IP Library Granted Patent US 9,181,405
Granted Patent B2
US 9,181,405 · App. 13/350,049 · Granted Nov 10, 2015

Formaldehyde-free lignin-amine coagulants

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Quick Facts
Patent No.
US 9,181,405
App. No.
13/350,049
Granted
Nov 10, 2015
Kind
B2
Abstract

A method for making lignin-amines is provided. The method comprises providing a lignin; then modifying the lignin with modifier to create a modified lignin; and then reacting the modified lignin with an amine to form a lignin-amine. Suitable modifiers comprise acrylates. A method for coagulating suspended materials in a water stream is also disclosed. The method comprises providing a water stream and contacting the suspended materials in the water stream with at least one lignin-amine.

Claims (10)

1. Coagulant composition comprising a lignin-amine having the formula:

where R 1 , R 2 , R 3 may be the same or different and selected from the group consisting of hydrogen, methyls, ethyls, alkyls, hydroxyl-substituted alkyls, and alkoxy-substituted alkyls of 1 to 20 carbon atoms; the alkyl groups may be straight or branched alkyl groups or a cycloalkyl ring, whereby said composition, when added to a water stream, coagulates suspended particles therein.

2. Coagulant composition comprising a lignin-amine having the formula:

where R 1 , R 2 , R 3 may be the same or different and selected from the group consisting of hydrogen, methyls, ethyls, alkyls, hydroxyl-substituted alkyls, and alkoxy-substituted alkyls of 1 to 20 carbon atoms; the alkyl groups may be straight or branched alkyl groups or a cycloalkyl ring, whereby said composition when added to a water stream coagulates suspended particles therein.

3. Coagulant composition as recited in claim 1 wherein said composition is water soluble.

4. Coagulant composition as recited in claim 3 wherein said composition is present in an aqueous solution including a salt.

5. Coagulant composition as recited in claim 4 wherein said salt is a hydrochloride salt.

6. Coagulant composition as recited in claim 4 wherein said aqueous solution has a pH of about 7 or less.

7. Coagulant composition as recited in claim 1 wherein R 1 =H and R 2 and R 3 are both ethyl.

8. Coagulant composition as recited in claim 1 wherein said composition is devoid of formaldehyde.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 12, 2018
From: GENERAL ELECTRIC COMPANY
To: BL TECHNOLOGIES, INC.
Reel/Frame 047502/0065 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2012
From: DONG, HONGCHEN; PENG, WENQING; LEWIS, LARRY NEIL
To: GENERAL ELECTRIC COMPANY
Reel/Frame 027900/0563 →