IP Library Granted Patent US 10,004,245
Granted Patent B2
US 10,004,245 · App. 13/509,552 · Granted Jun 26, 2018

Granulation of a stevia sweetener

Inventors: Siddhartha Purkayastha (London, GB); Avetik Markosyan (Yerevan, AM)
Assignee: PureCircle Sdn Bhd
A23C9/1307A23G3/36A23G3/48A23G9/32A23G9/42A23L27/36A23P10/25A23V2002/00
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Quick Facts
Patent No.
US 10,004,245
App. No.
13/509,552
Granted
Jun 26, 2018
Kind
B2
Abstract

A method for making a granulated Stevia sweetener is described. The resulting sweetener has a desirably high solubility level.

Claims (17)

1. A method for producing a sweetener comprising the steps of:

A) providing a Stevia sweetener powder;

B) reducing the particle size of the Stevia sweetener powder to a particle size of between about 20 to 60 μm;

C) treating the Stevia sweetener powder under reduced pressure of between about 0 mbar to 100 mbar and an elevated temperature of between about 90-130° C.;

D) cooling down the treated Stevia sweetener powder to a low temperature of about 25° C.; and

E) holding the cooled Stevia sweetener powder at the low temperature to obtain a high solubility Stevia sweetener powder with an increased solubility of at least about 30 g per 100 g of water; and

F) introducing the high solubility Stevia sweetener powder to a roll compaction apparatus to produce a compacted material; introducing the compacted material to a size reducing apparatus to obtain a granule mixture; and fractionating the granule mixture through a top screen having a screen size of US Mesh 10 and a bottom screen having a screen size of US Mesh 40, to obtain a granulated Stevia sweetener having a dissolution rate greater than a dissolution rate of the high solubility Stevia powder.

2. The method of claim 1 , wherein the dissolution rate of the granulated Stevia sweetener is at least about 0.75 grams per minute.

3. The method of claim 1 wherein Stevia sweetener is selected from a group consisting of: Stevioside, Rebaudioside A, Rebaudioside B, Rebaudioside C, Rebaudioside D Rebaudioside E, Rebaudioside F, Steviolbioside, Dulcoside A, Rubusoside, and a mixture thereof.

4. The method of claim 1 , wherein cooling the treated Stevia powder comprises introducing preheated nitrogen gas into a vacuum chamber and gradually reducing the nitrogen gas temperature.

5. The method of claim 1 , wherein the roll compaction apparatus operates at between about 5 rpm and about 20 rpm, and at a roll pressure of between about 10 bar to about 60 bar to produce the compacted material; and the size reducing apparatus comprises a set of sequentially located granulators equipped with rotors rotating at between about 50 rpm to about 2000 rpm to obtain the granule mixture.

6. The method of claim 1 wherein the Stevia sweetener powder is selected from a group consisting of: Stevioside, Rebaudioside A, Rebaudioside B, Rebaudioside C, Rebaudioside D, Rebaudioside E, Rebaudioside F, Steviolbioside, Dulcoside A, Rubusoside, and a mixture thereof.

7. The method of claim 1 , further comprising the step of combining the Stevia sweetener powder with an additional ingredient before introducing the powder to the roll compaction apparatus.

8. The method of claim 7 , wherein the additional ingredient is selected from the group consisting of: a high intensity sweetener; a natural sweetener; a sugar alcohol; a flavoring agent; a flavor modifying agent; a taste modifying agent; a bulking agent; and a combination thereof.

9. The method of claim 5 , wherein the granulators comprise U-shaped screens having opening sizes ranging from about 0.5 mm to about 6.0 mm.

10. The method of claim 5 , comprising a first granulator and a second granulator, said first granulator being equipped with a U-shaped screen having an opening size of about 3.1 mm and said second granulator being equipped with a U-shaped screen having an opening size of about 1.6 mm.

11. The method of claim 1 , wherein the dissolution rate of the granulated Stevia sweetener is at least 8.6% greater than the dissolution rate of the high solubility Stevia powder.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 8277948 PREVIOUSLY RECORDED AT REEL: 036178 FRAME: 0102. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jul 29, 2015
From: PURECIRCLE USA/PURECIRCLE USA, INC.
To: PURECIRCLE SDN BHD
Reel/Frame 036206/0070 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 24, 2015
From: PURECIRCLE USA/PURECIRCLE USA, INC.
To: PURECIRCLE SDN BHD
Reel/Frame 036178/0102 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 29, 2013
From: PURKAYASTHA, SIDDHARTHA; MARKOSYAN, AVETIK
To: PURECIRCLE USA INC.
Reel/Frame 030304/0663 →
Continuity (6)
Continuation In Part 12720888 · Mar 10, 2010
Continuation In Part 12753470 · Apr 2, 2010
Provisional Application 61260465 · Nov 12, 2009
Provisional Application 61260593 · Nov 12, 2009
Provisional Application 61290778 · Dec 29, 2009
Related Publication 20120282389A1 · Nov 8, 2012
Cited By (2)
US 12,193,460 US 12,514,274