IP Library Granted Patent US 8,454,890
Granted Patent B2
US 8,454,890 · App. 13/353,033 · Granted Jun 4, 2013

Peracetic acid vapor sterilization of food and beverage containers

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Quick Facts
Patent No.
US 8,454,890
App. No.
13/353,033
Granted
Jun 4, 2013
Kind
B2
Abstract

The present invention is directed to a method of sterilizing a surface comprising treating such surface with a vapor comprising peracetic acid at a concentration of at least about 3500 ppm at between about 57° and about 75° C. Such method is preferably conducted in the absence of a hydrogen peroxide initiator, and is particularly suitable for the sterilization of polyethylene terephthalate bottles.

Claims (11)

1. A method of sterilizing a surface comprising the steps of:

(a) adding a peracetic acid solution to a heated gas stream to form a vapor phase peracetic acid stream; and

(b) sterilizing said surface with said vapor phase peracetic acid stream wherein the peracetic acid is substantially entirely in the gaseous form with a concentration of between about 3500 ppm and about 10,000 ppm with a temperature between about 57° and about 75° C. wherein said sterilizing occurs for 5 to 10 seconds.

2. The method of claim 1 wherein said surface is composed of plastic.

3. The method of claim 1 wherein said surface is polyethylene terephthalate.

4. The method of claim 1 wherein said sterilizing is conducted in the absence of a hydrogen peroxide activator.

5. The method of claim 1 wherein the concentration of peracetic acid is at least about 3750 ppm.

6. The method of claim 5 wherein the concentration of peracetic acid is between about 3750 and about 4250 ppm.

7. The method of claim 1 wherein the vapor is less than 100% saturated.

8. The method of claim 7 wherein the saturation of the vapor is less than about 85%.

9. The method of claim 8 wherein the saturation of the vapor is between about 75% and about 85%.

Assignments (9)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2021
From: PEROXYCHEM LLC
To: EVONIK OPERATIONS GMBH
Reel/Frame 055622/0724 →
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 050605/0305 Recorded Feb 3, 2020
From: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
To: PEROXYCHEM LLC
Reel/Frame 051777/0957 →
SECURITY INTEREST Recorded Oct 2, 2019
From: PEROXYCHEM LLC
To: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
Reel/Frame 050605/0305 →
RELEASE OF SECURITY INTEREST Recorded Oct 2, 2019
From: BANK OF AMERICA, N.A., AS AGENT
To: PEROXYCHEM LLC
Reel/Frame 050606/0329 →
RELEASE OF SECURITY INTEREST Recorded Nov 4, 2015
From: MACQUARIE US TRADING LLC, AS COLLATERAL AGENT
To: PEROXYCHEM LLC
Reel/Frame 036953/0766 →
SECURITY INTEREST Recorded Oct 21, 2015
From: PEROXYCHEM LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036847/0594 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2014
From: FMC CORPORATION
To: PEROXYCHEM LLC
Reel/Frame 032558/0681 →
SHORT FORM PATENT SECURITY AGREEMENT Recorded Mar 3, 2014
From: PEROXYCHEM LLC
To: MACQUARIE US TRADING LLC
Reel/Frame 032379/0931 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2012
From: ROVISON, JOHN M.; LYMBURNER, CHARLES J.; ABRAHAM, SHIBU; THOMPSON, ANGELA
To: FMC CORPORATION
Reel/Frame 027900/0001 →