Method and apparatus for making vacuum insulated glass (VIG) window unit including pump-out tube sealing technique
View Patent ↗A method for making a vacuum insulated glass window assembly is provided in which an exposed end of a pump-out tube of a vacuum insulated glass window assembly is sealed using a laser that is applied to the end of the pump out tube in controlled sequential manner as opposed to a short duration, high-powered application of a laser. In particular, a method is disclosed in which a multiphase sequential variable power application of laser energy to an exposed end of a pump-out tube for controlled exposure times and decreasing laser trace diameters produces a more controlled melting of the tube glass to reduce or eliminate undesirable outgassing that may occur during a high-power short duration exposure of laser energy to the end of the pump-out tube to seal the tube.
1. A method of making a vacuum insulated glass window unit, the method comprising:
having a first substrate with a pump-out tube disposed in a hole formed in the first substrate; a second substrate; and an edge seal, the first and second substrates arranged to sandwich the edge seal and form a cavity therebetween;
sealing an end of the pump-out tube extending out of the first substrate, the sealing comprising: (i) performing at least one preheating treatment at a top of the pump-out tube and to begin heating the top of the pump-out tube; (ii) after said pre-heating, performing at least one core heating treatment to melt the top of the pump-out tube; and (iii) performing a plurality of chase treatments using successively reduced laser trace diameters to seal the pump-out tube.
2. The method of claim 1 , further comprising evacuating the cavity between the first substrate and a second substrate to a pressure less than atmospheric pressure using the pump-out tube prior to said sealing.
3. The method of claim 1 , wherein the sealing steps (i), (ii) and (iii) are performed using a laser.
4. The method of claim 1 , wherein the sealing steps (i), (ii) and (iii) are performed with a YAG laser.
5. The method of claim 1 , wherein the preheating treatment comprises applying a laser beam in a generally circular trace having a diameter of about 0.135 mm for about 8 to 12 repetitions and at a power of from about 14-18 W;
said core treatment comprises applying the laser with a trace diameter of about 0.135 mm for about 60-80 repetitions and at a power of form about 10-14 W; and
said plurality of chase treatments comprise: a first chase treatment applying the laser with a trace diameter of from about 0.10 to 0.14 mm for about 25-35 repetitions at a power of about 10-14 W; a second chase treatment applying the laser with a trace diameter of about 0.05 to 0.2 mm for about 10-30 repetitions at a power of from about 8-12 W; and a third chase treatment applying the laser with a trace diameter of from about 0.06 to 0.1 mm for about 3-10 repetitions at a power of from about 8-12 W.
6. The method of claim 5 , wherein a laser movement speed is about 25 inches/sec.
7. The method of claim 1 , wherein the preheating treatment comprises: a first preheating treatment applying the laser in a generally circular trace having a diameter of about 0.1 to 0.2 mm, for about 75-125 repetitions at a power of from about 6-10 W; and a second preheating treatment applying the laser with a smaller trace diameter of from about 0.08 to 0.150, for about 4-10 repetitions at a power of from about 14-18 W;
said core treatment comprises: applying the laser with a trace diameter of from about 0.1 to 0.2, for about 20-60 repetitions at a power of from about 10-14 W; and
said plurality of chase treatments comprise: a first chase treatment applying the laser with a trace diameter of from about 0.1 to 0.2 mm, for about 10-30 repetitions at a power of from about 8-12 W; a second chase treatment applying the laser with a smaller trace diameter of from about 0.08-0.15, for about 5-15 repetitions at a power of about from about 6-10 W; and a third chase treatment applying the laser with a still smaller trace diameter of from about 0.05 to 0.09 mm, for about 3-10 repetitions at a power of about 4-8 W.
8. The method of claim 7 , wherein a laser movement speed is about 25 inches/sec.
9. The method of claim 1 , wherein the preheating treatment comprises: applying the laser in a generally circular trace having a diameter of about 0.135 mm for about 200 repetitions at a power of about 6 W;
said core treatment comprises: applying the laser with a trace diameter of about 0.135 mm for about 90 repetitions at a power of about 10 W; and
said plurality of chase treatments comprise: a first chase treatment applying the laser with a trace diameter of about 0.12 mm for about 20 repetitions at a power of about 8 W; a second chase treatment applying the laser with a trace diameter of about 0.1 mm for about 10 repetitions at a power of about 7 W; and a third chase treatment applying the laser with a trace diameter of about 0.08 mm for about 5 repetitions at a power of about 6 W.
10. The method of claim 9 , wherein a laser movement speed is about 25 inches/sec.
11. The method of claim 1 , wherein the preheating treatment comprises: applying the laser in a generally circular trace having a diameter of about 0.135 mm for about 200 repetitions at a power of about 6 W;
said core treatment comprises: applying the laser with a trace diameter of about 0.135 mm for about 70 repetitions at a power of about 12 W; and
said plurality of chase treatments comprise: a first chase treatment applying the laser with a trace diameter of about 0.12 mm for about 20 repetitions at a power of about 8 W; a second chase treatment applying the laser with a trace diameter of about 0.1 mm for about 10 repetitions at a power of about 7 W; and a third chase treatment applying the laser with a trace diameter of about 0.08 mm for about 5 repetitions at a power of about 6 W.
12. The method of claim 11 , wherein a laser movement speed is about 25 inches/sec.
13. A method of making a vacuum insulated glass window unit, the method comprising:
sealing an end of a pump-out tube extending out of a first substrate of the vacuum insulated glass window unit, the sealing comprising:
performing at least one preheating treatment;
performing at least one core heating treatment; and
performing a plurality of chase treatments using successively reduced laser trace diameters.
14. The method of claim 13 , further comprising evacuating a cavity formed between the first substrate and a second substrate of the vacuum insulated glass window unit to a pressure less than atmospheric pressure via the pump-out tube prior to the sealing.
15. The method of claim 13 , wherein the sealing is performed using a laser.
16. The method of claim 13 , wherein the sealing is performed using a 20 W YAG laser.
17. The method of claim 13 , wherein said preheating treatment cleans a top of the pump-out tube and begins heating the top of the pump-out tube.
18. The method of claim 13 , wherein said core treatment begins melting of a top of the pump-out tube.
19. The method of claim 13 , wherein the chase treatments seal the end of the pump-out tube.
20. The method of claim 13 , wherein the pump-out tube is not melted during the preheating treatment.