Polymer powder storage and/or transport and/or degassing vessels
View Patent ↗Polymer powder vessel having a silo including a main vertical cylinder and a hopper at the bottom of the cylinder, a polymer powder which occupies the full volume of the hopper and at least a part of the volume of the cylinder, a polymer powder silo inlet pipe connected to the silo at a height located above the polymer powder, and a polymer hopper withdrawal pipe is also connected to the hopper. The polymer powder hopper withdrawal pipe is also connected to the silo at a location above the polymer powder for recirculating a part of the polymer powder within the silo.
1. Polymer powder vessel comprising:
a silo comprising a main vertical cylinder and a hopper at the bottom of the cylinder,
a polymer powder which occupies the full volume of the hopper and at least a part of the volume of the cylinder,
a polymer powder silo inlet pipe connected to the silo at a height located above the polymer powder, and
a polymer powder hopper withdrawal pipe connected to the hopper,
wherein the polymer powder hopper withdrawal pipe is also connected to the silo at a location above the polymer powder for recirculating a part of the polymer powder within the silo.
2. Polymer powder vessel according to claim 1 wherein the average (“mean”) particle size of the polymer powder is lower than 2000 microns.
3. Polymer powder vessel according to claim 1 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 6, as measured according to ASTM D 6773-02.
4. Polymer powder vessel according to claim 1 wherein the polymer powder which is introduced into the silo comprises residual hydrocarbons in an amount of 0.01 to 25% by weight, for example 0.05 to 10% by weight, of the one or more hydrocarbons having 3 to 10 carbon atoms.
5. Polymer powder vessel according to claim 1 wherein the polymer powder hopper withdrawal pipe is divided into a main polymer powder withdrawal pipe and at least one secondary polymer powder diversion pipe.
6. Polymer powder vessel according to claim 1 wherein the polymer powder vessel is a polymer powder degasser vessel.
7. Polymer powder vessel according to claim 1 wherein the silo contains at least 20 cubic meters of polymer powder.
8. Process for operating a polymer powder vessel which comprises
a silo comprising a main vertical cylinder and a hopper at the bottom of the cylinder,
a polymer powder which occupies the full volume of the hopper and at least a part of the volume of the cylinder,
a polymer powder silo inlet pipe connected to the silo at a height located above the polymer powder, and
a polymer powder hopper withdrawal pipe connected to the hopper,
wherein at least a part of the polymer powder which is withdrawn from the hopper is recirculated via the polymer powder hopper withdrawal pipe to a location upstream of the silo or to the silo at a height located above the polymer powder.
9. Process according to claim 8 wherein the average (“mean”) particle size of the polymer powder is lower than 2000 microns.
10. Process according to claim 8 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 6, as measured according to ASTM D 6773-02.
11. Process according to claim 8 wherein the polymer powder which is introduced into the silo comprises residual hydrocarbons in an amount of 0.01 to 25% by weight of the one or more hydrocarbons having 3 to 10 carbon atoms.
12. Process according to claim 8 wherein the polymer powder hopper withdrawal pipe is divided into a main polymer powder withdrawal pipe and at least one secondary polymer powder diversion pipe.
13. Process according to claim 8 wherein the polymer powder vessel is a polymer powder degasser vessel.
14. Process according to claim 8 wherein the silo contains at least 20 cubic meters of polymer powder.
15. Process according to claim 8 wherein the recirculation rate of the polymer powder is comprised between 1 and 30 percent per hour of the polymer powder present in the silo.
16. Process for operating a polymer powder degasser vessel used in a continuous polymerisation process wherein
said degassing vessel is located downstream of a polymerization reactor,
said degassing vessel is located upstream of a polymer powder extruder, and
said polymer powder extruder is shutting down, and
wherein said degassing vessel further comprises
a silo comprising a main vertical cylinder and a hopper at the bottom of the cylinder,
a polymer powder which occupies the full volume of the hopper and at least a part of the volume of the cylinder,
a polymer powder silo inlet pipe connected to the silo at a height located above the polymer powder, and
a polymer powder hopper withdrawal pipe connected to the hopper,
wherein at least a part of the polymer powder which is withdrawn from the hopper is recirculated via the polymer powder hopper withdrawal pipe to a location upstream of the silo or to the silo at a height located above the polymer powder.
17. Polymer powder vessel according to claim 1 wherein the polymer powder silo inlet pipe is connected to the top of the silo.
18. Polymer powder vessel according to claim 1 wherein the polymer powder hopper withdrawal pipe is connected to the bottom of the hopper.
19. Polymer powder vessel according to claim 2 wherein the average (“mean”) particle size of the polymer powder is between 200 and 1800 microns.
20. Polymer powder vessel according to claim 2 wherein the average (“mean”) particle size of the polymer powder is between 500 and 900 microns.
21. Polymer powder vessel according to claim 3 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 4, as measured according to ASTM D 6773-02.
22. Polymer powder vessel according to claim 3 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 2, as measured according to ASTM D 6773-02.
23. Polymer powder vessel according to claim 4 wherein the polymer powder which is introduced into the silo comprises residual hydrocarbons in an amount of 0.05 to 10% by weight of the one or more hydrocarbons having 3 to 10 carbon atoms.
24. Polymer powder vessel according to claim 5 wherein the at least one secondary polymer powder diversion pipe is the polymer powder recirculation pipe.
25. Process according to claim 8 wherein the polymer powder silo inlet pipe is connected to the top of the silo.
26. Process according to claim 8 wherein the polymer powder hopper withdrawal pipe is connected to the bottom of the hopper.
27. Process according to claim 8 wherein least a part of the polymer powder which is withdrawn from the hopper is recirculated via the polymer powder hopper withdrawal pipe to the top of the silo.
28. Process according to claim 9 wherein the average (“mean”) particle size of the polymer powder is between 200 and 1800 microns.
29. Process according to claim 9 wherein the average (“mean”) particle size of the polymer powder is between 500 and 900 microns.
30. Process according to claim 20 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 4, as measured according to ASTM D 6773-02.
31. Process according to claim 10 wherein the polymer powder flow properties are characterised by a flowability ratio of less than 2, as measured according to ASTM D 6773-02.
32. Process according to claim 11 wherein the polymer powder which is introduced into the silo comprises residual hydrocarbons in an amount of 0.05 to 10% by weight of the one or more hydrocarbons having 3 to 10 carbon atoms.
33. Process according to claim 12 wherein the secondary polymer powder diversion pipe is the polymer powder recirculation pipe.
34. Process according to claim 15 wherein the recirculation rate of the polymer powder is comprised between 5 and 20 percent per hour of the polymer powder present in the silo.
35. Process according to claim 15 wherein the recirculation rate of the polymer powder is comprised between 8 and 16 percent per hour of the polymer powder present in the silo.
36. Process according to claim 16 wherein the polymer powder silo inlet pipe is connected to the top of the silo.
37. Process according to claim 16 wherein the polymer powder hopper withdrawal pipe is connected to the bottom of the hopper.
38. Process according to claim 16 , wherein at least a part of the polymer powder which is withdrawn from the hopper is recirculated via the polymer powder hopper withdrawal pipe to the top of the silo.