IP Library Granted Patent US 9,243,150
Granted Patent B2
US 9,243,150 · App. 13/564,341 · Granted Jan 26, 2016

Oxide coated metal pigments and film-forming compositions

Inventors: Craig Matzdorf (California, MD); William Nickerson (Reston, VA)
Assignee: The United States of America As Represented by the Secretary of the Navy
C09D5/00C09D5/082C09D5/10C09D7/1291C23F11/00C22C21/00C23F11/08C23F11/10
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Quick Facts
Patent No.
US 9,243,150
App. No.
13/564,341
Granted
Jan 26, 2016
Kind
B2
Abstract

This invention relates to sacrificial-metal pigments coated with an effective amount of at least one metal oxide or a combination of metal oxides such as a chromium-zirconium oxide, and the process for preparing said coated pigments and combination thereof with film-forming binders for coating metal substrates to inhibit corrosion. The coated sacrificial-metal pigments are electrically active to prevent corrosion of metal substrates that are more cathodic (electropositive) than the metal oxide coated metal pigments.

Claims (18)

1. Electrochemically corrosion-resistant compositions for application onto metal substrates in amounts ranging up to ten mils consisting essentially of, in parts by weight, from about:

5 to 80 parts of lubricating grease, from about

0.1 to 10 parts of at least one organic corrosion inhibitor, from about

0.1 to 5.0 parts or a surfactant, from about

1.0 to 5.0 parts of an organic solvent, and from about

20-80 parts of a sacrificial-metal pigment having a particle size ranging from about 2 to 100 microns; said metal pigment coated with an effective amount of metal oxides derived from an acidic aqueous solution consisting essentially of from about:

0.01 to 22 parts of a trivalent chromium compound, from about

0.01 to 12 parts of hexafluorozirconate, from about

0.01 to 12 parts of at least one fluorocarbon, from about

0.0-12 parts of a divalent zinc compound, and from about

0.0-5 parts by weight of water soluble corrosion inhibitor.

2. The corrosion-resistant composition of claim 1 wherein the coated sacrificial-metal pigment is zinc.

3. The corrosion-resistant composition of claim 1 wherein the coated sacrificial-metal pigment is nickel and the acidic solution contains 12 parts of divalent zinc compound.

4. The corrosion-resistant composition of claim 1 wherein the coated sacrificial-metal pigment is aluminum and the oxide is derived from a trivalent chromate and a fluorozirconate.

5. The corrosion-resistant composition of claim 1 wherein the coated sacrificial-metal pigment is iron and the oxide is derived from a zirconate.

6. The corrosion-resistant composition of claim 1 wherein the corrosion inhibitor is a triazole.

7. The corrosion-resistant composition of claim 1 wherein the corrosion inhibitor is benzotriazole.

8. The corrosion-resistant composition of claim 7 wherein the corrosion-inhibitor is present in an amount of about 5 parts by weight.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded May 26, 2026
From: SOUTHWEST BANK; SIMMONS BANK
To: THE PATENT WELL LLC
Reel/Frame 074764/0495 →
SECURITY INTEREST Recorded Jan 18, 2017
From: THE PATENT WELL LLC
To: SOUTHWEST BANK
Reel/Frame 041003/0715 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2012
From: MATZDORF, CRAIG; NICKERSON, WILLIAM
To: DEPARTMENT OF THE NAVY
Reel/Frame 028700/0334 →
Continuity (4)
Continuation In Part 13192158 · Jul 27, 2011
Continuation In Part 13010830 · Jan 21, 2011
Continuation In Part 11116166 · Apr 21, 2005
Related Publication 20130168612A1 · Jul 4, 2013