Method for extracting rare earth material from monazite
A method for extracting rare earth elements from monazite is disclosed. The method includes milling a mixture of monazite including phosphates and rare earth elements and sodium hydroxides inside a mill containing a plurality of balls to form powder by colliding the mixture into balls with each other, converting the mixture into rare earth hydroxides and sodium phosphates through the reaction occurring in the process of repeated collision, and extracting rare earth elements from the powder.
1. A method for extracting rare earth elements in monazite comprising:
separating the monazite from sand, wherein separating is achieved by physical separation methods selected from the group consisting of gravity concentration, electrostatic separation, and magnetic separation;
milling a mixture of the monazite and sodium hydroxide in a mill to convert the mixture into a powder that comprise rare earth hydroxides and sodium phosphates;
solubilizing the sodium phosphates into water and allowing the rare earth hydroxides to remain as a water insoluble components in the powder;
filtering the powder;
drying the powder; and
extracting the rare earth element from the powder with sulfuric acid to leach the rare earth elements from the powder.
2. The method of claim 1 , wherein the chemically separating the sodium phosphates away from the rare earth hydroxides in the milled particles eliminates more than 90% of phosphates in the monazite.
3. The method of claim 1 , wherein the sand comprises sea sand.
4. The method of claim 1 , wherein the milling is continuously maintained for 100 minutes through 140 minutes.
5. The method of claim 1 , wherein the water is distilled water.
6. The method of claim 1 , wherein the physical separation method comprises gravity concentration.
7. The method of claim 1 , wherein the physical separation method comprises electrostatic separation.
8. The method of claim 1 , wherein the physical separation method comprises magnetic separation.
9. The method of claim 1 , wherein the sulfuric acid is at a concentration between about 0.05 N and about 5 N.
10. The method of claim 1 , wherein milling the mixture results in a peak temperature of between about 60° C. to about 200° C.
11. The method of claim 1 , wherein the mill comprises a planetary ball mill.