IP Library Granted Patent US 8,945,243
Granted Patent B2
US 8,945,243 · App. 13/332,322 · Granted Feb 3, 2015

Systems capable of adding cellulosic biomass to a digestion unit operating at high pressures and associated methods for cellulosic biomass processing

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Quick Facts
Patent No.
US 8,945,243
App. No.
13/332,322
Granted
Feb 3, 2015
Kind
B2
Abstract

When processing cellulosic biomass, it may be desirable for a digestion unit to operate without being fully depressurized for process efficiency purposes. Methods for processing cellulosic biomass may comprise providing a biomass conversion system comprising a pressurization zone and a digestion unit that are operatively connected to one another; providing cellulosic biomass at a first pressure; introducing at least a portion of the cellulosic biomass into the pressurization zone and pressurizing the pressurization zone to a second pressure higher than the first pressure; after pressurizing the pressurization zone, transferring at least a portion of the cellulosic biomass from the pressurization zone to the digestion unit, which is at a third pressure that is less than or equal to the second pressure but higher than the first pressure; and digesting at least a portion of the cellulosic biomass in the digestion unit to produce a hydrolysate comprising soluble carbohydrates.

Claims (38)

1. A method comprising:

providing a biomass conversion system comprising a pressurization zone and a digestion unit that are operatively connected to one another;

providing a cellulosic biomass at a first pressure;

introducing at least a portion of the cellulosic biomass into the pressurization zone and then pressurizing the pressurization zone to a second pressure that is higher than the first pressure;

after pressurizing the pressurization zone, transferring at least a portion of the cellulosic biomass from the pressurization zone to the digestion unit, which is at a third pressure that is less than or equal to the second pressure but higher than the first pressure; and

digesting at least a portion of the cellulosic biomass in the digestion unit to produce a hydrolysate comprising soluble carbohydrates within a liquor phase.

2. The method of claim 1 , wherein providing a cellulosic biomass and introducing at least a portion of the cellulosic biomass take place at the same time.

3. The method of claim 1 , wherein introducing at least a portion of the cellulosic biomass into the pressurization zone comprises a technique or apparatus selected from the group consisting of a screw feeder, a conveyer, a bin dispenser, manual addition, and any combination thereof.

4. The method of claim 1 , wherein, after transferring at least a portion of the cellulosic biomass, the digestion unit is at a pressure of at least about 30 bar.

5. The method of claim 1 , further comprising:

converting the hydrolysate into a biofuel.

6. The method of claim 1 , wherein at least about 60% of the cellulosic biomass, on a dry basis, is digested to produce hydrolysate.

7. The method of claim 1 , wherein at least about 90% of the cellulosic biomass, on a dry basis, is digested to produce hydrolysate.

8. The method of claim 1 , further comprising:

before transferring at least a portion of the cellulosic biomass, reducing the pressure in the digestion unit to a fourth pressure that is at least about 75% of the third pressure.

9. The method of claim 1 , wherein the third pressure ranges between about 30 bar and about 430 bar.

10. The method of claim 1 , wherein the third pressure ranges between about 50 bar and about 330 bar.

11. The method of claim 1 , wherein the third pressure ranges between about 70 bar and about 130 bar.

12. The method of claim 1 , wherein pressurizing takes place, at least in part, by introducing at least a portion of the liquor phase into the pressurization zone.

13. The method of claim 12 , wherein the liquor phase comprises an organic solvent.

14. The method of claim 12 , wherein pressurizing takes place, at least in part, by introducing a gas into the pressurization zone.

15. The method of claim 1 , wherein the cellulosic biomass comprises wood.

16. A method comprising:

providing a biomass conversion system comprising a pressurization zone and a digestion unit that are operatively connected to one another;

providing a cellulosic biomass;

introducing at least a portion of the cellulosic biomass into the pressurization zone and then pressurizing the pressurization zone, at least in part, with a liquor phase comprising an organic solvent;

after pressurizing the pressurization zone, transferring at least a portion of the cellulosic biomass from the pressurization zone to the digestion unit, wherein the digestion unit is at a pressure that is less than or equal to the pressure of the pressurization zone; and

digesting at least about 90% of the cellulosic biomass, on a dry basis, to produce a hydrolysate comprising soluble carbohydrates within a liquor phase.

17. The method of claim 16 , wherein introducing at least a portion of the cellulosic biomass into the pressurization zone comprises a technique or apparatus selected from the group consisting of a screw feeder, a conveyer, a bin dispenser, manual addition, and any combination thereof.

18. The method of claim 16 , wherein pressurizing takes place, at least in part, by introducing a gas into the pressurization zone.

19. The method of claim 16 , further comprising:

converting the hydrolysate into a biofuel.

20. The method of claim 16 , wherein, after transferring at least a portion of the cellulosic biomass, the digestion unit is at a pressure of at least about 30 bar.

21. The method of claim 16 , wherein the pressure of the digestion unit ranges between about 30 bar and about 130 bar.

22. The method of claim 16 , wherein the pressure of the digestion unit ranges between about 50 bar and about 330 bar.

23. The method of claim 16 , wherein the pressure of the digestion unit ranges between about 70 bar and about 130 bar.

24. The method of claim 16 , further comprising:

recirculating at least a portion of a reaction product produced from the hydrolysate back into the digestion unit.

Assignments (2)
CHANGE OF NAME Recorded Mar 7, 2022
From: SHELL OIL COMPANY
To: SHELL USA, INC.
Reel/Frame 059694/0819 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2012
From: POWELL, JOSEPH BROUN; CHEDDA, JUBEN NEMCHAND; FLOWERS, THOMAS LAMAR
To: SHELL OIL COMPANY
Reel/Frame 027815/0256 →