IP Library Granted Patent US 9,149,663
Granted Patent B2
US 9,149,663 · App. 13/361,212 · Granted Oct 6, 2015

Antiperspirant emulsion compositions and processes for making antiperspirant emulsion compositions

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Quick Facts
Patent No.
US 9,149,663
App. No.
13/361,212
Granted
Oct 6, 2015
Kind
B2
Abstract

Processes for making an antiperspirant emulsion composition and antiperspirant emulsion compositions are provided herein. In an embodiment, a process for making an antiperspirant emulsion composition includes combining water and an antiperspirant active component to form a water phase. A hydrophobic carrier and a structurant are combined to form an oil phase. The structurant has a melting point above ambient temperature. The oil phase is heated to a first temperature of at least a melting point of the structurant that is disposed in the oil phase. The water phase and the heated oil phase are mixed to form the antiperspirant emulsion composition. The antiperspirant emulsion composition is cooled under continued mixing.

Claims (27)

1. A process for making an antiperspirant emulsion composition, the process comprising the steps of:

combining water and an antiperspirant active component to form a water phase;

combining a hydrophobic carrier and a structurant to form an oil phase, the structurant having a melting point above ambient temperature;

heating the oil phase to a first temperature of at least a melting point of the structurant disposed therein;

mixing the water phase and the heated oil phase at a mixing temperature of at least the melting point of the structurant and different from the first temperature to form the antiperspirant emulsion composition; and

cooling the antiperspirant emulsion composition under continued mixing

wherein the antiperspirant emulsion composition is cooled to a cooling temperature below a pour point of the antiperspirant emulsion composition under continued mixing.

2. The process of claim 1 , wherein the cooling temperature is ambient temperature.

3. The process of claim 1 , wherein the cooling temperature is above ambient temperature, and wherein mixing is ceased prior to further cooling to ambient temperature.

4. The process of claim 1 , wherein the structurant has a melting point within a range of from about 50 to about 100° C.

5. The process of claim 1 , wherein the water phase is present in the antiperspirant emulsion composition in an amount of from about 60 to about 85 weight % and the oil phase is present in the antiperspirant emulsion composition in an amount of from about 15 to about 40 weight %, both based upon the total weight of the antiperspirant emulsion composition.

6. The process of claim 5 wherein the antiperspirant active component is present in the water phase in an amount of from about 10 to about 90 weight %, based upon the total weight of the water phase.

7. The process of claim 5 wherein the structurant is present in the oil phase in an amount of from about 20 to about 60 weight %, based upon the total weight of the oil phase.

8. The process of claim 1 , wherein the water phase further comprises an additional structurant.

9. The process of claim 1 , wherein the antiperspirant emulsion composition has a hardness of less than or equal to about 150 grams force.

10. An antiperspirant emulsion composition made by a process comprising the steps of:

combining water and an antiperspirant active component to form a water phase;

combining a hydrophobic carrier and a structurant to form an oil phase, the structurant having a melting point above ambient temperature;

heating said oil phase to a first temperature of at least a melting point of said structurant disposed therein;

mixing said water phase and said heated oil phase at a mixing temperature of at least the melting point of the structurant and different from the first temperature to form said antiperspirant emulsion composition; and

cooling said antiperspirant emulsion composition under continued mixing; wherein the antiperspirant emulsion composition is cooled to a cooling temperature below a pour point of the antiperspirant emulsion composition under continued mixing.

11. The antiperspirant emulsion composition of claim 10 , wherein said structurant has a melting point within a range of from about 50 to about 100° C.

12. The antiperspirant emulsion composition of claim 10 , wherein said water phase is present in said antiperspirant emulsion composition in an amount of from about 60 to about 85 weight % and said oil phase is present in said antiperspirant emulsion composition in an amount of from about 15 to about 40 weight %, both based upon the total weight of said antiperspirant emulsion composition.

13. The antiperspirant emulsion composition of claim 12 wherein said antiperspirant active component is present in said water phase in an amount of from about 10 to about 90 weight %, based upon the total weight of said water phase.

14. The antiperspirant emulsion composition of claim 12 , wherein said structurant is present in said oil phase in an amount of from about 20 to about 60 weight %, based upon the total weight of said oil phase.

15. The antiperspirant emulsion composition of claim 10 , wherein said water phase further comprises an additional structurant.

16. The antiperspirant emulsion composition of claim 10 having a hardness of less than or equal to about 150 grams force.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: HENKEL IP & HOLDING GMBH
To: HENKEL AG & CO. KGAA
Reel/Frame 059357/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2017
From: HENKEL US IV CORPORATION
To: HENKEL IP & HOLDING GMBH
Reel/Frame 042108/0150 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 9, 2017
From: THE DIAL CORPORATION
To: HENKEL US IV CORPORATION
Reel/Frame 041671/0407 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 30, 2012
From: THOMPSON, BEREA
To: THE DIAL CORPORATION
Reel/Frame 027617/0542 →