Method of making an enhanced natural sweetener
View Patent ↗A method of making a natural sweetening composition comprising the steps of (a) steam stripping a crude mixture of at least one plant based natural high intensity sweetening compound; and (b) at least one step of filtering the crude mixture.
1. A method of making a natural sweetening composition comprising stevia components having improved natural flavor qualities, consisting of:
(a) preparing a crude extract comprising water and at least one plant-based natural high intensity sweetener, wherein the high intensity sweetener compound is selected from the group consisting of steviol glycosides, glycyrrhizin, mogrosides, and mixtures thereof,
(b) providing at least one step of steam stripping the crude extract through a steam stripping column, wherein the steam stripping column has a head cap with a feed inlet and a vapor outlet disposed on a first end of the column and a bottom take-off with steam inlet and feed outlet disposed on an opposing second end of the column, and establishing a countercurrent flow by:
(i) allowing the crude extract to flow from the first end of the column against a rate of steam that flows from the opposing second end,
(ii) introducing the crude extract at a feed rate of about 5 mL/min, and a steam flow at a feed ratio of about 12:1 to about 19:1 relative to the feed rate of the crude extract, and
(iii) transferring the volatile components to a vapor phase,
(iv) removing from the crude extract the volatile components; and
(c) providing a first stage membrane fractionation and a second stage membrane fractionation, both fractionation stages being performed with a semi-permeable membrane having a porosity between about 2,000 to about 10,000 nm wco to filter the crude extract after removal of said volatile components, and to form a permeate and a retentate,
wherein the first stage of membrane fractionation is performed for about 2 hours by using a permeate flow rate of 80 ml/min, and the second stage of membrane fractionation is performed for about 3 hours by using a permeate flow rate from 5 ml/min to 17 ml/min,
wherein the resulting permeate at the end of second stage of fractionation is golden in color and has a higher total percentage of a mixture of rebaudioside A and stevioside in the permeate compared to total percentage of a mixture of rebaudioside F, D, C and dulcoside A in the permeate.
2. The method of claim 1 , wherein the sweetening composition is subjected to a drying process.
3. The method of claim 1 , wherein the sweetening composition is combined with a carrier material.
4. The method of claim 1 , wherein the sweetening composition is co-crystallized with a carrier material.
5. The method of claim 1 , further comprising a plant based natural low intensity sweetening compound.
6. The method of claim 5 , wherein the crude extract of stevia includes the plant based natural low intensity sweetening compound.
7. The method of claim 5 wherein the plant based natural low intensity sweetening compound is a fruit-derived sweetener.
8. The method of claim 1 , wherein the crude extract of stevia is modified by enzymatic action or microbial fermentation.
9. The method of claim 1 , wherein the process of making the composition does not include the recovery of volatile components.
10. The method of claim 1 , wherein the membrane fractionation is accomplished using a hollow fiber configuration.
11. The method of claim 1 , wherein the steam strip column is operated in a vertical orientation, perpendicular to the ground.
12. The method of claim 1 , wherein the steam strip column is operated in a continuous flow method.