a pressure shell enclosing a heating chamber;
a heat shield shaped as an open-ended cylinder, said cylindrical heat shield being disposed within the heating chamber and concentric therewith;
at least one heating element shaped as an open-ended cylinder, said cylindrical heating element being disposed within an interior volume of the cylindrical heat shield and concentric therewith; and
a spacer shaped as a closed-ended cylinder, said spacer being disposed within an interior volume of the cylindrical heating element;
causing at least a portion of said reactant stream to flow through an annular heating region defined by said cylindrical heat shield and said spacer, thereby bringing the reactant stream into direct physical contact with the cylindrical heating element; and
directing said reactant stream through an outlet of the heater and into an inlet of any of a hydrochlorination reactor and a hydrogenation reactor.
2. The method of claim 1 , further comprising applying electrical current to said at least one heating element from at least one electrical power source.
3. The method of claim 1 , wherein the reactant stream flows from the inlet to the outlet through a channel that does not reverse its direction.