IP Library Granted Patent US 9,034,937
Granted Patent B2
US 9,034,937 · App. 13/519,617 · Granted May 19, 2015

Surface treatment method for a substrate using denatured urushiol derived from

Inventors: Hye Jin Yoo (Busan, KR); In Woo Cheong (Daegu, KR); Chang Se Byeon (Gwangyang-si, KR); Jae Ryung Lee (Goyang-si, KR); Jin Tae Kim (Gwangyang-si, KR); Jung Hwan Lee (Gwangyang-si, KR); Yang Ho Choi (Gwangyang-si, KR)
Assignee: POSCO
C09D5/14C09D193/00C09D4/00
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Quick Facts
Patent No.
US 9,034,937
App. No.
13/519,617
Granted
May 19, 2015
Kind
B2
Abstract

A method of treating a surface of a substrate using modified urushiol derived from Toxicodendron vernicifluum is provided. More particularly, the reactivity of a hydroxyl group of urushiol extracted from fresh Toxicodendron vernicifluum is removed before the lacquer is used as a UV coating agent for a substrate such as a steel sheet. Therefore, the substrate may have high antibacterial activity, and excellent appearance and functionalities such as far-infrared radiation, blocking of electromagnetic waves, enhanced corrosion resistance, high crosslinking speed when a low content of a photoinitiator is used, excellent surface gloss and high scratch resistance.

Claims (55)

1. A composition for coating surface of steel sheet, comprising:

a binder comprising an oligomer and an acrylate monomer, in which the oligomer includes a urethane-based modified epoxy acrylate and a urethane acrylate, and the acrylate monomer includes a monofunctional acrylate monomer and a trifunctional acrylate monomer; and

a compound represented by Formula 1:

wherein,

R 1 is alkyl having 12 to 25 carbon atoms or alkylene having 12 to 25 carbon atoms,

R 2 and R 3 are independently —O—C(O)NHR, —O—C(O)—R, —O—Si(R) x (R′) 3-x , —O—C(R) x (R′) 3-x , or —O—C(O)—(CH 2 ) y —C(O)—OH,

R is alkyl having 1 to 12 carbon atoms, aryl having 5 to 12 carbon atoms, or aralkyl having 6 to 12 carbon atoms,

the substituent R may be substituted or unsubstituted with at least one substituent selected from the group consisting of alkyl having 1 to 6 carbon atoms, alkylene having 2 to 6 carbon atoms, and aryl having 5 to 12 carbon atoms,

R′ is alkoxy having 1 to 6 carbon atoms,

x is an integer of 1 to 3, and

y is an integer of 1 to 4,

wherein said composition is curable by UV irradiation.

2. The composition of claim 1 , wherein R 1 is C 15 H 31-2n , and n is one of 1 to 3,

R 2 and R 3 are independently —O—C(O)NHR, and

R is aralkyl having 6 to 12 carbon atoms, which is substituted or unsubstituted with alkyl having 1 to 12 carbon atoms or alkylene having 2 to 6 carbon atoms.

3. The composition of claim 1 , wherein R 1 is (CH 2 ) 14 CH 3 , (CH 2 ) 7 CH═CH(CH 2 ) 5 CH 3 , (CH 2 ) 7 CH═CHCH 2 CH═CH(CH 2 ) 2 CH 3 , (CH 2 ) 7 CH═CHCH 2 CH═CHCH═CHCH 3 , or (CH 2 ) 7 CH═CHCH 2 CH═CHCH 2 CH═CH 2 ,

R 2 and R 3 are independently —O—C(O)NHR, and

R is aralkyl having 6 to 12 carbon atoms, which is substituted or unsubstituted with alkyl having 1 to 8 carbon atoms, benzyl or alkylene having 2 to 4 carbon atoms.

4. The composition of claim 1 , wherein the compound of Formula 1 is included at a content of 1 to 50 parts by weight.

5. The composition of claim 1 , wherein the oligomer includes

25 to 45 parts by weight of the urethane-based modified epoxy acrylate; and

10 to 25 parts by weight of the urethane acrylate.

6. The composition of claim 1 , wherein the acrylate monomer includes

25 to 35 parts by weight of the monofunctional acrylate monomer; and

7 to 15 parts by weight of the trifunctional acrylate monomer.

7. The composition of claim 1 , further comprising a photoinitiator.

8. The composition of claim 7 , wherein the photoinitiator is at least one selected from the group consisting of a benzophenone containing photoinitiator, diphenoxy benzophenone containing photoinitiator, an anthraquinone derivative, a xantone derivative, a thioxantone derivative, or a benzyl containing photoinitiator.

9. The composition of claim 7 , wherein the photoinitiator is included at a content of 0.1 to 10 parts by weight.

10. A surface-treated steel sheet, comprising:

a steel sheet; and

a coating layer formed by curing the composition for coating surface of steel sheet according to claim 1 on one or both surfaces of the steel sheet.

11. A surface-treated steel sheet, comprising:

a steel sheet; and

a coating layer formed by curing the composition for coating surface of steel sheet according to claim 3 on one or both surfaces of the steel sheet.

12. A surface-treated steel sheet, comprising:

a steel sheet; and

a coating layer formed by curing the composition for coating surface of steel sheet according to claim 3 on one or both surfaces of the steel sheet.

13. A surface-treated steel sheet, comprising:

a steel sheet; and

a coating layer formed by curing the composition for coating surface of steel sheet according to claim 5 on one or both surfaces of the steel sheet.

14. A composition for coating the surface of steel sheet, comprising:

a binder comprising an oligomer and a diluent, wherein the oligomer includes 25 to 45 parts by weight of the urethane-based modified epoxy acrylate, and 10 to 25 parts by weight of the urethane acrylate; and

a compound represented by Formula 1:

wherein,

R 1 is alkyl having 1 to 30 carbon atoms, alkylene having 2 to 30 carbon atoms, alkynyl having 2 to 30 carbon atoms, or aryl having 5 to 12 carbon atoms,

R 2 and R 3 are independently —O—C(O)NHR, —O—C(O)—R, —O—Si(R) x (R′) 3-x , —O—C(R) x (R′) 3-x , or —O—C(O)—(CH 2 ) y —C(O)—OH,

R is alkyl having 1 to 30 carbon atoms, alkylene having 2 to 30 carbon atoms, alkynyl having 2 to 30 carbon atoms, aryl having 5 to 12 carbon atoms, or aralkyl having 6 to 24 carbon atoms,

the substituent R may be substituted or unsubstituted with at least one substituent selected from the group consisting of alkyl having 1 to 12 carbon atoms, alkylene having 2 to 12 carbon atoms, alkynyl having 2 to 12 carbon atoms, and aryl having 5 to 12 carbon atoms,

R′ is alkoxy having 1 to 12 carbon atoms,

x is an integer of 1 to 3, and

y is an integer of 1 to 4,

wherein said composition is curable by UV irradiation.

15. A surface-treated steel sheet, comprising:

a steel sheet; and

a coating layer formed by curing the composition for coating surface of steel sheet according to claim 14 on one or both surfaces of the steel sheet.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2022
From: POSCO HOLDINGS INC.
To: POSCO CO., LTD
Reel/Frame 061777/0943 →
CHANGE OF NAME Recorded Sep 28, 2022
From: POSCO
To: POSCO HOLDINGS INC.
Reel/Frame 061561/0831 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 28, 2012
From: YOO, HYE JIN; CHEONG, IN WOO; BYEON, CHANG SE; LEE, JAE RYUNG; KIM, JIN TAE; LEE, JUNG HWAN; CHOI, YANG HO
To: POSCO
Reel/Frame 028459/0038 →
Priority Claims (1)
KR 10-2009-0133647 · Dec 30, 2009 · national
Continuity (1)
Related Publication 20120288550A1 · Nov 15, 2012