IP Library Granted Patent US 8,791,154
Granted Patent B2
US 8,791,154 · App. 13/475,607 · Granted Jul 29, 2014

High concentration olopatadine ophthalmic composition

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Quick Facts
Patent No.
US 8,791,154
App. No.
13/475,607
Granted
Jul 29, 2014
Kind
B2
Abstract

The present invention is an ophthalmic composition containing a relatively high concentration of olopatadine. The composition is typically an ophthalmic aqueous solution containing relatively high concentrations of olopatadine solubilized within the solution. The composition is preferably capable of providing enhanced relief from symptoms of ocular allergic conjunctivitis, particularly late phase symptoms of ocular allergic conjunctivitis.

Claims (57)

1. An aqueous ophthalmic solution for treatment of ocular allergic conjunctivitis, the solution comprising:

at least 0.67 w/v % olopatadine dissolved in the solution;

PEG having a molecular weight of 300 to 500;

polyvinylpyrrolidone;

hydroxypropyl-γ-cyclodextrin;

benzalkonium chloride; and

water.

2. A solution as in claim 1 further comprising borate.

3. A solution as in claim 2 further comprising a polyol.

4. An aqueous ophthalmic solution for treatment of ocular allergic conjunctivitis, the solution comprising:

at least 0.67 w/v % but no greater than 1.0 w/v % olopatadine dissolved in the solution;

2.0 w/v % to 6.0 w/v % PEG having a molecular weight of 300 to 500;

2.0 w/v % to 6.0 w/v % polyvinylpyrrolidone;

at least 0.5 w/v % but no greater than 2.0 w/v % cyclodextrin derivative selected from the group consisting of SAE-β-cyclodextrin, HP-γ-cyclodextrin, HP-β-cyclodextrin and combinations thereof; and

water.

5. A solution as in claim 4 further comprising borate at a concentration of at least 0.18 w/v % but less than 0.5 w/v %.

6. A solution as in claim 5 further comprising a polyol.

7. A solution as in claim 6 wherein the polyol is propylene glycol at a concentration of at least 0.4 w/v % but no greater than 2.2 w/v %.

8. An aqueous ophthalmic solution for treatment of ocular allergic conjunctivitis, the solution comprising:

at least 0.67 w/v % but no greater than 1.0 w/v % olopatadine dissolved in the solution;

2.0 w/v % to 6.0 w/v % PEG having a molecular weight of 300 to 500;

2.0 w/v % to 6.0 w/v % polyvinylpyrrolidone;

at least 0.5 w/v % but no greater than 2.0 w/v % hydroxypropyl-γ-cyclodextrin; and

water.

9. A solution as in claim 8 further comprising borate at a concentration of at least 0.18 w/v % but less than 0.5 w/v %.

10. A solution as in claim 9 further comprising a polyol.

11. A solution as in claim 10 wherein the polyol is propylene glycol at a concentration of at least 0.4 w/v % but no greater than 2.2 w/v %.

12. A method of treating at least one ocular allergy symptom in humans, the method comprising:

topically applying to an eye of a human an amount of the solution of claim 4 sufficient to treat the at least one ocular allergy symptom.

13. A method as in claim 12 wherein the step of topically applying the solution includes dispensing at least one drop of the solution to the eye.

14. A method as in claim 13 wherein the at least one ocular allergy symptom includes ocular itching.

15. A solution as in claim 1 further comprising hydroxypropylmethyl cellulose.

16. A solution as in claim 4 further comprising at least 0.15 w/v % but no greater than 1.0 w/v % hydroxypropylmethyl cellulose.

17. A solution as in claim 8 further comprising at least 0.15 w/v % but no greater than 1.0 w/v % hydroxypropylmethyl cellulose.

18. A solution as in claim 3 wherein the polyol is mannitol.

19. A solution as in claim 6 wherein the polyol is mannitol solution at a concentration that is at least 0.05 w/v % but no greater than 0.5 w/v %.

20. A solution as in claim 10 wherein the polyol is mannitol at a concentration that is at least 0.05 w/v % but no greater than 0.5 w/v %.

21. An aqueous ophthalmic solution for treatment of ocular allergic conjunctivitis, the solution comprising:

at least 0.67 w/v % but no greater than 1.0 w/v % olopatadine dissolved in the solution;

2.0 w/v % to 6.0 w/v % PEG having a molecular weight of 300 to 500;

2.0 w/v % to 6.0 w/v % polyvinylpyrrolidone;

at least 0.5 w/v % but no greater than 2.0 w/v % hydroxypropyl-γ-cyclodextrin;

greater than 0.003 w/v % but less than 0.03 w/v % benzalkonium chloride; and

water;

wherein the pH of the solution is 6.0 to 7.8 and the osmolality of the solution is 200 to 400 mOsm/kg.

22. A solution as in claim 21 further comprising at least 0.15 w/v % but no greater than 1.0 w/v % hydroxypropylmethyl cellulose.

23. A solution as in claim 22 wherein:

i) the concentration of PEG is at least 3.0 w/v % but no greater than 5.0 w/v %;

ii) the concentration of polyvinylpyrrolidone is at least 3.0 w/v % but no greater than 5.0 w/v %; and

iii) the concentration of hydroxypropyl methylcellulose is at least 0.3 w/v % but no greater than 0.5 w/v %.

24. A solution as in claim 23 further comprising:

at least 0.18 w/v % but less than 0.4 w/v % boric acid; and

at least 0.05 w/v % but no greater than 0.5 w/v % mannitol.

25. A method of treating ocular allergy symptoms in humans, the method comprising:

topically applying to an eye of a human an amount of the solution of claim 23 sufficient to treat ocular allergy symptoms.

26. A method as in claim 25 wherein the step of topically applying the solution includes dispensing at least one drop of the solution to the eye.

27. A method as in claim 26 wherein the ocular allergy symptoms include ocular itching.

Assignments (5)
CONFIRMATORY DEED OF ASSIGNMENT EFFECTIVE DECEMBER 1, 2020 Recorded Dec 3, 2020
From: NOVARTIS AG
To: ALCON INC.
Reel/Frame 054585/0626 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS. PREVIOUSLY RECORDED AT REEL: 050746 FRAME: 0431. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT.. Recorded Oct 18, 2019
From: ALCON RESEARCH, LLC
To: NOVARTIS AG
Reel/Frame 050767/0001 →
CONFIRMATORY DEED OF ASSIGNMENT EFFECTIVE APRIL 8, 2019 Recorded Oct 17, 2019
From: ALCON RESEARCH, LLC
To: NOVARTIS AG
Reel/Frame 050746/0431 →
MERGER Recorded Oct 16, 2019
From: ALCON RESEARCH, LTD.
To: ALCON RESEARCH, LLC
Reel/Frame 050735/0465 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 26, 2012
From: GAMACHE, DANIEL A.; ALANI, LAMAN; GHOSH, MALAY; GALAN, FRANCISCO JAVIER; PERDIGUER, NURIA CARRERAS; SINGH, ONKAR N.
To: ALCON RESEARCH, LTD.
Reel/Frame 028446/0052 →