IP Library Granted Patent US 9,150,780
Granted Patent B2
US 9,150,780 · App. 13/326,561 · Granted Oct 6, 2015

Environmentally friendly stimulation fluids, processes to create wormholes in carbonate reservoirs, and processes to remove wellbore damage in carbonate reservoirs

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,150,780
App. No.
13/326,561
Granted
Oct 6, 2015
Kind
B2
Abstract

The present invention includes processes to create wormholes in carbonate reservoirs by contacting a formation with a solution comprising glutamic acid N,N-diacetic acid (GLDA) and/or a salt thereof, methylglycine-N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof. The present invention also includes processes to remove wellbore damage in a carbonate reservoir by contacting a damaged zone of the carbonate reservoir with a solution comprising GLDA and/or a salt thereof, methylglycine-N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof. The present invention further includes solutions comprising a salt and further comprising GLDA and/or a salt thereof, methylglycine-N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof.

Claims (20)

1. Process to create wormholes in a carbonate reservoir by contacting a formation with a solution comprising a wormhole-forming agent, said wormhole forming agent consisting of a chelating agent selected from the group consisting of glutamic acid N,N-diacetic acid (GLDA) and/or a salt thereof, methylglycine-N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof.

2. Process of claim 1 , wherein the solution is an aqueous solution of about 10 to about 30 wt % of GLDA and/or a salt thereof, MGDA and/or a salt thereof, or a combination thereof.

3. Process of claim 1 , wherein the solution further comprises a salt other than a salt of either GLDA or MGDA.

4. Process of claim 3 , wherein the salt other than a salt of either GLDA or MGDA comprises a chloride salt, a formate salt, a bromide salt, or a combination thereof.

5. Process of claim 1 , wherein the pH of the solution is about 3 to about 5.

6. Process of claim 1 , wherein the injection rate of the solution is about 0.25 to about 5 barrels/min.

7. Process to remove wellbore damage in a carbonate reservoir by contacting a damaged zone of the carbonate reservoir with a solution comprising a wormhole- forming agent, said wormhole forming agent consisting of a chelating agent selected from the group consisting of glutamic acid N,N-diacetic acid (GLDA) and/or a salt thereof, methylglycine-N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof.

8. Process of claim 7 , wherein the solution is an aqueous solution of about 10 to about 30 wt % of GLDA and/or a salt thereof, MGDA and/or a salt thereof, or a combination thereof.

9. Process of claim 7 , wherein the solution further comprises a salt other than a salt of either GLDA or MGDA.

10. Process of claim 9 , wherein the salt other than a salt of either GLDA or MGDA comprises a chloride salt, a formate salt, a bromide salt, or a combination thereof.

11. Process of claim 7 , wherein the pH of the solution is about 3 to about 5.

12. Process of claim 7 , wherein the injection rate of the solution is about 0.25 to about 5 barrels/min.

13. A solution consisting of a salt other than a salt of either GLDA or MGDA and glutamic acid N,N-diacetic acid (GLDA) and/or a salt thereof, methylglycine- N,N-diacetic acid (MGDA) and/or a salt thereof, or a combination thereof.

14. The solution of claim 13 , wherein the salt other than a salt of either GLDA or MGDA comprises a chloride salt, a formate salt, a bromide salt, or a combination thereof.

15. The solution of claim 13 , wherein the solution is an aqueous solution of a salt other than a salt of either GLDA or MGDA and about 10 to about 30 wt % of GLDA and/or a salt thereof, MGDA and/or a salt thereof, or a combination thereof.

16. The solution of claim 13 , wherein the pH of the solution is about 3 to about 5.

17. The process of claim 1 wherein said wormhole forming agent consists of said chelating agent.

18. The process of claim 7 wherein said wormhole forming agent consists of said chelating agent.

19. The process of claim 1 wherein said chelating agent is selected from the group consisting of GLDA, salts of GLDA, and combinations thereof.

20. The process of claim 7 wherein said chelating agent is selected from the group consisting of GLDA, salts of GLDA, and combinations thereof.

Assignments (7)
CHANGE OF NAME Recorded Sep 18, 2019
From: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: NOURYON CHEMICALS INTERNATIONAL B.V.
Reel/Frame 050426/0671 →
SECURITY INTEREST Recorded Oct 1, 2018
From: STARFRUIT US MERGER SUB 1 LLC; STARFRUIT US MERGER SUB 2 LLC; AKZO NOBEL SURFACE CHEMISTRY LLC; AKZO NOBEL CHEMICALS B.V.; AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: WILMINGTON TRUST (LONDON) LIMITED, AS COLLATERAL AGENT
Reel/Frame 047231/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 14, 2018
From: NASR-EL-DIN MAHMOUD, MOHAMED AHMED
To: THE TEXAS A&M UNIVERSITY SYSTEM
Reel/Frame 045202/0127 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 14, 2018
From: THE TEXAS A&M UNIVERSITY SYSTEM
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 045207/0310 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 14, 2018
From: NASR-EL-DIN, HISHAM
To: THE TEXAS A&M UNIVERSITY SYSTEM
Reel/Frame 045202/0051 →
CHANGE OF ADDRESS Recorded May 15, 2017
From: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 042745/0406 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2012
From: DE WOLF, CORNELIA ADRIANA; NASR-EL-DIN, HISHAM; LEPAGE, JAMES N.; NASR-EL-DIN MAHMOUD, MOHAMED AHMED; BEMELAAR, JOHANNA HENDRIKA
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 028099/0092 →