IP Library Patent Application 13424680
Patent Application
App. No. 13/424,680

USE OF HIGH RATIO AQUEOUS ALKALI SILICATES FOR PROFILE MODIFICATION, WATER CONTROL AND STABILIZATION

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Quick Facts
Patent No.
US None
App. No.
13/424,680
Abstract

Soluble silicates are commonly used to block and strengthen permeable zones in subterranean formations. These applications include conformance for oil field, grouting for the construction industry and water shut-off for mining. It was discovered that set times and set properties could be improved by using novel, high ratio alkali silicates. Ratio being defined as the mol ratio of SiO 2 :Me 2 O, where Me is an alkali metal and is most commonly sodium or potassium (i.e. Na 2 O and K 2 O).

Claims (18)

1 . A conformance agent for use in managing water and gas flows comprising a high ratio aqueous alkali silicate wherein the molar ratio of silica oxide to alkali oxide is greater than 4.0 and less than 12.0

2 . The conformance agent of claim 1 wherein the molar ratio of silica oxide to alkali oxide is greater than 4.5.

3 . The conformance agent of claim 1 wherein the alkali oxide is sodium oxide.

4 . The conformance agent of claim 1 wherein the silica oxide is potassium oxide.

5 . The conformance agent of claim 1 further comprising a setting agent.

6 . The conformance agent of claim 5 wherein the setting agent is one of sodium acid pyrophosphate and citric acid.

7 . A water shut off agent comprising a high ratio alkali silicate wherein the molar ratio of silica oxide to alkali oxide is greater than 4.0.

8 . The water shut off agent of claim 7 wherein the molar ratio of silica oxide to alkali oxide is greater than 4.5.

9 . The water shut off agent of claim 7 wherein the alkali oxide is sodium oxide.

10 . The water shut off agent of claim 7 wherein the silica oxide is potassium oxide.

11 . The water shut off agent of claim 7 further comprising a setting agent.

12 . The water shut off agent of claim 11 wherein the setting agent is one of sodium acid pyrophosphate and citric acid.

13 . A grouting agent comprising a high ratio alkali silicate wherein the molar ratio of silica oxide to alkali oxide is greater than 4.0.

14 . The grouting agent of claim 13 wherein the molar ratio of silica oxide to alkali oxide is greater than 4.5.

15 . The grouting agent of claim 13 wherein the alkali oxide is sodium oxide.

16 . The grouting agent of claim 13 wherein the silica oxide is potassium oxide.

17 . The grouting agent of claim 13 further comprising a setting agent.

18 . The grouting agent of claim 17 wherein the setting agent is one of sodium acid pyrophosphate and citric acid.

Assignments (9)
RELEASE OF SECURITY INTEREST Recorded May 5, 2016
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS ADMINISTRATIVE AGENT
To: PQ CORPORATION; POTTERS INDUSTRIES, LLC
Reel/Frame 038612/0222 →
RELEASE OF SECURITY INTEREST Recorded May 4, 2016
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: PQ CORPORATION; POTTERS INDUSTRIES, LLC
Reel/Frame 038611/0927 →
SECURITY AGREEMENT Recorded Nov 30, 2012
From: PQ CORPORATION; POTTERS INDUSTRIES, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 029377/0878 →
SECURITY AGREEMENT Recorded Nov 29, 2012
From: PQ CORPORATION; POTTERS INDUSTRIES, LLC
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS ADMINISTRATIVE AGENT
Reel/Frame 029370/0103 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Nov 26, 2012
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: PQ CORPORATION
Reel/Frame 029349/0592 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Nov 26, 2012
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: PQ CORPORATION
Reel/Frame 029349/0556 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2012
From: MCDONALD, MICHAEL J.
To: PQ CORPORATION
Reel/Frame 028148/0833 →
FIRST LIEN GRANT OF SECURITY INTEREST IN PATENTS AMENDMENT NO. 1 Recorded Apr 3, 2012
From: PQ CORPORATION
To: CREDIT SUISSE AG, AS SUCCESSOR AGENT
Reel/Frame 027980/0194 →
SECOND LIEN GRANT OF SECURITY INTEREST IN PATENTS AMENDMENT NO. 1 Recorded Apr 3, 2012
From: PQ CORPORATION
To: CREDIT SUISSE AG, AS SUCCESSOR AGENT
Reel/Frame 027980/0219 →