IP Library Granted Patent US 10,071,184
Granted Patent B2
US 10,071,184 · App. 13/408,319 · Granted Sep 11, 2018

Collagen-coated tissue-based membranes

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Quick Facts
Patent No.
US 10,071,184
App. No.
13/408,319
Granted
Sep 11, 2018
Kind
B2
Abstract

A collagen-coated tissue-based membrane that is smooth on both sides so as to inhibit cell and tissue adhesion. The tissue-based membrane is a serous membrane having a fibrous surface and a smooth surface and the collagen is coated on the fibrous surface. Also provided are methods for making the collagen-coated tissue-based membrane.

Claims (19)

1. A tissue-based coated membrane, comprising a serous membrane and a type I collagen coating, wherein the serous membrane has a fibrous surface and a smooth surface, the type I collagen coating, having a thickness of 5 μm to 100 μm, is in contact with the fibrous surface, wherein the type I collagen coating is present as a single layer, the type I collagen-coated fibrous surface being smooth, and both the type I collagen-coated fibrous surface and the smooth surface adhere poorly to cells and tissues.

2. The tissue-based membrane of claim 1 , wherein the serous membrane is pericardium, peritoneum, amnion, small intestine submucosa, pleural, or vaginal tunics.

3. The tissue-based membrane of claim 1 , wherein the serous membrane is pericardium or peritoneum.

4. A biocompatible collagen-coated serous membrane prepared by the steps of:

scraping a fibrous side of a serous membrane to remove adhering fibers;

treating the serous membrane to remove cells, lipids, and extractable blood and non-collagenous molecules;

freeze-drying the treated serous membrane;

compressing the fibrous side of the serous membrane;

coating type I collagen onto the fibrous side of the serous membrane, thereby rendering the fibrous side of the serous membrane smooth, wherein the type I collagen is coated onto the fibrous side of the serous membrane in a single layer; and

exposing the type I collagen-coated serous membrane to a crosslinking agent to effect crosslinking,

wherein the type I collagen coating has a thickness of 5 μm to 100 μm.

5. A biocompatible collagen-coated serous membrane prepared by the steps of:

scraping a fibrous side of a serous membrane to remove adhering fibers;

treating the serous membrane to remove cells, lipids, and extractable blood and non-collagenous molecules;

freeze-drying the treated serous membrane;

compressing the fibrous side of the serous membrane;

spraying a collagen coat onto the fibrous side of the serous membrane, thereby rendering the fibrous side of the serous membrane smooth, wherein the collagen coat is sprayed onto the fibrous side of the serous membrane in a single layer; and

exposing the collagen-coated serous membrane to a crosslinking agent to effect crosslinking,

wherein the serous membrane is pericardium or peritoneum, the collagen coating has a thickness of 5 μm to 100 μm, and the collagen is type I collagen.

Assignments (12)
RELEASE OF SECURITY INTEREST Recorded Jan 26, 2026
From: GOLUB CAPITAL MARKETS LLC, AS ADMINISTRATIVE AGENT
To: COLLAGEN MATRIX, INC.
Reel/Frame 073583/0580 →
SECURITY INTEREST Recorded Jan 26, 2026
From: COLLAGEN MATRIX, INC.
To: GOLUB CAPITAL MARKETS LLC, AS COLLATERAL AGENT
Reel/Frame 073583/0614 →
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 049933/0378 Recorded Aug 1, 2024
From: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY
To: COLLAGEN MATRIX, INC.
Reel/Frame 068256/0450 →
SECURITY INTEREST Recorded Aug 1, 2019
From: COLLAGEN MATRIX, INC.
To: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY
Reel/Frame 049933/0378 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Aug 1, 2019
From: CAPITAL ONE, NATIONAL ASSOCIATION
To: COLLAGEN MATRIX, INC.
Reel/Frame 049934/0317 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Aug 1, 2019
From: COLLAGEN MATRIX, INC.
To: GOLUB CAPITAL, LLC
Reel/Frame 051594/0368 →
SECURITY INTEREST Recorded May 7, 2019
From: COLLAGEN MATRIX, INC.
To: CAPITAL ONE, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 049105/0505 →
SECURITY INTEREST Recorded Nov 6, 2018
From: COLLAGEN MATRIX, INC.
To: HEALTHCARE FINANCIAL SOLUTIONS, LLC, AS COLLATERAL AGENT
Reel/Frame 047418/0873 →
ASSIGNMENT OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Nov 14, 2015
From: GENERAL ELECTRIC CAPITAL CORPORATION, AS RETIRING AGENT
To: HEALTHCARE FINANCIAL SOLUTIONS, LLC, AS SUCCESSOR AGENT
Reel/Frame 037111/0808 →
SECURITY INTEREST Recorded Oct 23, 2014
From: COLLAGEN MATRIX, INC.
To: GENERAL ELECTRIC CAPITAL CORPORATION, AS COLLATERAL AGENT
Reel/Frame 034021/0474 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NAME OF ASSIGNEE PREVIOUSLY RECORDED ON REEL 027934 FRAME 0346. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Apr 6, 2012
From: LI, SHU-TUNG; YUEN, DEBBIE
To: COLLAGEN MATRIX, INC.
Reel/Frame 028003/0724 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 27, 2012
From: LI, SHU-TUNG; YUEN, DEBBIE
To: COLLAGEN MATRIX
Reel/Frame 027934/0346 →