IP Library Granted Patent US 8,722,685
Granted Patent B2
US 8,722,685 · App. 13/343,231 · Granted May 13, 2014

Pyrazine derivatives and uses thereof in renal monitoring

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Quick Facts
Patent No.
US 8,722,685
App. No.
13/343,231
Granted
May 13, 2014
Kind
B2
Abstract

The present invention relates to pyrazine derivatives such as those represented by Formulas I and II below. X 1 to X 4 of the compounds of Formulas I and II may be characterized as electron withdrawing groups. In contrast, Y 1 to Y 4 of the compounds of Formulas I and II may be characterized as electron donating groups. Pyrazine derivatives of the present invention may be utilized in assessing renal function. In particular, an effective amount of a pyrazine derivative of the invention may be administered into a body of a patient. The pyrazine derivative that is in the body may be exposed to visible and/or infrared light to cause spectral energy to emanate from the pyrazine derivative. This emanating spectral energy may be detected and utilized to determine renal function of the patient.

Claims (30)

1. A compound of Formula I, wherein:

each of X 1 and X 2 is independently —CN, —CO 2 R 1 , —CONR 2 R 3 , or —CONH(PS);

each of Y 1 and Y 2 is independently —NR 4 R 5 or

Z 1 is a single bond, —CR 18 R 19 —, —O—, —NR 20 —, —NCOR 21 —, —S—, —SO—, or —SO 2 —;

each of R 1 to R 5 and R 18 to R 21 is independently —H, —CH 2 (CHOH) a R 44 , —CH 2 (CHOH) a CO 2 H, —(CHCO 2 H) a CO 2 H, —(CH 2 CH 2 O) c R 49 , —(CH 2 ) a SO 3 H, —(CH 2 ) a SO 3 − , —(CH 2 ) a NHSO 3 H, —(CH 2 ) a NHSO 3 − ,

each of R 44 and R 49 is independently —H or —CH 3 ;

(PS) is a sulfated or non-sulfated polysaccharide chain comprising one or more monosaccharide units connected by glycosidic linkages; and

‘a’ is an integer from 1 to 10, ‘c’ is an integer from 1 to 100, and each of ‘m’ and ‘n’ independently is an integer from 1 to 3;

with the proviso that if:

each of X 1 and X 2 is independently —CN, —CO 2 R 1 or —CONR 2 R 3 ;

each of Y 1 and Y 2 is independently —NR 4 R 5 or

and

Z 1 is a direct bond, then:

each of R 1 , R 2 , R 3 , R 4 and R 5 is not simultaneously —H; and

m, n, N and Z 1 together do not form a 5- or 6-membered ring.

2. The compound of claim 1 , wherein each of X 1 and X 2 is independently —CONR 2 R 3 , and each of Y 1 and Y 2 is independently —NR 4 R 5 .

3. The compound of claim 2 , wherein each of R 2 and R 4 is —H, and R 3 is —CH 2 (CHOH) a R 44 or —(CH 2 CH 2 O) c R 49 , and R 5 is —H or —(CH 2 CH 2 O) c R 49 .

4. The compound of claim 3 , wherein R 3 is —(CH 2 CH 2 O) c R 49 , and R 5 is —H.

5. The compound of claim 4 , wherein R 49 is —CH 3 , and ‘c’ is an integer from 1 to 20.

6. The compound of claim 1 , wherein each of X 1 and X 2 is independently —CO 2 R 1 , and each of Y 1 and Y 2 is independently —NR 4 R 5 .

7. The compound of claim 6 , wherein each of R 1 and R 4 is —H, and R 5 is —CH 2 (CHOH) a R 44 or —(CH 2 CH 2 O) c R 49 .

8. The compound of claim 7 , wherein R 44 is —H, R 49 is —CH 3 , ‘a’ is an integer from 1 to 6, and ‘c’ is an integer from 1 to 20.

9. The compound of claim 1 , wherein each of X 1 and X 2 is —CN, and each of Y 1 and Y 2 is

—NR 4 R 5 .

10. The compound of claim 9 , wherein R 4 is —H, and R 5 is —CH 2 (CHOH) a R 44 or —(CH 2 CH 2 O) c R 49 .

11. The compound of claim 10 , wherein R 44 is —H, R 49 is —CH 3 , ‘a’ is an integer from 1 to 6, and ‘c’ is an integer from 1 to 20.

12. The compound of claim 1 , wherein each of X 1 and X 2 is —CONH(PS), and each of Y 1 and Y 2 is —NR 4 R 5 .

13. The compound of claim 12 , wherein each of R 4 and R 5 is independently —H or —CH 2 (CHOH) a R 44 .

14. The compound of claim 13 , wherein each of R 4 and R 5 is —H.

15. The compound of claim 12 , wherein the one or more monosaccharide units of the polysaccharide chain (PS) are selected from the group consisting of glucose, fructose, mannose, xylose, and ribose.

Assignments (3)
ENTITY CONVERSION Recorded Oct 13, 2015
From: MEDIBEACON, LLC
To: MEDIBEACON, INC.
Reel/Frame 036852/0201 →
CHANGE OF NAME Recorded Feb 10, 2014
From: MEDIBEACON DEVELOPMENT, LLC
To: MEDIBEACON, LLC
Reel/Frame 032186/0575 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2012
From: MALLINCKRODT LLC
To: MEDIBEACON DEVELOPMENT LLC
Reel/Frame 029453/0920 →