IP Library Granted Patent US 8,753,413
Granted Patent B1
US 8,753,413 · App. 13/292,900 · Granted Jun 17, 2014

Polycrystalline diamond compacts and applications therefor

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Quick Facts
Patent No.
US 8,753,413
App. No.
13/292,900
Granted
Jun 17, 2014
Kind
B1
Abstract

Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a polycrystalline diamond (“PCD”) table including a catalyst material therein that has been implanted with ions (e.g., carbon ions) and/or infiltrated from a host material implanted with carbon ions. In an embodiment, a PDC comprises a substrate and a PCD table bonded to the substrate. The PCD table includes a plurality of bonded diamond grains defining a plurality of interstitial regions. The PCD table includes an upper surface from which a region inwardly extends. At least a portion of the interstitial regions of the region includes a catalyst material disposed therein. At least a portion of the catalyst material may be at least saturated with carbon.

Claims (36)

1. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of bonded diamond grains defining a plurality of interstitial regions, the polycrystalline diamond table including an upper surface from which a region inwardly extends and at least one lateral surface extending about the upper surface, the region further extends laterally from the at least one lateral surface to a distance about equal to a depth to which the region extends from the upper surface, at least a portion of the interstitial regions of the region including a catalyst material disposed therein, at least a portion of the catalyst material being at least saturated with carbon.

2. The polycrystalline diamond compact of claim 1 wherein the at least a portion of the catalyst material is supersaturated with the carbon.

3. The polycrystalline diamond compact of claim 1 wherein the at least a portion of the catalyst material comprises carbon fibrules.

4. The polycrystalline diamond compact of claim 1 wherein the region extends from the upper surface of the polycrystalline diamond table to a depth of about 1 nm to about 1500 nm.

5. The polycrystalline diamond compact of claim 1 wherein the region extends from the upper surface of the polycrystalline diamond table to a depth of about 50 nm to about 800 nm.

6. The polycrystalline diamond compact of claim 1 wherein the region is remote from the substrate and another region is adjacent to the substrate, and the region is more thermally stable than the another region.

7. The polycrystalline diamond compact of claim 1 wherein the catalyst material comprises at least one member selected from the group consisting of iron, nickel, cobalt, and alloys thereof.

8. A rotary drill bit, comprising a plurality of cutting elements mounted to a bit body configured to engage a subterranean formation, at least one of the plurality of cutting elements comprising the polycrystalline diamond compact of claim 1 .

9. A polycrystalline diamond compact, comprising:

a polycrystalline diamond body including a plurality of bonded diamond grains defining a plurality of interstitial regions, the polycrystalline diamond body including an upper surface from which a thermally-stable region inwardly extends and at least one lateral surface extending about the upper surface, the thermally-stable region further extends laterally from the at least one lateral surface to a distance about equal to a depth to which the thermally-stable region extends from the upper surface, at least a portion of the interstitial regions of the thermally-stable region including a sintering aid disposed therein, at least a portion of the sintering aid being supersaturated with carbon and including carbon fibrules.

10. The polycrystalline diamond compact of claim 9 wherein the thermally-stable region extends from the upper surface of the polycrystalline diamond body to a depth of about 1 nm to about 1500 nm.

11. The polycrystalline diamond compact of claim 9 wherein the thermally-stable region extends from the upper surface of the polycrystalline diamond body to a depth of about 50 nm to about 800 nm.

12. The polycrystalline diamond compact of claim 9 , further comprising a substrate bonded to the polycrystalline diamond body wherein the thermally-stable region is remote from the substrate and another region is adjacent to the substrate, and the thermally-stable region is more thermally stable than the another region.

13. The polycrystalline diamond compact of claim 9 wherein the sintering aid comprises at least one member selected from the group consisting of iron, nickel, cobalt, aluminum, a refractory metal, and alloys thereof.

14. The polycrystalline diamond compact of claim 9 wherein the sintering aid comprises a catalyst material.

15. The polycrystalline diamond compact of claim 9 , further comprising a cemented carbide substrate bonded to the polycrystalline diamond body.

16. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond table bonded to the substrate, the polycrystalline diamond table including a plurality of bonded diamond grains defining a plurality of interstitial regions, the polycrystalline diamond table including an upper surface from which a first region inwardly extends and a second region adjacent to the substrate, the first region being remote from the substrate and more thermally stable than the second region, at least a portion of the interstitial regions of the first region including a catalyst material disposed therein, at least a portion of the catalyst material being at least saturated with carbon.

17. The polycrystalline diamond compact of claim 16 wherein the at least a portion of the catalyst material is supersaturated with the carbon.

18. The polycrystalline diamond compact of claim 16 wherein the at least a portion of the catalyst material comprises carbon fibrules.

19. The polycrystalline diamond compact of claim 16 wherein the region extends from the upper surface of the polycrystalline diamond table to a depth of about 1 nm to about 1500 nm.

20. The polycrystalline diamond compact of claim 16 wherein the region extends from the upper surface of the polycrystalline diamond table to a depth of about 50 nm to about 800 nm.

21. The polycrystalline diamond compact of claim 16 wherein the polycrystalline diamond table comprises at least one lateral surface extending about the upper surface, and wherein the first region further extends laterally from the at least one lateral surface to a distance about equal to a depth to which the first region extends from the upper surface.

22. The polycrystalline diamond compact of claim 16 wherein the catalyst material comprises at least one member selected from the group consisting of iron, nickel, cobalt, and alloys thereof.

23. A polycrystalline diamond compact, comprising:

a substrate; and

a polycrystalline diamond body bonded to the substrate, the polycrystalline diamond body including a plurality of bonded diamond grains defining a plurality of interstitial regions, the polycrystalline diamond body including an upper surface from which a thermally-stable region inwardly extends and another region adjacent to the substrate, the thermally-stable region being remote from the substrate and more thermally stable than the another region, at least a portion of the interstitial regions of the thermally-stable region including a sintering aid disposed therein, at least a portion of the sintering aid being supersaturated with carbon and including carbon fibrules.

24. The polycrystalline diamond compact of claim 23 wherein the thermally-stable region extends from the upper surface of the polycrystalline diamond body to a depth of about 1 nm to about 1500 nm.

25. The polycrystalline diamond compact of claim 23 wherein the thermally-stable region extends from the upper surface of the polycrystalline diamond body to a depth of about 50 nm to about 800 nm.

26. The polycrystalline diamond compact of claim 23 wherein the polycrystalline diamond body comprises at least one lateral surface extending about the upper surface, and wherein the thermally-stable region further extends laterally from the at least one lateral surface to a distance about equal to a depth to which the thermally-stable region extends from the upper surface.

27. The polycrystalline diamond compact of claim 23 wherein the sintering aid comprises at least one member selected from the group consisting of iron, nickel, cobalt, aluminum, a refractory metal, and alloys thereof.

28. The polycrystalline diamond compact of claim 23 wherein the sintering aid comprises a catalyst material.

29. The polycrystalline diamond compact of claim 23 , further comprising a cemented carbide substrate bonded to the polycrystalline diamond body.

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →