IP Library Granted Patent US 9,045,463
Granted Patent B2
US 9,045,463 · App. 13/389,269 · Granted Jun 2, 2015

Phenyl ethynyl derivatives as hepatitis C virus inhibitors

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Quick Facts
Patent No.
US 9,045,463
App. No.
13/389,269
Granted
Jun 2, 2015
Kind
B2
Abstract

Inhibitors of HCV replication of formula I including stereochemically isomeric forms, and salts, hydrates, solvates thereof, wherein R and R* have the meaning defined in the claims. The present invention also relates to processes for preparing said compounds, pharmaceutical compositions containing them and their use, alone or in combination with other HCV inhibitors, in the treatment or prophylaxis of HCV.

Claims (18)

1. A compound of formula I:

or a stereoisomer thereof, wherein:

R and R* are each independently —CR 1 R 2 R 3 , C 1-4 alkylamino, benzylamino, arylamino, aryl optionally substituted with 1 or 2 substituents selected from halo and methyl, hetero C 4-7 cycloalkyl; wherein

R 1 is selected from C 1-4 alkyl; phenyl optionally substituted with 1, 2 or 3 substituents independently selected from halo, C 1-4 alkyl, C 1-4 alkoxy, trifluoromethoxy or 2 substituents on adjacent ring atoms form a 1,3-dioxolane group; benzyl optionally substituted with halo or methoxy; phenylsulfonylmethyl; heteroaryl; heteroarylmethyl; and C 3-6 cycloalkyl;

R 2 is selected from hydrogen, hydroxyl, amino, mono- and di-C 1-4 alkylamino, C 1-4 alkylcarbonylamino, C 1-4 alkyloxycarbonylamino, C 1-4 alkylamino-carbonylamino, piperidin-1-yl or imidazol-1-yl;

R 3 is hydrogen, or alternatively,

R 2 and R 3 together form an oxo group; or

R 1 and R 3 together form cyclopropyl;

provided that when either one of R or R* represents —CH(C 6 H 5 )N(CH 3 ) 2 then the other cannot be —CH(C 6 H 5 )NHC(═O)OCH 3 ; and when R and R* are identical, then R 1 is other than phenyl when R 2 is hydroxyl, acetylamino, methoxycarbonylamino or tert. butoxycarbonylamino and R 3 is hydrogen; and R 1 is other than C 1-4 alkyl when R 2 is C 1-4 alkylcarbonylamino and R 3 is hydrogen;

or a pharmaceutically acceptable salt thereof.

2. A compound according to claim 1 wherein R and R* are —CR 1 R 2 R 3 or benzylamino.

3. A compound according to claim 2 wherein R and R* are —CR 1 R 2 R 3 .

4. A compound according to claim 1 wherein R 2 is hydrogen, hydroxyl, dimethylamino, acetylamino, methoxycarbonylamino, methylaminocarbonylamino, piperidin-1-yl or imidazol-1-yl.

5. A compound according to claim 1 wherein R 1 is selected from C 1-4 alkyl; phenyl optionally substituted with 1 or 2 substituents independently selected from halo, methyl, methoxy or 2 substituents on adjacent ring atoms form a 1,3-dioxolane group; heteroaryl and heteroarylmethyl.

6. A compound according to claim 5 wherein said heteroaryl is pyridinyl.

7. A compound according to claim 1 wherein the compound is of formula I-b

8. A pharmaceutical composition comprising a compound as defined in claim 1 , and a pharmaceutically acceptable carrier.

9. A method for treating an HCV infection in a mammal comprising administering to said mammal a pharmaceutical composition according to claim 8 .

Assignments (11)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2015
From: JANSSEN R & D IRELAND
To: JANSSEN SCIENCES IRELAND UC
Reel/Frame 035496/0382 →
CORRECTIVE ASSIGNMENT TO ADD PAGE 3 TO THE DOCUMENT PREVIOUSLY RECORDED ON REEL 027825 FRAME 0111. ASSIGNOR(S) HEREBY CONFIRMS ASSIGNMENT. Recorded Sep 25, 2014
From: MCGOWAN, DAVID C.; DEMIN, SAMUEL D.; LAST, STEFAAN J.; VANDYCK, KOEN; RABOISSON, PIERRE J-M.B.
To: TIBOTEC BVBA
Reel/Frame 033833/0833 →
CHANGE OF NAME Recorded Oct 28, 2013
From: TIBOTEC PHARMACEUTICALS
To: JANSSEN R&D IRELAND
Reel/Frame 031491/0376 →
CORRECT A TYPOGRAPHICAL ERROR IN A COVER SHEET PREVIOUSLY RECORDED. Recorded Oct 15, 2013
From: MCGOWAN, DAVID C.
To: TIBOTEC BVBA
Reel/Frame 031422/0103 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2013
From: DEMIN, SAMUEL D
To: TIBOTEC BVBA
Reel/Frame 031374/0636 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2013
From: MCGOWAN, DAVID C.
To: TIBOTEC BVBA
Reel/Frame 031374/0901 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2013
From: LAST, STEFAAN J.
To: TIBOTEC BVBA
Reel/Frame 031333/0720 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2013
From: RABOISSON, PIERRE JEAN-MARIE B.
To: TIBOTEC BVBA
Reel/Frame 031333/0726 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2013
From: VANDYCK, KOEN
To: TIBOTEC BVBA
Reel/Frame 031333/0724 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2012
From: TIBOTEC BVBA
To: TIBOTEC PHARMACEUTICALS
Reel/Frame 027825/0150 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2012
From: MCGOWAN, DAVID C.; DEMIN, SAMUEL D.; LAST, STEFAAN J.; VANDYCK, KOEN; RABOISSON, PIERRE J-M.B.
To: TIBOTEC BVBA
Reel/Frame 027825/0111 →