IP Library Granted Patent US 8,580,778
Granted Patent B2
US 8,580,778 · App. 13/271,957 · Granted Nov 12, 2013

Substituted dihydropyrazolones and their use

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Quick Facts
Patent No.
US 8,580,778
App. No.
13/271,957
Granted
Nov 12, 2013
Kind
B2
Abstract

The present application relates to novel substituted dihydropyrazolone derivatives, processes for their preparation, their use for treatment and/or prophylaxis of diseases and their use for the preparation of medicaments for treatment and/or prophylaxis of diseases, in particular cardiovascular and haematological diseases and kidney diseases, and for promoting wound healing.

Claims (80)

1. A method for treating cardiac insufficiency, coronary heart disease, myocardial infarction, or stroke in a subject comprising administering a therapeutically effective amount of a compound of the formula

in which

X represents N or CH;

R 1 represents hydrogen or cyano; and

R 2 represents a saturated 4- to 7-membered heterocyclyl radical which is attached via a nitrogen atom,

where the heterocyclyl radical may be substituted by a substituent, where the substituent is selected from the group consisting of hydroxyl, hydroxycarbonyl, C 1 -C 3 -alkyl, C 1 -C 3 -alkylamino and C 3 -C 6 -cycloalkyl,

or

where the heterocyclyl radical may be substituted by 1 to 4 fluorine substituents, or a salt thereof.

2. A method for increasing the haematocrit in a subject comprising administering a therapeutically effective amount of a compound of the formula

in which

X represents N or CH;

R 1 represents hydrogen or cyano; and

R 2 represents a saturated 4- to 7-membered heterocyclyl radical which is attached via a nitrogen atom,

where the heterocyclyl radical may be substituted by a substituent, where the substituent is selected from the group consisting of hydroxyl, hydroxycarbonyl, C 1 -C 3 -alkyl, C 1 -C 3 -alkylamino and C 3 -C 6 -cycloalkyl,

or

where the heterocyclyl radical may be substituted by 1 to 4 fluorine substituents, or a salt thereof.

3. A method for treating acute renal failure or for promoting wound healing in a subject comprising administering a therapeutically effective amount of a compound of the formula

in which

X represents N or CH;

R 1 represents hydrogen or cyano; and

R 2 represents a saturated 4- to 7-membered heterocyclyl radical which is attached via a nitrogen atom,

where the heterocyclyl radical may be substituted by a substituent, where the substituent is selected from the group consisting of hydroxyl, hydroxycarbonyl, C 1 -C 3 -alkyl, C 1 -C 3 -alkylamino and C 3 -C 6 -cycloalkyl,

or

where the heterocyclyl radical may be substituted by 1 to 4 fluorine substituents, or a salt thereof.

4. A method for treating retinopathy in premature babies (retinopathia prematurorum) in a subject comprising administering a therapeutically effective amount of a compound of the formula

in which

X represents N or CH;

R 1 represents hydrogen or cyano; and

R 2 represents a saturated 4- to 7-membered heterocyclyl radical which is attached via a nitrogen atom,

where the heterocyclyl radical may be substituted by a substituent, where the substituent is selected from the group consisting of hydroxyl, hydroxycarbonyl, C 1 -C 3 -alkyl, C 1 -C 3 -alkylamino and C 3 -C 6 -cycloalkyl,

or

where the heterocyclyl radical may be substituted by 1 to 4 fluorine substituents, or a salt thereof.

5. The method of claim 1 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

or a salt thereof.

6. The method of claim 1 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl }-1H-imidazole-4-carbonitrile, as represented by the formula

7. The method of claim 1 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

or a salt thereof.

8. The method of claim 1 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

9. The method of claim 1 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

or a salt thereof.

10. The method of claim 1 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

11. The method of claim 1 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pryrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

or a salt thereof.

12. The method of claim 1 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

13. The method of claim 2 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

or a salt thereof.

14. The method of claim 2 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

15. The method of claim 2 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

or a salt thereof.

16. The method of claim 2 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

17. The method of claim 2 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

or a salt thereof.

18. The method of claim 2 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

19. The method of claim 2 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

or a salt thereof.

20. The method of claim 3 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

21. The method of claim 3 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

or a salt thereof.

22. The method of claim 3 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

23. The method of claim 3 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine -3-carboxylic acid, as represented by the formula

or a salt thereof.

24. The method of claim 3 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

25. The method of claim 3 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

or a salt thereof.

26. The method of claim 3 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

27. The method of claim 3 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

or a salt thereof.

28. The method of claim 3 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

29. The method of claim 4 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

or a salt thereof.

30. The method of claim 4 , wherein the compound of formula (I) is 1-{2-[6-(4-Cyclobutylpiperazin-1-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-imidazole-4-carbonitrile, as represented by the formula

31. The method of claim 4 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

or a salt thereof.

32. The method of claim 4 , wherein the compound of formula (I) is 1-{6-[5-Oxo-4-(1H-1,2,3-triazol-1-yl)-2,5-dihydro-1H-pyrazol-1-yl]pyrimidin-4-yl}azetidine-3-carboxylic acid, as represented by the formula

33. The method of claim 4 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

or a salt thereof.

34. The method of claim 4 , wherein the compound of formula (I) is 2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-4-(1H-1,2,3-triazol-1-yl)-1,2-dihydro-3H-pyrazol-3-one, as represented by the formula

35. The method of claim 4 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

or a salt thereof.

36. The method of claim 4 , wherein the compound of formula (I) is 1-{2-[6-(1,2-Oxazinan-2-yl)pyrimidin-4-yl]-3-oxo-2,3-dihydro-1H-pyrazol-4-yl}-1H-1,2,3-triazole-4-carbonitrile, as represented by the formula:

Assignments (2)
CHANGE OF ADDRESS Recorded Jun 12, 2023
From: BAYER INTELLECTUAL PROPERTY GMBH
To: BAYER INTELLECTUAL PROPERTY GMBH
Reel/Frame 064021/0344 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 1, 2013
From: BAYER PHARMA AKTIENGESELLSCHAFT
To: BAYER INTELLECTUAL PROPERTY GMBH
Reel/Frame 029905/0112 →