IP Library Granted Patent US 9,975,061
Granted Patent B2
US 9,975,061 · App. 13/344,196 · Granted May 22, 2018

Evaporative concentrator and associated methods

Inventors: Russell M. Keckler, III (Findlay, OH); Daniel K. DeArment (Findlay, OH)
Assignee: Aptim Intellectual Property Holdings, LLC
B01D3/4216B01D45/12B01D45/16B01D1/16
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Quick Facts
Patent No.
US 9,975,061
App. No.
13/344,196
Granted
May 22, 2018
Kind
B2
Abstract

Disclosed herein are methods of concentrating liquid waste streams including methods comprising drawing a fluidized gas liquid mixture containing water from a mixing cavity into a multi-stage cyclonic separator comprising a first cyclonic separation chamber and a second cyclonic separation chamber in fluid communication with the first cyclonic separation chamber; draining a liquid discharge from the cyclonic separator into a liquid sump; and supplying a liquid contained in the sump to the mixing cavity. Related methods comprise steps such as supplying a liquid waste feed to a concentrator having a mixing cavity and a first cyclonic separation chamber and feeding a supply gas to the mixing cavity. Evaporative concentrators configured to practice these methods are also disclosed.

Claims (48)

1. A method of concentrating a liquid waste stream comprising:

a. supplying a first exhaust feed gas to a supply conduit through a first exhaust flow control device;

b. regulating the first exhaust flow control device based on the pressure of the first exhaust feed gas;

c. providing the first exhaust feed gas from the supply conduit to a mixing cavity;

d. introducing a mixing cavity liquid feed into the mixing cavity to form a fluidized gas liquid mixture;

e. conveying the fluidized gas liquid mixture from the mixing cavity to a first cyclonic separation chamber;

f. removing a first liquid portion from the fluidized gas liquid mixture by centrifugal force within the first cyclonic separation chamber;

g. removing a second liquid portion from the fluidized gas liquid mixture by centrifugal force in a second cyclonic separation chamber and introducing the second liquid portion to the first cyclonic separation chamber; and

h. draining a liquid discharge from the first cyclonic separation chamber into a liquid sump.

2. The method of claim 1 wherein the first exhaust feed gas is a byproduct of the combustion of a biofuel.

3. The method of claim 1 wherein a gaseous discharge from the second cyclonic separation chamber flows into a gaseous concentrator discharge line.

4. The method of claim 3 further comprising conveying a second exhaust feed gas to the gaseous concentrator discharge line to form a combined gaseous discharge, wherein the gaseous discharge from the second cyclonic separation chamber has a relative humidity that is greater than the combined gaseous discharge from the gaseous concentrator discharge line.

5. The method of claim 3 wherein the temperature of the first exhaust feed gas is greater than 600° F.

6. The method of claim 3 wherein the second exhaust feed gas comprises a biofuel combustion exhaust stream.

7. The method of claim 3 wherein the gaseous discharge has a relative humidity that is higher than the relative humidity of the first exhaust feed gas.

8. The method of claim 1 , wherein the mixing cavity liquid feed is the only substantial source of liquid phase water added to the mixing cavity.

9. The method of claim 1 , wherein the liquid discharge has a volumetric flow rate that is less than 50% of the volumetric flow rate of the mixing cavity liquid feed.

10. The method of claim 1 , wherein a volume reduction rate is represented by the difference between the mixing cavity liquid feed flow rate and the liquid discharge flow rate and the volume reduction rate is greater than 2% of the mixing cavity liquid feed flow rate.

11. The method of claim 1 , wherein the mixing cavity liquid feed comprises solids.

12. The method of claim 1 , wherein the mixing cavity liquid feed is aqueous.

13. The method of claim 1 , wherein the mixing cavity liquid feed is not potable.

14. A method of concentrating a liquid waste stream comprising:

a. supplying a first exhaust feed gas to a supply conduit through a first exhaust flow control device;

b. regulating the first exhaust flow control device based on the pressure of the first exhaust feed gas;

c. providing the first exhaust feed gas from the supply conduit to a mixing cavity;

d. introducing a mixing cavity liquid feed into the mixing cavity to form a fluidized gas liquid mixture;

e. conveying the fluidized gas liquid mixture from the mixing cavity to a first cyclonic separation chamber;

f. separating a first liquid portion from the fluidized gas liquid mixture by centrifugal force and removing the first liquid portion from the first cyclonic separation chamber;

g. conveying a first exhaust from the first cyclonic separation chamber to a second cyclonic separation chamber,

h. separating a second liquid portion from the first exhaust by centrifugal force and removing the second liquid portion from the second cyclonic separation chamber; and

i. conveying the second liquid portion from the second cyclonic separation chamber to the first cyclonic separation chamber; and

j. draining a liquid discharge from the first cyclonic separation chamber into a liquid sump.

15. An evaporative concentrator comprising:

a. a supply conduit in fluid communication with a source of a combustion heated gas;

b. a mixing cavity in fluid communication with the supply conduit;

c. a venturi in fluid communication with the mixing cavity;

d. a multi-stage cyclonic separator in fluid communication with the venturi;

e. wherein the cyclonic separator comprises a first cyclonic separation chamber and a second cyclonic separation chamber for separation by centrifugal force;

f. a sump;

g. a recycle line arranged and configured to deliver liquid from the sump to the mixing cavity;

h. a gaseous concentrator discharge line;

i. a gaseous flow path connecting the supply conduit, the mixing cavity, the venturi, the first cyclonic separation chamber, the second cyclonic separation chamber, and the gaseous concentrator discharge line respectively;

j. a first cyclonic separation chamber drain fluidly connected to the sump;

k. a second cyclonic separation chamber drain, wherein the second cyclonic separation chamber drain drains to the first cyclonic separation chamber; and

l. wherein the gaseous flow path from the venturi to the first cyclonic separation chamber changes direction at an approximately right angle.

16. The evaporative concentrator of claim 15 , wherein the first cyclonic separation chamber, the second cyclonic separation chamber, the sump and the gaseous concentrator discharge line comprise a single vessel.

17. The evaporative concentrator of claim 16 , wherein the first cyclonic separation chamber, the second cyclonic separation chamber, the sump and the gaseous concentrator discharge line are aligned about a central axis.

18. The evaporative concentrator of claim 17 , wherein the second cyclonic separation chamber drain is configured to pass fluid from the second cyclonic separation chamber through the first cyclonic separation chamber proximate the central axis to the first cyclonic separation chamber drain.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded May 28, 2024
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
To: APTIM INTELLECTUAL PROPERTY HOLDINGS, LLC (FKA SHAW INTELLECTUAL PROPERTY HOLDINGS, LLC); APTIM GOVERNMENT SOLUTIONS, LLC (FKA CB&I GOVERNMENT SOLUTIONS, LLC)
Reel/Frame 067535/0309 →
SECURITY INTEREST Recorded May 24, 2024
From: APTIM GOVERNMENT SOLUTIONS, LLC; APTIM INTELLECTUAL PROPERTY HOLDINGS, LLC
To: JPMORGAN CHASE BANK, N.A., AS JUNIOR LIEN COLLATERAL AGENT
Reel/Frame 067524/0085 →
SECURITY INTEREST Recorded May 23, 2024
From: APTIM GOVERNMENT SOLUTIONS, LLC; APTIM INTELLECTUAL PROPERTY HOLDINGS, LLC
To: JPMORGAN CHASE BANK, N.A., AS SENIOR SECURED COLLATERAL AGENT
Reel/Frame 067514/0322 →
CHANGE OF NAME Recorded Mar 2, 2018
From: SHAW INTELLECTUAL PROPERTY HOLDINGS, LLC
To: APTIM INTELLECTUAL PROPERTY HOLDINGS, LLC
Reel/Frame 045513/0376 →
SECURITY INTEREST Recorded Jul 6, 2017
From: SHAW INTELLECTUAL PROPERTY HOLDINGS, LLC; CB&I GOVERNMENT SOLUTIONS, LLC; LFG SPECIALTIES, L.L.C.; CB&I ENVIRONMENTAL & INFRASTRUCTURE, INC.
To: U.S. BANK NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 042915/0657 →
SECURITY INTEREST Recorded Jun 30, 2017
From: SHAW INTELLECTUAL PROPERTY HOLDINGS, LLC; CB&I GOVERNMENT SOLUTIONS, LLC; LFG SPECIALTIES, L.L.C.; CB&I ENVIRONMENTAL & INFRASTRUCTURE, INC.
To: UBS AG, STAMFORD BRANCH, AS ABL COLLATERAL AGENT
Reel/Frame 042875/0116 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 12, 2013
From: KECKLER, RUSSELL M., III; DEARMENT, DANIEL K.
To: SHAW INTELLECTUAL PROPERTY HOLDINGS, LLC
Reel/Frame 029617/0819 →
Continuity (2)
Provisional Application 61429843 · Jan 5, 2011
Related Publication 20120168092A1 · Jul 5, 2012