IP Library Granted Patent US 9,814,744
Granted Patent B2
US 9,814,744 · App. 13/515,661 · Granted Nov 14, 2017

Decellularized adipose cell growth scaffold

Inventors: Stephen F. Badylak (Pittsburgh, PA); Bryan N. Brown (Pittsburgh, PA); John M. Freund (Pittsburgh, PA); J. Peter Rubin (Pittsburgh, PA)
Assignee: University of Pittsburg—Of the Commonwealth System of Higher Education
A61K35/35A61L26/0057A61L26/0076A61L27/3804A61L27/60C07K14/78C12N5/0068C12N5/0667C12N2533/90
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Quick Facts
Patent No.
US 9,814,744
App. No.
13/515,661
Granted
Nov 14, 2017
Kind
B2
Abstract

Provided herein are methods of making a cell growth scaffold from adipose tissue, cell growth scaffolds having low lipid content and methods of using the cell growth scaffold.

Claims (25)

1. A method of preparing an adipose tissue-derived cell growth scaffold comprising, in order: digesting an adipose tissue sample with a proteinase and a chelating agent; washing the adipose tissue sample with an emulsifier; disinfecting the adipose tissue sample; depyrogenating the adipose tissue sample; drying the adipose tissue sample; and washing the adipose tissue sample with n-propanol, isopropanol or a mixture thereof.

2. The method of claim 1 , wherein the method comprises the following steps, in order:

a. rinsing an adipose tissue sample;

b. mechanically massaging the adipose tissue sample;

c. digesting the adipose tissue sample with a proteinase and a chelating agent;

d. rinsing the adipose tissue sample;

e. mechanically massaging the tissue sample;

f. washing the adipose tissue sample with a surfactant while the adipose tissue sample is agitated;

g. rinsing the adipose tissue sample;

h. washing the adipose tissue sample with an emulsifier;

i. rinsing the adipose tissue sample;

j. disinfecting the adipose tissue sample;

k. depyrogenating the adipose tissue sample;

l. rinsing the adipose tissue sample;

m. drying the adipose tissue sample;

n. washing the dried adipose tissue sample in n-propanol, isopropanol or a mixture thereof;

o. washing the adipose tissue sample in an aqueous solvent; and

p. drying the adipose tissue sample.

3. The method of claim 2 , in which in step m. the sample is dried by lyophilization.

4. The method of claim 2 , in which step p. drying the sample comprises lyophilizing the sample.

5. The method of claim 2 , further comprising step q. comminuting the sample to produce a powder.

6. The method of claim 5 , wherein the powder has a maximum size of 250 μM.

7. The method of claim 1 , in which the adipose tissue sample is washed with n-propanol.

8. The method of claim 1 , in which the adipose tissue sample is washed with isopropanol.

9. The method of claim 1 , further comprising after washing the adipose tissue sample with n-propanol, isopropanol or a mixture thereof, placing the adipose tissue sample in a covering prepared from one or more sheets of ECM material.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 10, 2013
From: BADYLAK, STEPHEN F.; BROWN, BRYAN N.; FREUND, JOHN M.; RUBIN, JOHN PETER
To: UNIVERSITY OF PITTSBURGH-OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
Reel/Frame 029604/0647 →
Continuity (2)
Provisional Application 61289082 · Dec 22, 2009
Related Publication 20130202563A1 · Aug 8, 2013