IP Library Granted Patent US 8,784,679
Granted Patent B2
US 8,784,679 · App. 13/280,987 · Granted Jul 22, 2014

Aqueous powder water treatment compositions and methods for making same

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Quick Facts
Patent No.
US 8,784,679
App. No.
13/280,987
Granted
Jul 22, 2014
Kind
B2
Abstract

Embodiments of a method of producing an aqueous powder composition for treating water comprise mixing sodium metabisulfite powder with amines, wherein the amines comprises liquid cyclohexylamine, and adding water to the mixture of sodium metabisulfite powder and liquid cyclohexylamine to catalyze the production of the aqueous powder composition.

Claims (9)

1. A method of producing a dry powder composition for treating water comprising:

mixing sodium metabisulfite powder with amines, wherein the amines comprise liquid cyclohexylamine; and

adding water to the mixture of sodium metabisulfite powder and liquid cyclohexylamine to catalyze production of the dry powder composition,

wherein the dry powder composition consists of about 35 to about 55% by weight of amines, wherein the amines comprise liquid cyclohexylamine and optionally one or more additional amines, about 35 to about 55% by weight of bisulfites selected from the group consisting of sodium bisulfite, sodium metabisulfite, and mixtures thereof, and about 5 to about 10% by weight of water.

2. The method of claim 1 wherein the dry powder composition is free of phosphates.

3. The method of claim 1 further comprising adding additional amines to the mixture of sodium metabisulfite powder and liquid cyclohexylamine prior to the addition of water.

4. The method of claim 3 wherein the additional amines are selected from the group consisting of diethylaminoethanol, morpholine, or combinations thereof.

5. The method of claim 1 further comprising cooling the dry powder composition to room temperature.

6. The method of claim 1 wherein the sodium metabisulfite and amines are mixed at a ratio by weight of about 1.5:1 to about 1:1.5.

Assignments (15)
PATENT SECURITY AGREEMENT Recorded Jun 18, 2024
From: DUBOIS CHEMICALS, INC.
To: ANTARES CAPITAL LP, AS COLLATERAL AGENT
Reel/Frame 067774/0852 →
SECURITY INTEREST Recorded Jul 22, 2022
From: DUBOIS CHEMICALS, INC.
To: ANTARES CAPITAL LP, AS COLLATERAL AGENT
Reel/Frame 060588/0838 →
RELEASE OF SECURITY INTEREST Recorded Apr 4, 2021
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: DUBOIS CHEMICALS, INC.
Reel/Frame 055814/0512 →
SECURITY INTEREST Recorded Jun 30, 2020
From: DUBOIS CHEMICALS, INC., AS GRANTOR
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 053085/0382 →
CORRECTIVE ASSIGNMENT TO CORRECT THE TITLE TO READ RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 042038/0101 PREVIOUSLY RECORDED ON REEL 050598 FRAME 0028. ASSIGNOR(S) HEREBY CONFIRMS THE RELEASE OF SECURITY INTEREST. Recorded Oct 10, 2019
From: ANTARES CAPITAL LP
To: DUBOIS CHEMICALS, INC.
Reel/Frame 052091/0032 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 04238/0101 Recorded Oct 1, 2019
From: ANTARES CAPITAL LP
To: DUBOIS CHEMICALS, INC.
Reel/Frame 050598/0028 →
SECURITY INTEREST Recorded Oct 1, 2019
From: DUBOIS CHEMICALS, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 050573/0202 →
SECURITY INTEREST Recorded Oct 1, 2019
From: DUBOIS CHEMICALS, INC.
To: ANTARES CAPITAL LP, AS COLLATERAL AGENT
Reel/Frame 050573/0867 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 042038/0153 Recorded Oct 1, 2019
From: ANTARES CAPITAL LP
To: DUBOIS CHEMICALS, INC.
Reel/Frame 050597/0851 →
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 17, 2017
From: DUBOIS CHEMICALS, INC.
To: ANTARES CAPITAL LP
Reel/Frame 042038/0101 →
SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 17, 2017
From: DUBOIS CHEMICALS, INC.
To: ANTARES CAPITAL LP
Reel/Frame 042038/0153 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL RECORDED AT REEL 029549/FRAME 0142 Recorded Mar 15, 2017
From: ANTARES CAPITAL LP, SUCCESSOR AGENT TO GENERAL ELECTRIC CAPITAL CORPORATION
To: DUBOIS CHEMICALS, INC.
Reel/Frame 042020/0826 →
ASSIGNMENT OF INTELLECTUAL PROPERTY SECURITY AGREEMENTS Recorded Oct 9, 2015
From: GENERAL ELECTRIC CAPITAL CORPORATION, AS RETIRING AGENT
To: ANTARES CAPITAL LP, AS SUCCESSOR AGENT
Reel/Frame 036826/0621 →
SECURITY AGREEMENT Recorded Dec 28, 2012
From: DUBOIS CHEMICALS, INC.
To: GENERAL ELECTRIC CAPITAL CORPORATION, AS AGENT
Reel/Frame 029549/0142 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2011
From: MOORE, RICHARD; STEIMEL, LYLE H.
To: DUBOIS CHEMICALS, INC.
Reel/Frame 027117/0642 →