Method for producing a template for epitaxial growth having a sapphire (0001) substrate, an initial-stage A1N layer and laterally overgrown A1XGAYN (0001) layer
View Patent ↗A surface of a sapphire (0001) substrate is processed to form recesses and protrusions so that protrusion tops are flat and a given plane-view pattern is provided. An initial-stage AlN layer is grown on the surface of the sapphire (0001) substrate having recesses and protrusions by performing a C+ orientation control so that a C+ oriented AlN layer is grown on flat surfaces of the protrusion tops, excluding edges, in such a thickness that the recesses are not completely filled and the openings of the recesses are not closed. An Al x Ga y N(0001) layer (1≧x>0, x+y=1) is epitaxially grown on the initial-stage AlN layer by a lateral overgrowth method. The recesses are covered with the Al x Ga y N(0001) layer laterally overgrown from above the protrusion tops. Thus, an template for epitaxial growth having a fine and flat surface and a reduced threading dislocation density is produced.
1. A method for producing a template for epitaxial growth, comprising:
processing a surface of a sapphire (0001) substrate to form recesses and protrusions on the surface so that protrusion tops are made flat with a given plan-view pattern;
epitaxially growing an initial-stage AlN layer at a growth temperature higher than a crystallization temperature of AlN on the surface of the sapphire (0001) substrate having the recesses and protrusions by performing C axis orientation control so that a C+ axis oriented AlN layer grows on flat surfaces of the protrusion tops, excluding edges, and that the AlN layer deposited on the recesses obtained by the recesses and protrusions forming process forms new recesses over the recesses; and
epitaxially growing an Al x Ga y N(0001) layer (1≧x>0, x+y=1) on the initial-stage AlN layer by a lateral overgrowth method so as to cover the new recesses with the Al x Ga y N(0001) layer laterally overgrown from above the protrusion tops, wherein:
a growth method for epitaxially growing the initial-stage AlN layer by performing C axis orientation control is different from the lateral overgrowth method for epitaxially growing the Al x Ga y N (0001) layer, and
the initial-stage AlN layer is grown and deposited on the flat surfaces of the protrusion tops and on side walls and bottom surfaces of the recesses obtained by the recesses and protrusions forming process.
2. The method for producing a template for epitaxial growth according to claim 1 , wherein the recesses are formed on the surface of the sapphire (0001) substrate at a depth of 1.0 μm or less.
3. The method for producing a template for epitaxial growth according to claim 1 , wherein an AlN layer that is not oriented in C+ axis is grown near steps formed by the recesses and protrusions during growth of the initial-stage AlN layer.
4. The method for producing a template for epitaxial growth according to claim 2 , wherein an AlN layer that is not oriented in C+ axis is grown near steps formed by the recesses and protrusions during growth of the initial-stage AlN layer.
5. The method for producing a template for epitaxial growth according to claim 1 , wherein the Al x Ga y N(0001) layer is an AlN(0001) layer.
6. The method for producing a template for epitaxial growth according to claim 2 , wherein the Al x Ga y N(0001) layer is an AlN(0001) layer.
7. The method for producing a template for epitaxial growth according to claim 1 , wherein a growth condition for epitaxially growing the initial-stage AlN layer by performing C axis orientation control is different from that for epitaxially growing the Al x Ga y N (0001) layer by the lateral overgrowth method.
8. The method for producing a template for epitaxial growth according to claim 1 , wherein a growth speed for epitaxially growing the initial-stage AlN layer by performing C axis orientation control is lower than that for epitaxially growing the Al x Ga y N (0001) layer by the lateral overgrowth method.