IP Library Granted Patent US 8,673,777
Granted Patent B2
US 8,673,777 · App. 13/249,818 · Granted Mar 18, 2014

In-line deposition system and process for deposition of a thin film layer

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Quick Facts
Patent No.
US 8,673,777
App. No.
13/249,818
Granted
Mar 18, 2014
Kind
B2
Abstract

An apparatus for vapor deposition of a sublimated source material as a thin film on a substrate is provided. The apparatus includes a receptacle configured to hold a source material and a distribution plate positioned above the receptacle. The distribution plate defines a pattern of passages therethrough. The apparatus also includes a conveyor configured to travel in a continuous loop such that its transfer surface passes above the distribution plate in a first direction to receive thereon sublimated source material passing through the passages of the distribution plate. The conveyor is also configured to travel in a second direction while carrying a substrate on its raised edges. A heating system heats the conveyor while it travels in the second direction to transfer the source material from the transfer surface to the substrate. A process is provided for vapor deposition of a sublimated source material to form thin film.

Claims (37)

1. An apparatus for vapor deposition of a sublimated source material as a thin film on a substrate, said apparatus comprising:

a receptacle configured to hold a source material;

a distribution plate positioned above the receptacle, wherein the distribution plate defines a pattern of passages therethrough;

a conveyor defining a pair of raised edges and a transfer surface such that the raised edges are raised with respect to the transfer surface, wherein the conveyor is configured to travel in a continuous loop such that the transfer surface passes above the distribution plate in a first direction to receive thereon sublimated source material passing through the passages of the distribution plate, and wherein the conveyor is configured to travel in a second direction while carrying a substrate on the raised edges;

a heating system configured to heat the conveyor while it travels in the second direction; and

a cooling system configured to cool the conveyor while it travels in the first direction, wherein the heating system and the cooling system are positioned within the continuous loop defined by the conveyor.

2. The apparatus as in claim 1 , wherein the conveyor is configured to support the substrate only along its raised edges.

3. The apparatus as in claim 1 , further comprising:

a heating element positioned to sublimate the source material in the receptacle.

4. The apparatus as in claim 1 , further comprising:

a shutter plate between the receptacle and the distribution plate, wherein the shutter plate is movable between an open position and a closed position.

5. The apparatus as in claim 1 , further comprising:

a feed system configured to supply source material to the receptacle.

6. The apparatus as in claim 1 , wherein the conveyor comprises graphite.

7. The apparatus as in claim 1 , further comprising:

a second heating system configured to heat the substrate as it is being carried by the conveyor in the second direction.

8. An apparatus for vapor deposition of a sublimated source material as a thin film on a substrate, said apparatus comprising:

a receptacle configured to hold a source material;

a distribution plate positioned above the receptacle, wherein the distribution plate defines a pattern of passages therethrough;

a conveyor defining a pair of raised edges and a transfer surface such that the raised edges are raised with respect to the transfer surface, wherein the conveyor is configured to travel in a continuous loop such that the transfer surface passes above the distribution plate in a first direction to receive thereon sublimated source material passing through the passages of the distribution plate, and wherein the conveyor is configured to travel in a second direction while carrying a substrate on the raised edges; and

a heating system configured to heat the conveyer while it travels in the second direction,

wherein the substrate defines an arc when supported by the conveyor such that each lateral edge on a lower surface of the substrate is below a middle portion of the lower surface of the substrate, wherein the lower surface faces the transfer surface.

9. The apparatus as in claim 8 , wherein the transfer surface of the conveyor defines an arc that is substantially parallel to the arc of the substrate.

10. A process for vapor deposition of a sublimated source material to form thin film on a substrate, the process comprising:

sublimating a source material such that source vapors pass through a plurality of passages defined in a deposition plate;

moving a conveyor around a continuous loop, wherein the conveyor defines a pair of raised edges and a transfer surface such that the raised edges are raised with respect to the transfer surface; depositing the source vapors onto the transfer surface of the conveyor as the conveyor travels in a first direction above the distribution plate;

carrying a substrate on the raised edges of the conveyor in a second direction;

heating the conveyor while it travels in the second direction carrying the substrate such that the deposited source vapors on the transfer surface of the conveyor transfers to the substrate; and

cooling the conveyor while it travels in the first direction, wherein the conveyor is cooled to a plating temperature while traveling in the first direction, wherein the plating temperature is about 350° C. to about 500° C.

11. The process as in claim 10 , wherein the transfer surface of the conveyor has a transfer temperature when traveling in the second direction, wherein the transfer temperature is about 500° C. to about 650° C.

12. The process as in claim 10 , wherein the substrate bends to define a concave arc while being carried by the conveyor such that each lateral edge on the upper surface of the substrate is above a middle portion of the upper surface of the substrate.

13. The process as in claim 12 , wherein the transfer surface of the conveyor defines an arc that is substantially parallel to the concave arc of the substrate.

14. The process as in claim 12 , further comprising:

transporting the substrates through a heating apparatus and onto the conveyor to heat the substrates to a deposition temperature, wherein the substrates are initially substantially planar and, upon heating, the substrates are deformed to define the arc.

15. The process as in claim 10 , further comprising:

supplying additional source material to the receptacle via a feed system without interrupting the deposition process.

16. The process as in claim 10 , wherein the substrate is supported by the conveyor only on its raised edges.

Assignments (6)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Nov 15, 2021
From: JPMORGAN CHASE BANK, N.A.
To: FIRST SOLAR, INC.
Reel/Frame 058132/0566 →
PATENT SECURITY AGREEMENT Recorded Jul 12, 2017
From: FIRST SOLAR, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 043177/0581 →
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NUMBER FROM '13/301162' PREVIOUSLY RECORDED ON REEL 032045 FRAME 0657. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECT APPLICATION NUMBER SHOULD BE '13/601162'. Recorded Feb 10, 2014
From: FIRST SOLAR MALAYSIA SDN. BHD.
To: FIRST SOLAR, INC.
Reel/Frame 032239/0005 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 14, 2014
From: FIRST SOLAR MALAYSIA SDN. BHD.
To: FIRST SOLAR, INC.
Reel/Frame 032045/0657 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 5, 2013
From: PRIMESTAR SOLAR, INC.
To: FIRST SOLAR MALAYSIA SDN. BHD.
Reel/Frame 031581/0891 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 30, 2011
From: BLACK, RUSSELL WELDON; FELDMAN-PEABODY, SCOTT DANIEL; RATHWEG, CHRISTOPHER
To: PRIMESTAR SOLAR, INC.
Reel/Frame 026999/0283 →