IP Library Granted Patent US 8,980,815
Granted Patent B2
US 8,980,815 · App. 13/404,577 · Granted Mar 17, 2015

Composition for cleaning a heat transfer system having an aluminum component

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Quick Facts
Patent No.
US 8,980,815
App. No.
13/404,577
Granted
Mar 17, 2015
Kind
B2
Abstract

Disclosed herein is a cleaner concentrate comprising: greater than 10 weight percent of a freezing point depressant, 0.5 to 35 weight percent of oxalic acid, and an azole compound, wherein weight percent is based on the total weight of the cleaner concentrate.

Claims (29)

1. A cleaner concentrate for a heat transfer system comprising:

greater than 15 weight percent of a freezing point depressant,

about 8 to 35 weight percent of oxalic acid, and

an azole compound,

wherein weight percent is based on the total weight of the cleaner concentrate,

wherein the cleaner concentrate is an uniform solution, and

wherein the solution is stable at about 10° F. to about 55° F.

2. The cleaner concentrate of claim 1 , wherein the freezing point depressant comprises ethylene glycol, propylene glycol, or a combination thereof.

3. The cleaner concentrate of claim 1 , wherein the oxalic acid is present in an amount of about 8 to 20 weight percent.

4. The cleaner concentrate of claim 1 , wherein the azole compound comprises benzotriazole, tolyltriazole, methyl benzotriazole, butyl benzotriazole, alkyl benzotriazoles, mercaptobenzothiazole, thiazole, substituted thiazoles, imidazole, benzimidazole, substituted imidazoles, indazole, substituted indazoles, tetrazole, substituted tetrazoles, and mixtures thereof.

5. The cleaner concentrate of claim 1 , wherein the azole compound is present in an amount of 0.001 to 20 weight percent based on the total weight of the cleaner concentrate.

6. The cleaner composition of claim 1 , further comprising a surfactant.

7. The cleaner composition of claim 1 , further comprising a colorant.

8. A method of cleaning a heat transfer system aluminum component comprising contacting the aluminum component with a cleaning solution comprising water and a cleaner concentrate according to claim 1 to produce a cleaned aluminum component wherein the aluminum component is made using controlled atmosphere brazing.

9. The method of claim 8 , wherein the aluminum component is exposed to the cleaning solution prior to being exposed to a heat transfer fluid.

10. The method of claim 8 , wherein the aluminum component is exposed to the cleaning solution prior to being exposed to a heat transfer fluid.

11. The method of claim 8 , wherein contacting occurs at a temperature greater than ambient temperature and less than the boiling point of the cleaning solution.

12. The method of claim 8 , further comprising contacting the cleaned aluminum component with water to produce a rinsed, cleaned aluminum component.

13. The method of claim 12 , further comprising contacting the rinsed, cleaned aluminum component with a conditioner to produce a passivated aluminum component.

14. The method of claim 13 , wherein the conditioner comprises water, a water soluble alkaline metal phosphate, and an azole compound.

15. The method of claim 13 , wherein the conditioner has a pH of 8.5 to 11 at room temperature.

16. The method of claim 8 , wherein the cleaning solution is filtered and recirculated for contact with the aluminum component.

17. A cleaner concentrate for a heat transfer system comprising:

greater than 15 weight percent of a freezing point depressant,

about 5 to 10 weight percent of oxalic acid, and

an azole compound,

wherein weight percent is based on the total weight of the cleaner concentrate,

wherein the cleaner concentrate is an uniform solution, and

wherein the solution is stable at about 10° F. to about 55° F.

Assignments (18)
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Sep 8, 2024
From: PRESTONE PRODUCTS LLC
To: GOLDMAN SACHS MIDDLE MARKET LENDING CORP. II
Reel/Frame 068892/0272 →
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Aug 15, 2024
From: PRESTONE PRODUCTS LLC
To: GOLDMAN SACHS MIDDLE MARKET LENDING CORP. II, AS COLLATERAL AGENT
Reel/Frame 068630/0147 →
RELEASE/TERMINATION OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jul 8, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; NC BRANDS, L.P.; PRESTONE PRODUCTS CORPORATION
Reel/Frame 068220/0306 →
RELEASE AND TERMINATION OF INTELLECTUAL PROPERTY SECURITY INTEREST Recorded Jul 8, 2024
From: BARCLAYS BANK PLC
To: AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS, INC.; KIK INTERNATIONAL, LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; NC BRANDS L.P.; CYGNUS CORPORATION
Reel/Frame 068220/0455 →
ENTITY CONVERSION Recorded Jun 25, 2024
From: PRESTONE PRODUCTS CORPORATION
To: PRESTONE PRODUCTS LLC
Reel/Frame 067826/0319 →
PARTIAL RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0634 →
PARTIAL RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0649 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0671 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0751 →
SECURITY AGREEMENT Recorded Dec 27, 2021
From: AQUA CLEAR INDUSTRIES, LLC; ASEPIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK INTERNATIONAL LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; CYGNUS CORPORATION; NC BRANDS L.P.
To: BARCLAYS BANK PLC
Reel/Frame 058592/0835 →
RELEASE OF INTELLECTUAL PROPERTY SECURITY INTEREST Recorded Jul 29, 2021
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; JAMES AUSTIN COMPANY; KIK INTERNATIONAL LLC; NC BRANDS L.P.; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC
Reel/Frame 057650/0125 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (NOTES) Recorded Dec 22, 2020
From: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; KIK INTERNATIONAL LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; JAMES AUSTIN COMPANY; CYGNUS CORPORATION; NC BRANDS L.P.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; HI-LEX LLC; HOMECARE LABS, INC.; SUNBELT POOL PRODUCTS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 055327/0754 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (2019) Recorded Jan 28, 2019
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; CBI LABORATORIES, INC.; CYGNUS CORPORATION; NC BRANDS L.P.
To: BARCLAYS BANK PLC, AS AGENT
Reel/Frame 048180/0101 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (ABL) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049518/0001 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (TERM LOAN) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049517/0967 →
RELEASE OF SECURITY INTEREST Recorded Sep 14, 2016
From: BARCLAYS BANK PLC
To: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC; PRESTONE PRODUCTS CORPORATION
Reel/Frame 040031/0793 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 5, 2016
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS, INC. (TEXAS); KIK CUSTOM PRODUCTS INC. (DELAWARE); KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 038354/0938 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 13, 2012
From: YANG, BO; WOYCIESJES, PETER M.
To: PRESTONE PRODUCTS COMPANY
Reel/Frame 028542/0172 →