IP Library Granted Patent US 8,551,310
Granted Patent B2
US 8,551,310 · App. 13/328,115 · Granted Oct 8, 2013

Method for making a nano-composite gas sensor

Inventors: Li-Chun Wang (Taoyuan County, TW); Tseng-Hsiung Su (Tainan, TW); Shang-Ren Yang (Yilan County, TW); Cheng-Long Ho (New Taipei, TW); Han-Wen Kuo (New Taipei, TW); Kea-Tiong Tang (Hsinchu, TW)
Assignee: Chung-Shan Institute of Science and Technology, Armaments Bureau, Dept. of National Defense
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Quick Facts
Patent No.
US 8,551,310
App. No.
13/328,115
Granted
Oct 8, 2013
Kind
B2
Abstract

There is disclosed a method for making a nano-composite gas sensor. At first, there is provided a substrate. Then, electrodes are provided on the substrate in an array. Finally, a gas-sensing membrane is provided on the electrodes. The gas-sensing membrane includes a nano-conductive film and a peptide film.

Claims (29)

1. A method for making a nano-composite gas sensor including the steps of:

providing a substrate;

providing electrodes on the substrate in an array; and

providing a gas-sensing membrane on the electrodes, wherein the gas-sensing membrane includes a nano-conductive film and a peptide film, wherein the peptide film is made of a material selected from the group consisting of Beta-Amyloid (1-40), Human galectin-1 and Human albumin.

2. The method for making a nano-composite gas sensor according to claim 1 , wherein the substrate includes an insulating material coated on a material selected from the group consisting of metal, semiconductor and ceramic materials.

3. The method for making a nano-composite gas sensor according to claim 2 , wherein the semiconductor is provided in the form of a silicon wafer.

4. The method for making a nano-composite gas sensor according to claim 1 , wherein the electrodes are made of a material selected from the group consisting of gold, platinum, silver and aluminum.

5. The method for making a nano-composite gas sensor according to claim 1 , wherein the electrodes are made of a configuration selected from the group consisting of fork-shaped, elongated and helical.

6. The method for making a nano-composite gas sensor according to claim 1 , wherein the peptide film is provided on the nano-conductive film.

7. The method for making a nano-composite gas sensor according to claim 1 , wherein the nano-conductive film is made of a material selected from the group consisting of carbon nanotubes, carbon black, carbon balls and graphene.

8. The method for making a nano-composite gas sensor according to claim 7 , wherein the carbon nanotubes are evenly dispersed in a solvent selected from the group consisting of MEK, IPA, H 2 O and PVA to provide a carbon nanotube-based mixture of 0.1 wt % to 2.0 wt % of carbon nanotubes.

9. The method for making a nano-composite gas sensor according to claim 7 , wherein the carbon nanotubes are evenly dispersed in a solvent selected from the group consisting of MEK, IPA, H 2 O and PVA to provide a carbon nanotube-based mixture that includes 0.5 wt % to 1.0 wt % of carbon nanotubes.

10. The method for making a nano-composite gas sensor according to claim 1 , wherein the peptide film is made by evenly dispersing peptide in a solvent selected from the group consisting of Toluene, THF and H 2 O to provide a peptide-based mixture that includes 5 wt % to 50 wt % of peptide.

11. The method for making a nano-composite gas sensor according to claim 1 , wherein the peptide film is made by evenly dispersing peptide in a solvent selected from the group consisting of Toluene, THF and H 2 O to provide a peptide-based mixture that includes 10 wt % to 45 wt % of peptide.

12. The method for making a nano-composite gas sensor according to claim 1 , wherein the step of providing the gas-sensing membrane includes the steps of:

providing the nano-conductive film by evenly dispersing carbon nanotubes in a solvent to provide a carbon nanotube-based mixture; providing the peptide film by evenly dispersing peptide in the solvent to provide a peptide-based mixture;

evenly providing 1 to 3 μL of the carbon nanotube-based mixture on the electrodes;

drying the carbon nanotube-based mixture in a vacuum oven at 50 to 70 degrees Celsius for 1 to 3 hours to form the nano-conductive film with a resistance of 1 to 10 KΩ;

evenly providing 1 to 3 μl of the peptide-based mixture on the nano-conductive film; and

drying the peptide-based mixture in a vacuum oven at 50 to 60 degrees Celsius for 1 to 4 hours to form the peptide film.

13. The method for making a nano-composite gas sensor according to claim 12 , wherein the solvent is selected from the group consisting of MEK, IPA, H 2 O and PVA.

14. The method for making a nano-composite gas sensor according to claim 1 , wherein the step of providing the gas-sensing membrane includes the steps of:

providing the nano-conductive film by evenly dispersing carbon nanotubes in a solvent to provide a carbon nanotube-based mixture;

providing the peptide film by evenly dispersing peptide in the solvent to provide a peptide-based mixture;

evenly providing 1 to 10 μL of the carbon nanotube-based mixture on the electrodes;

drying the carbon nanotube-based mixture in a vacuum oven at 40 to 80 degrees Celsius for 1 to 5 hours to form the nano-conductive film with a resistance of 1 to 50 KΩ;

evenly providing 1 to 10 μl of the peptide-based mixture on the nano-conductive film; and

drying the peptide-based mixture in a vacuum oven at 40 to 60 degrees Celsius for 1 to 5 hours to form the peptide film.

15. The method for making a nano-composite gas sensor according to claim 14 , wherein the solvent is selected from the group consisting of MEK, IPA, H 2 O and PVA.

Assignments (2)
CHANGE OF NAME Recorded Apr 17, 2015
From: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS, BUREAU, MINISTRY OF NATIONAL DEFENSE
To: NATIONAL CHUNG SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY
Reel/Frame 035453/0379 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 16, 2011
From: WANG, LI-CHUN; SU, TSENG-HSIUNG; YANG, SHANG-REN; HO, CHENG-LONG; KUO, HAN-WEN; TANG, KEA-TIONG
To: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS, BUREAU, MINISTRY OF NATIONAL DEFENSE
Reel/Frame 027396/0494 →
Continuity (1)
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