Methods and devices for circulating air
View Patent ↗A gas chromatography system comprising a sample introduction device, an oven coupled to the sample introduction device and a detector coupled to the oven is disclosed. In certain examples, the oven may be configured to receive a chromatography column in a space in the oven. In some examples, the oven may be constructed and arranged to provide a substantially constant temperature to the space during an analysis stage of the gas chromatography system.
1. A gas chromatography system comprising:
an oven having an air intake aperture and an air exhaust aperture, where at least one of the air intake aperture and the air exhaust aperture is adjusted during a stage of operation of the gas chromatography system;
a fan positioned in the oven, and
a controller configured to relate a fan speed and a degree of opening of at least one of the air intake aperture and the air exhaust aperture.
2. The gas chromatography system of claim 1 , wherein the fan can be modulated to rotate at two or more speeds during operation of the oven.
3. The gas chromatography system of claim 2 , wherein the fan speed can be modulated continuously.
4. The gas chromatography system of claim 2 , wherein the fan speed can be modulated intermittently.
5. The gas chromatography system of claim 1 , wherein the fan is fluidically coupled to at least one of the air intake aperture and the air exhaust aperture.
6. The gas chromatography system of claim 1 , further comprising a programmable motor coupled to the fan and configured to modulate a fan speed of the fan.
7. The gas chromatography system of claim 1 , further comprising a vent fluidically coupled to the air exhaust aperture and configured to exhaust hot air away from the space in the oven.
8. The gas chromatography system of claim 1 , wherein the fan is modulated at a second speed to reduce cool down time by at least 50-75% as compared to modulating the fan at a first speed.
9. The gas chromatography system of claim 1 , wherein the fan is modulated to rotate at a first speed of about 1400 rpm during an analysis stage.
10. The gas chromatography system of claim 1 , wherein the fan is modulated to rotate at a second speed of about 2800 rpm during a cool down stage.
11. The gas chromatography system of claim 1 , further comprising a detector coupled to the oven.
12. The gas chromatography system of claim 11 , wherein the detector comprises at least one of: an ionization detector, a hot wire detector, a thermal conductivity detector, a nitrogen phosphorous detector, a photometric detector, and a mass spectrometer.
13. The gas chromatography system of claim 1 , wherein the controller is configured to heat the oven space at a known rate during the analysis stage.
14. The gas chromatography system of claim 1 , wherein the controller is configured to cool the oven space at a known rate during a cooling stage.
15. The gas chromatography system of claim 1 , wherein the controller is configured to linearly relate the fan speed and the degree of opening of at least one of the air intake aperture and the air exhaust aperture.
16. The gas chromatography system of claim 1 , wherein the controller is configured to close at least one of the air intake aperture and the air exhaust aperture during an analysis stage, and further configured to open at least one of the air intake aperture and the air exhaust aperture during a cooling stage.
17. The gas chromatography system of claim 1 , wherein the opening and closing of the air intake aperture and the air exhaust aperture can be controlled independently.
18. The gas chromatography system of claim 1 , wherein the oven is configured to provide a recirculation path to circulate air to provide a substantially constant temperature to the oven space during an analysis stage.
19. The gas chromatography system of claim 18 , wherein the recirculation path includes a shroud with at least one through-hole.
20. The gas chromatography system of claim 18 , wherein the recirculation path includes a shroud comprising at least one air scoop.
21. The gas chromatography system of claim 18 , wherein the recirculation path provides a substantially constant injection-to-injection time.
22. The gas chromatography system of claim 1 , further comprising a second fan fluidically coupled to at least one of the air intake aperture and the air exhaust aperture, whose speed can be independently modulated.