IP Library Granted Patent US 8,907,080
Granted Patent B2
US 8,907,080 · App. 13/511,253 · Granted Dec 9, 2014

Process for imparting water solubility or water dispersibility to hydrophobic cluster compound

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Quick Facts
Patent No.
US 8,907,080
App. No.
13/511,253
Granted
Dec 9, 2014
Kind
B2
Abstract

Provided is a complex comprising a hydrophobic cluster compound and a β-1,3-1,6-D-glucan having a degree of branching (a ratio of β-1,6 linkages to β-1,3 linkages) of 50 to 100%.

Claims (15)

1. A complex comprising

a hydrophobic cluster compound selected from the group consisting of a carborane, a fullerene, a carbon nanotube, a carbon nanocoil, and a microparticle, wherein the microparticle is an aggregation of at least one kind of metal atom selected from the group consisting of platinum, gold, silver, copper, titanium, zinc, iron, cobalt, magnesium, aluminum, and zirconium, and

a β-1,3-1,6-D-glucan having a degree of branching (a ratio of β-1,6 linkages to β-1,3 linkages) of 85 to 100%.

2. The complex according to claim 1 , wherein the β-1,3-1,6-D-glucan was produced by Aureobasidium pullulans.

3. The complex according to claim 1 , wherein the β-1,3-1,6-D-glucan was subjected to alkali treatment at a pH of 12 or higher followed by neutralization.

4. A production process for a complex comprising a hydrophobic cluster compound and a β-1,3-1,6-D-glucan, the process comprising the steps of

agitating a hydrophobic cluster compound selected from the group consisting of a carborane, a fullerene, a carbon nanotube, a carbon nanocoil, and a microparticle, wherein the microparticle is an aggregation of at least one kind of metal atom selected from the group consisting of platinum, gold, silver, copper, titanium, zinc, iron, cobalt, magnesium, aluminum, and zirconium, with a β-1,3-1,6-D-glucan having a degree of branching (a ratio of β-1,6 linkages to β-1,3 linkages) of 50 to 100% while maintaining the solid state, and

agitating the mixture with added water.

5. A production process for a complex comprising a hydrophobic cluster compound and a β-1,3-1,6-D-glucan, the process comprising the steps of

mixing, in a polar solvent, a hydrophobic cluster compound selected from the group consisting of a carborane, a fullerene, a carbon nanotube, a carbon nanocoil, and a microparticle, wherein the microparticle is an aggregation of at least one kind of metal atom selected from the group consisting of platinum, gold, silver, copper, titanium, zinc, iron, cobalt, magnesium, aluminum, and zirconium, and a β-1,3-1,6-D-glucan having a degree of branching (a ratio of β-1,6 linkages to β-1,3 linkages) of 50 to 100%, and

adding water to the obtained mixture and allowing the mixture to ripen.

6. The production process according to claim 4 , wherein the β-1,3-1,6-D-glucan was produced by Aureobasidium pullulans.

7. The production process according to claim 4 , wherein the β-1,3-1,6-D-glucan was subjected to alkali treatment at a pH of 12 or higher followed by neutralization.

8. The production process according to claim 5 , wherein the β-1,3-1,6-D-glucan was produced by Aureobasidium pullulans.

9. The production process according to claim 5 , wherein the β-1,3-1,6-D-glucan was subjected to alkali treatment at a pH of 12 or higher followed by neutralization.

Assignments (2)
CHANGE OF NAME Recorded May 18, 2016
From: DAISO CO., LTD.
To: OSAKA SODA CO., LTD.
Reel/Frame 038742/0210 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 29, 2012
From: SUZUKI, TOSHIO; UEDA, HIDEAKI; NAGASAKI, TAKESHI; KIRIHATA, MITSUNORI; NUMATA, MUNENORI; IKEDA, ATSUSHI
To: DAISO CO., LTD.; OSAKA CITY UNIVERSITY; OSAKA PREFECTURE UNIVERSITY PUBLIC CORPORATION; KYOTO PREFECTURAL PUBLIC UNIVERSITY CORPORATION; NATIONAL UNIVERSITY CORPORATION NARA INSTITUTE OF SCIENCE AND TECHNOLOGY
Reel/Frame 028468/0095 →