IP Library Granted Patent US 8,833,681
Granted Patent B2
US 8,833,681 · App. 13/379,778 · Granted Sep 16, 2014

Method and apparatus for defibrillating cellulose fibers

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,833,681
App. No.
13/379,778
Granted
Sep 16, 2014
Kind
B2
Abstract

The current invention is directed to a method and apparatus for defibrillating cellulose fibers achieved through single or multiple passes of raw or pre-processed cellulose fiber slurry with a preferred solid material consistency range of 35% to 55% through twin-screw fiber processing machines. During this processing operation fiber slurries are optionally further enhanced with additional fiber and mineral additives to optimize performance of the material for specific end purposes. The hyper defibrillated fiber slurry produced can be defined as one reaching a Schopper-Riegler (SR) level between 75 SR and 85 SR and/or producing a pressed, dried board with a density of preferably at least 850 kg/m 3 .

Claims (19)

1. Method for the treatment of a composition comprising cellulose fibres into a composition comprising cellulose microfibers, said method comprises the steps of:

a) Providing a composition comprising fibres;

b) Admixing aqueous solution/solvent to said composition comprising cellulose fibres to provide a pulp suspension comprising cellulose fibres;

c) Feeding said pulp suspension comprising cellulose fibres into a mechanical defibrillation process using a refining twin screw;

d) Refining said pulp suspension comprising cellulose fibres with at least the use of said refining twin screw, to provide a composition comprising cellulose microfibers,

e) wherein in step b) the pulp suspension has a consistency of between 45% and 55%, and the composition comprising cellulose microfibers has a Schopper-Riegler value (SR) upon leaving the twin screw of step c) of at least 80° SR.

2. The method according to claim 1 wherein said composition comprising cellulose microfibers at the end of the refining step has a density of at least 850 kg/m 3 .

3. The method according to claim 1 wherein said composition comprising cellulose microfibers has a density of between, and including, 1000 kg/m 3 and 1450 kg/m 3 .

4. The method according to claim 1 wherein the composition comprising cellulose microfibers has a Schopper-Riegler value (SR) before any drying and upon leaving the twin-screw of the process, of between and including 80° SR and 90° SR.

5. The method according to claim 1 wherein the composition comprising cellulose fibres of step a) is selected from the group consisting of paper, waste paper, and recycled paper.

6. The method according to claim 1 , comprising a further step of adding one or more further additives after the refining step.

7. The method according to claim 6 , wherein the further additives are selected from the group comprising mineral and organic fillers, flow modifiers, sizing agents, dyes, coloured pigments and mordents.

8. Method according to claim 1 , wherein the refining twin screw is a co-rotating twin screw or a counter-rotating twin screw.

9. Method according to claim 1 , further comprising the step of moulding a 2- or 3-dimensional shaped body from said composition comprising cellulose microfiber stock.

10. Method according to claim 1 further comprising the step of moulding of a sheet from said composition comprising cellulose microfibers and attaching said sheet to a carrier to form a flooring tile.

11. A method according to claim 1 wherein the fibres are introduced dry and inlets are provided to introduce liquid to be combined with the fibres.

12. The method according to claim 1 wherein said composition comprising cellulose microfibers has a density of between, and including, 1150 kg/m 3 and 1400 kg/m 3 .

13. The method according to claim 1 wherein said composition comprising cellulose microfibers has a density of between, and including, 1300 kg/m 3 and 1400 kg/m 3 .

14. The method according to claim 1 wherein the composition comprising cellulose microfibers has a Schopper-Riegler value (SR) before any drying and upon leaving the twin-screw of the process, of between and including 80° SR and 88° SR.

Assignments (13)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2020
From: BASF SE
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 054735/0659 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2013
From: ZELFO TECHNOLOGY GMBH
To: BASF SE
Reel/Frame 031169/0669 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2013
From: INTERFACE INTERNATIONAL BV
To: INTERFACE EUROPEAN MANUFACTURING BV
Reel/Frame 030055/0745 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2013
From: INTERFACE EUROPEAN MANUFACTURING BV
To: ZELFO TECHNOLOGY GMBH
Reel/Frame 030055/0697 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 2, 2012
From: DEAN, TREVOR W R; TARVERDI, KARNIK; BRAMSTEIDL, ROBERT; ACHILLI, LUCA
To: INTERFACE INTERNATIONAL B.V.
Reel/Frame 028534/0560 →