IP Library Granted Patent US 8,337,899
Granted Patent B2
US 8,337,899 · App. 13/554,894 · Granted Dec 25, 2012

Solid pharmaceutical dispersions with enhanced bioavailability

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Quick Facts
Patent No.
US 8,337,899
App. No.
13/554,894
Granted
Dec 25, 2012
Kind
B2
Abstract

Spray dried solid dispersions comprising a sparingly soluble drug and hydroxypropylmethylcellulose acetate succinate (HPMCAS) provide increased aqueous solubility and/or biavailability in a use environment.

Claims (12)

1. A spray dried solid dispersion consisting of a sparingly water-soluble drug, hydroxypropyl methylcellulose acetate succinate (HPMCAS), and a surface-active agent, wherein said dispersion is a homogeneous solid solution, such that said drug is molecularly dispersed and amorphous in said dispersion, and having a drug:polymer weight ratio between 1:0.4 and 1:20.

2. The spray dried solid dispersion of claim 1 , wherein said surface-active agent is selected from fatty acid and alkyl sulfonates, benzethanium chloride, docusate sodium, polyoxyethylene sorbitan fatty acid esters, sodium taurocholic acid, 1-palmitoyl-2-oleoyl-sn-glycero-3-phosphocholine, and lecithin.

3. The spray dried solid dispersion of claim 1 , wherein said surface-active agent comprises up to 25 wt % of said spray dried solid dispersion.

4. The spray dried solid dispersion of claim 1 , in the form of particles less than 100 μm in diameter.

5. The spray dried solid dispersion of claim 1 , wherein said dispersion comprises spray dried particles that are solidified in less than 2 seconds.

6. The spray dried solid dispersion of claim 1 , in the form of particles having a residual solvent content less than 2 wt %.

7. The spray dried solid dispersion of claim 1 , in the form of spray dried particles from a solution in which the concentration of drug in the solvent is less than 20 g/100 g and in which the total solids content is less than 25 weight %.

8. The spray dried solid dispersion of claim 1 , wherein said drug has a dose to aqueous solubility ratio greater than 100.

9. The spray dried solid dispersion of claim 1 , wherein said drug is crystalline when undispersed.

10. The spray dried solid dispersion of claim 1 , having a drug:polymer weight ratio between 1:0.5 and 1:20.

11. The spray dried solid dispersion of claim 1 , having a drug:polymer weight ratio between 1:1 and 1:20.

12. The spray dried solid dispersion of claim 1 , wherein said spray dried solid dispersion is supersaturated in said drug.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2012
From: PFIZER INC.; PFIZER PRODUCTS INC.
To: BEND RESEARCH, INC.
Reel/Frame 028933/0321 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2012
From: CURATOLO, WILLIAM J.; HERBIG, SCOTT M.; NIGHTINGALE, JAMES A. S.
To: PFIZER INC.
Reel/Frame 028902/0199 →