IP Library Granted Patent US 8,877,149
Granted Patent B2
US 8,877,149 · App. 13/369,881 · Granted Nov 4, 2014

Combustion flue gas NO

Inventors: Henry A. Pfeffer (Mercerville, NJ); David E. Smith (Plainsboro, NJ)
Assignee: Peroxychem LLC
B01D53/60B01D2251/106B01D2251/2062B01D53/869B01D53/58B01D2251/404B01D53/56B01D53/75B01D2251/206B01D2251/606B01D2251/2067B01D2251/304Y02C20/10B01D53/8625
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Quick Facts
Patent No.
US 8,877,149
App. No.
13/369,881
Granted
Nov 4, 2014
Kind
B2
Abstract

Combustion flue gas containing NO X and SO X is treated to remove NO X in a multistep system in which NO X is reduced in the flue gas stream via selective catalytic reduction or selective non-catalytic reduction with ammonia or an ammonia-forming compound, followed treatment with hydrogen peroxide to remove residual ammonia and, optionally, treatment with an alkali reagent to reduce residual NO X in the flue gas stream. The NO X -depleted flue gas stream may also be subjected to a desulfurization treatment for removal of SO X .

Claims (7)

1. A method for removing NOx from a flue gas stream comprising

subjecting an electric utility power plant combustion flue gas stream containing NOx to a selective catalytic reduction operation or selective non-catalytic reduction operation by injecting ammonia or an ammonia-forming compound into the flue gas stream as an agent for reducing the NOx, wherein an excess of ammonia is introduced to yield a flue gas stream containing unreacted residual ammonia and a reduced concentration of NOx; and

thereafter injecting hydrogen peroxide into the flue gas stream containing unreacted residual ammonia, in an amount sufficient to react with the residual ammonia present in the flue gas stream, the flue gas having a temperature of up to about 700° F. during the hydrogen peroxide injection operation, and wherein the reduction operation and the hydrogen peroxide injection operation are downstream from an economizer, to yield a flue gas stream having a reduced concentration of residual ammonia.

2. The method of claim 1 wherein the ammonia is introduced into flue gas stream in an amount sufficient to provide at least about 50% stoichiometric molar excess, based on the amount of NO X present in the flue gas stream.

3. The method of claim 1 wherein the hydrogen peroxide is employed as an aqueous hydrogen peroxide solution in combination with an activator.

4. The method of claim 1 wherein the hydrogen peroxide is injected into the ammonia-containing flue gas stream in an amount sufficient to provide at least about ¼ mole H 2 O 2 per mole NH 3 up to about 15 moles of H 2 O 2 per mole NH 3 present in the flue gas stream.

5. The method of claim 1 wherein sufficient hydrogen peroxide is contacted with the ammonia-containing flue gas stream to reduce the ammonia concentration in the H 2 O 2 -treated flue gas stream to less than about 10 ppm NH 3 .

Assignments (7)
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 050605/0305 Recorded Feb 3, 2020
From: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
To: PEROXYCHEM LLC
Reel/Frame 051777/0957 →
RELEASE OF SECURITY INTEREST Recorded Oct 2, 2019
From: BANK OF AMERICA, N.A., AS AGENT
To: PEROXYCHEM LLC
Reel/Frame 050606/0329 →
SECURITY INTEREST Recorded Oct 2, 2019
From: PEROXYCHEM LLC
To: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
Reel/Frame 050605/0305 →
RELEASE OF SECURITY INTEREST Recorded Nov 4, 2015
From: MACQUARIE US TRADING LLC, AS COLLATERAL AGENT
To: PEROXYCHEM LLC
Reel/Frame 036953/0766 →
SECURITY INTEREST Recorded Oct 21, 2015
From: PEROXYCHEM LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036847/0594 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2014
From: FMC CORPORATION
To: PEROXYCHEM LLC
Reel/Frame 032558/0681 →
SHORT FORM PATENT SECURITY AGREEMENT Recorded Mar 3, 2014
From: PEROXYCHEM LLC
To: MACQUARIE US TRADING LLC
Reel/Frame 032379/0931 →
Continuity (3)
Continuation 12778675 · May 12, 2010
Provisional Application 61178689 · May 15, 2009
Related Publication 20120141346A1 · Jun 7, 2012