IP Library Granted Patent US 8,992,964
Granted Patent B2
US 8,992,964 · App. 13/453,818 · Granted Mar 31, 2015

Process for demineralization of bone matrix with preservation of natural growth factors

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Quick Facts
Patent No.
US 8,992,964
App. No.
13/453,818
Granted
Mar 31, 2015
Kind
B2
Abstract

A demineralized bone matrix is produced by a process in which a bone body is placed in a first processing solution comprising an acid to demineralize the bone body. The bone body is periodically removed from the first solution at specific time intervals to perform at least one test, such as a compression test, on a mechanical property of the bone body. When the test yields a desired result, the bone body is exposed to a second processing solution that is less acidic than the first, thus minimizing the exposure of the bone body to the harsh acidic conditions of the demineralization phase of the process.

Claims (17)

1. A demineralized bone matrix having greater than about 5000 pg/g of bone morphogenetic protein-2 (BMP-2), wherein the matrix contains less than 2 percent residual calcium, wherein at least one dimension of the matrix is at least 2 mm, wherein the matrix is compressible to 5 to 60 percent of an original shape of the matrix when between 10 and 1000 grams-force/cm 2 of force is applied to the matrix and wherein the matrix is a sponge-like bone graft matrix.

2. The demineralized bone matrix of claim 1 , wherein the matrix is infiltrated with stem cells.

3. The demineralized bone matrix of claim 1 , wherein the matrix is coated with stem cells.

4. The demineralized bone matrix of claim 1 , wherein the matrix is a single piece.

5. The demineralized bone matrix of claim 1 , wherein the bone matrix comprises an open porous structure.

6. The demineralized bone matrix of claim 1 , wherein the bone matrix is not in a carrier.

7. The demineralized bone matrix of claim 1 , further comprising a secondary material selected from the group consisting of bone void filler, a metal, a plastic and a composite.

8. The demineralized bone matrix of claim 1 , wherein the matrix is reversibly deformable.

9. The demineralized bone matrix of claim 1 , wherein a structure of the matrix will not dissolve with irrigation.

10. The demineralized bone matrix of claim 1 , wherein the matrix is osteoinductive.

11. The demineralized bone matrix of claim 1 , wherein the matrix is osteoconductive.

12. The demineralized bone matrix of claim 1 , wherein the matrix is osteogenic.

13. The demineralized bone matrix of claim 1 , wherein the matrix has bone properties selected from the group consisting of osteoinductive, osteoconductive, osteogenic, and combinations thereof.

14. The demineralized bone matrix of claim 1 , wherein the matrix provides scaffolding.

15. The demineralized bone matrix of claim 1 , wherein the matrix is three dimensional.

16. The demineralized bone matrix of claim 1 , wherein the matrix is in a shape of a dowel.

17. The demineralized bone matrix of claim 1 , wherein the matrix is in the shape of a cylinder.

Assignments (12)
SECURITY INTEREST Recorded Aug 11, 2024
From: XTANT MEDICAL, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.; SURGALIGN SPV, INC.; XTANT MEDICAL HOLDINGS, INC.
To: MIDCAP FUNDING IV TRUST
Reel/Frame 068539/0492 →
SECURITY INTEREST Recorded Aug 11, 2024
From: XTANT MEDICAL, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.; SURGALIGN SPV, INC.; XTANT MEDICAL HOLDINGS, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 068539/0665 →
RELEASE OF SECURITY INTEREST Recorded Jun 18, 2021
From: ROS ACQUISITION OFFSHORE LP
To: BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
Reel/Frame 056627/0795 →
RELEASE OF SECURITY INTEREST Recorded Jun 4, 2021
From: SILICON VALLEY BANK
To: XTANT MEDICAL, INC.; XTANT MEDICAL HOLDINGS, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
Reel/Frame 056493/0457 →
SECURITY INTEREST (REVOLVING) Recorded May 21, 2021
From: XTANT MEDICAL HOLDINGS, INC.; XTANT MEDICAL, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 056323/0536 →
SECURITY INTEREST (TERM) Recorded May 21, 2021
From: XTANT MEDICAL HOLDINGS, INC.; XTANT MEDICAL, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 056323/0586 →
RELEASE OF SECURITY INTEREST Recorded May 20, 2021
From: ROS ACQUISITION OFFSHORE LP
To: BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
Reel/Frame 056323/0218 →
SECURITY AGREEMENT Recorded Jun 6, 2016
From: XTANT MEDICAL HOLDINGS, INC.; BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.; XTANT MEDICAL, INC.
To: SILICON VALLEY BANK
Reel/Frame 038884/0063 →
RELEASE OF SECURITY INTEREST Recorded Aug 3, 2015
From: ROS ACQUISITION OFFSHORE LP
To: BACTERIN INTERNATIONAL, INC.
Reel/Frame 036234/0711 →
SECURITY INTEREST Recorded Aug 3, 2015
From: BACTERIN INTERNATIONAL, INC.; X-SPINE SYSTEMS, INC.
To: ROS ACQUISITION OFFSHORE, LP
Reel/Frame 036252/0338 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 29, 2014
From: SHELBY, NANCY J.; SCOTT, STEVEN M.; LUCHSINGER, BENJAMIN P.; JUDA, GREGORY A.; KIRKER, KELLY R.; HERNANDEZ, JESUS; HOLMES, DARREL L.
To: BACTERIN INTERNATIONAL, INC.
Reel/Frame 033410/0020 →
SECURITY AGREEMENT Recorded Aug 28, 2012
From: BACTERIN INTERNATIONAL, INC.
To: ROS ACQUISITION OFFSHORE LP
Reel/Frame 028859/0395 →