IP Library Granted Patent US 8,999,066
Granted Patent B2
US 8,999,066 · App. 13/264,418 · Granted Apr 7, 2015

Bleached dextrin and methods of forming same

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Quick Facts
Patent No.
US 8,999,066
App. No.
13/264,418
Granted
Apr 7, 2015
Kind
B2
Abstract

A method of forming a bleached dextrin, comprising combining a dextrin-based composition selected from the group consisting of starch dextrin, cyclodextrins, inulin, hydrogenated indigestible dextrins, hydrogenated starch hydrolysates, highly branched maltodextrins, and combinations of any thereof with a caustic agent and an oxidant to form a mixture; heating the mixture for a period of time; and drying the mixture to form the bleached dextrin.

Claims (33)

1. A method of forming a bleached dextrin, comprising:

combining a dextrin-based composition selected from the group consisting of starch dextrin, cyclodextrins, inulin, hydrogenated indigestible dextrins, hydrogenated starch hydrolysates, highly branched maltodextrins, and combinations of any thereof with a caustic agent and an oxidant to form a mixture;

heating the mixture for a period of time; and

drying the mixture to form the bleached dextrin.

2. The method of claim 1 , wherein the dextrin-based composition is selected from the group consisting of a paste, a slurry and a combination thereof

3. The method of claim 2 , wherein the paste comprises water.

4. The method of claim 1 , wherein the caustic agent is added to the dextrin-based composition in an amount ranging from 0.01% to 10% on dextrin dry basis.

5. The method of claim 1 , wherein the caustic agent is combined at a pH ranging from 1 to 10.

6. The method of claim 1 , wherein the oxidant is added to the dextrin-based composition in an amount ranging from 0.1% to 10%.

7. The method of claim 1 , wherein the oxidant at a concentration of 0.1 to 70% is added to the dextrin-based composition in an amount ranging from 3 to 15%.

8. The method of claim 1 , wherein the mixture has a pH ranging from 6 to 10.

9. The method of claim 1 , wherein the mixture is heated to a temperature ranging from 10 to 80° C. for a period of time ranging from 10 to 360 minutes.

10. The method of claim 1 , wherein the drying occurs at a temperature ranging from 40 to 500° C. for a period of time ranging from 1 to 120 minutes.

11. The method of claim 1 , further comprising grinding the mixture.

12. The method of claim 1 , wherein the bleached dextrin has a whiteness level ranging from 90 to 100% based on CIE Lab model.

13. A method of forming a bleached dextrin, comprising:

forming a dextrin-based slurry;

combining the dextrin-based slurry with a caustic agent, thus producing a first mixture;

combining the first mixture with an oxidant, thus producing a second mixture;

drying the second mixture to form the bleached dextrin; and

grinding the bleached dextrin.

14. The method of claim 13 , further comprising adding an enzyme to the second mixture to remove excess of the oxidant before drying.

15. The method of claim 13 , wherein the dextrin of the dextrin-based slurry is digestion resistant and soluble.

16. A method of forming a bleached dextrin, the method comprising:

hydrating 0.3 to 3 parts powdered dextrin with 1 to 5 parts water by weight to form a dextrin-based composition;

combining the dextrin-based composition with sodium hydroxide to form a first mixture with a pH of 6 to 10;

combining hydrogen peroxide with the first mixture to form a second mixture;

incubating the second mixture between 20° C. and 50° C. for 0 to 2 hours; and

drying the second mixture to form the bleached dextrin.

17. The method of claim 16 , wherein the hydrogen peroxide is added to the first mixture for 10 to 20 minutes.

18. The method of claim 17 , wherein the hydrogen peroxide is added to the first mixture under a controlled pH with sodium hydroxide.

19. The method of claim 18 , wherein the pH is controlled for 30 to 45 minutes to complete the reaction.

20. The method of claim 16 , further comprising grinding the bleached dextrin.

Assignments (2)
RELEASE OF SECURITY INTEREST Recorded Jul 7, 2025
From: WELLS FARGO CAPITAL FINANCE CORPORATION CANADA
To: KSR IP HOLDINGS LLC
Reel/Frame 071918/0562 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 14, 2011
From: GERMAIN, NORMAND
To: ARCHER DANIELS MIDLAND COMPANY
Reel/Frame 027061/0309 →