IP Library Granted Patent US 9,404,878
Granted Patent B2
US 9,404,878 · App. 13/387,406 · Granted Aug 2, 2016

Systems and methods for detecting an H

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Quick Facts
Patent No.
US 9,404,878
App. No.
13/387,406
Granted
Aug 2, 2016
Kind
B2
Abstract

A system for detecting a hydrogen peroxide (H2O2) concentration in a cold aseptic filling system that uses a peracetic acid (PAA)-based cleaning solution is shown and described. The system includes a conductivity sensor configured to receive the PAA-based cleaning solution and to provide a signal representative of the electrical conductivity of the PAA-based cleaning solution. The system further includes a controller configured to receive the signal representative of the electrical conductivity of the PAA-based cleaning solution and to compare the signal to a threshold value associated with a setpoint H2O2 concentration.

Claims (41)

1. A system for detecting a hydrogen peroxide (H 2 O 2 ) concentration in a cold aseptic filling system that uses a peracetic acid (PAA)-based cleaning solution, the system comprising:

a primary conduit through which the PAA-based cleaning solution is circulated;

a bypass conduit fluidly coupled to the primary conduit;

a conductivity sensor positioned in the bypass conduit, the conductivity sensor configured to receive a portion of the PAA-based cleaning solution from the primary conduit via the bypass conduit and to provide a signal representative of the electrical conductivity of the PAA-based cleaning solution and to compare the signal to a threshold value associated with a setpoint H 2 O 2 concentration,

wherein the concentration of PAA in the PAA-based cleaning solution is depleted over time,

wherein the cold aseptic filling system is configured to dose the PAA-based cleaning solution with additional PAA to counteract the depletion, and

wherein the portion of the PAA-based cleaning solution provided to the conductivity sensor is returned to the primary conduit.

2. The system of claim 1 , wherein the cold aseptic filling system is configured to recirculate the PAA-based cleaning solution.

3. The system of claim 1 , wherein the controller is configured to generate an alarm when the signal representative of the electrical conductivity of the PAA-based cleaning solution is greater than the threshold value associated with the setpoint H 2 O 2 concentration.

4. The system of claim 1 , wherein the controller is remote from the conductivity sensor and the system further comprises:

a transmitter locally coupled to the conductivity sensor, the transmitter configured to receive the signal representative of the electrical conductivity of the PAA-based cleaning solution and to provide the signal to the controller.

5. The system of claim 4 , further comprising:

a display coupled to the transmitter and configured to display indicia representative of the electrical conductivity of the PAA-based cleaning solution.

6. The system of claim 4 , wherein the transmitter is configured to wirelessly transmit the signal via radio frequency communications.

7. The system of claim 1 , wherein the controller includes a processing circuit configured to receive the signal representative of the electrical conductivity of the PAA-based cleaning solution, wherein the processing circuit is configured to cause a display coupled to the processing circuit to display indicia representative of the electrical conductivity of the PAA-based cleaning solution.

8. The controller of claim 7 , wherein the processing circuit is further configured to generate an alarm when the signal representative of the electrical conductivity of the PAA-based cleaning solution is greater than the threshold value associated with the setpoint H 2 O 2 concentration.

9. A method for detecting a hydrogen peroxide (H 2 O 2 ) concentration in a cold aseptic filling system, the method comprising:

circulating a peracetic acid (PAA)-based cleaning solution through a primary conduit of the cold aseptic filling system;

bypassing a portion of the PAA-based cleaning solution to a conductivity sensor;

measuring the electrical conductivity of the PAA-based cleaning solution with the conductivity sensor;

providing a signal representative of the measured electrical conductivity from the conductivity sensor to a controller;

using the controller to compare the signal representative of the electrical conductivity of the PAA-based cleaning solution to a threshold value associated with a setpoint H 2 O 2 concentration;

routing the portion of the PAA-based cleaning solution back to the primary conduit; recirculating the PAA-based cleaning solution such that the concentration of PAA in the PAA-based cleaning solution is depleted over time; and

dosing the recirculated PAA-based cleaning solution with additional PAA to counteract the depletion.

10. The method of claim 9 , further comprising:

generating an alarm when the signal representative of the electrical conductivity of the PAA-based cleaning solution is greater than the threshold value associated with the setpoint H 2 O 2 concentration.

11. The method of claim 9 , further comprising:

initiating a process to empty and refill the cold aseptic filling system with new PAA-based cleaning solution when the electrical conductivity of the PAA-based cleaning solution is greater than the threshold value associated with the setpoint H 2 O 2 .

12. The method of claim 9 , wherein providing a signal representative of the measured electrical conductivity from the conductivity sensor to a controller comprises:

providing the signal to a circuit local to the conductivity sensor that scales the signal for interpretation by the controller; and

transmitting the scaled signal to the controller via a transmitter.

13. The method of claim 9 , further comprising:

displaying indicia representative of the electrical conductivity of the PAA-based cleaning solution.

14. A method for detecting a hydrogen peroxide (H 2 O 2 ) concentration in a cold aseptic filling system, the method comprising:

circulating a peracetic acid (PAA)-based cleaning solution through the cold aseptic filling system to a conductivity sensor;

measuring the electrical conductivity of the PAA-based cleaning solution with the conductivity sensor;

providing a signal representative of the measured electrical conductivity from the conductivity sensor to a controller; and

using the controller to compare the signal representative of the electrical conductivity of the PAA-based cleaning solution to a threshold value associated with a setpoint H 2 O 2 concentration;

wherein the conductivity sensor is in parallel with hydraulics of the cold aseptic filling system such that the conductivity sensor continuously receives a flow of the PAA-based cleaning solution when the cold aseptic filling system is active with fluid flow, and

wherein the flow of PAA-based cleaning solution received by the conductivity sensor is directed back into fluid flow circulating through the cold aseptic filling system.

15. The method of claim 9 , wherein the threshold conductivity value is associated with a setpoint H 2 O 2 concentration of more than 7500 parts per million.

Assignments (13)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
RELEASE OF SECURITY AGREEMENT REEL/FRAME 045300/0141 Recorded Jul 10, 2023
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: DIVERSEY, INC.; THE BUTCHER COMPANY
Reel/Frame 064236/0722 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
2021 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0576 →
NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064348/0235 →
ABL PATENT SECURITY AGREEMENT Recorded Jul 6, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 064222/0751 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Jul 6, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 064223/0526 →
SECURITY AGREEMENT Recorded Feb 9, 2018
From: DIVERSEY, INC.; THE BUTCHER COMPANY
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 045300/0141 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2012
From: TROST, DETLEF; THEYSSEN, HOLGER
To: DIVERSEY, INC.
Reel/Frame 027846/0061 →