Polycrystalline diamond compact and applications therefor
View Patent ↗Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) including a polycrystalline diamond (“PCD”) table having a structure for enhancing at least one of abrasion resistance, thermal stability, or impact resistance. In an embodiment, a PDC includes a PCD table. The PCD table includes a lower region including a plurality of diamond grains exhibiting a lower average grain size and at least an upper region adjacent to the lower region and including a plurality of diamond grains exhibiting an upper average grain size. The lower average grain size may be at least two times greater than that of the upper average grain size. The PDC includes a substrate having an interfacial surface that is bonded to the lower region of the PCD table. Other embodiments are directed methods of forming PDCs, and various applications for such PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
1. A polycrystalline diamond compact, comprising:
a polycrystalline diamond table including:
a single lower region including a plurality of bonded diamond grains exhibiting a lower region average grain size; and
at least an upper region directly bonded to the single lower region, the upper region at least partially defining at least one upper exterior surface of the polycrystalline diamond table, the upper region including a plurality of bonded diamond grains exhibiting an upper region average grain size of less than about 40 μm, the lower region average grain size being about two times to about 3.5 times greater than that of the upper region average grain size and at least about 60 μm; and
a substrate including an interfacial surface that is bonded directly to the single lower region of the polycrystalline diamond table, the substrate being separated from the upper region by the single lower region.
2. The polycrystalline diamond compact of claim 1 wherein the lower region average grain size is about 60 μm to about 80 μm and the upper region average grain size is about 20 μm to about 35 μm.
3. The polycrystalline diamond compact of claim 1 wherein the lower region average grain size is about 65 μm to about 75 μm and the upper region average grain size is about 25 μm to about 35 μm.
4. The polycrystalline diamond compact of claim 1 wherein the lower region average grain size is about 68 μm to about 72 μm and the upper region average grain size is about 28 μm to about 32 μm.
5. The polycrystalline diamond compact of claim 1 wherein the lower region average grain size is about 2.5 to about 3.5 times the upper region average grain size.
6. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table exhibits a G ratio , as determined by a ratio of the volume of a workpiece cut to the volume of the polycrystalline diamond table worn in a vertical lathe test, of at least about 2×10 6 .
7. The polycrystalline diamond compact of claim 6 wherein the G ratio is at least about 4×10 6 .
8. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table in integrally formed with the substrate.
9. The polycrystalline diamond compact of claim 1 wherein the substrate includes a cemented carbide substrate.
10. The polycrystalline diamond compact of claim 1 wherein the polycrystalline diamond table comprises a leached region extending inwardly from the at least one upper exterior surface into at least the upper region.
11. A method of fabricating a polycrystalline diamond compact, comprising:
enclosing a combination in a pressure transmitting medium to form a cell assembly, wherein the combination includes:
a substrate including an interfacial surface;
a lower region including a plurality of diamond particles positioned at least proximate to the interfacial surface of a substrate, the plurality of diamond particles of the lower region exhibiting a lower average particle size;
at least an upper region including a plurality of diamond particles positioned adjacent to the lower region, the plurality of diamond particles of the at least an upper region exhibiting an upper average particle size that is at least twice, to about 3.5 times greater than, that of the lower average particle size; and
subjecting the cell assembly to a high-pressure/high-temperature process to form a polycrystalline diamond table integrally with the substrate from the combination; and
wherein the lower average particle size is at least about 60 μm and the upper average particle size is less than about 40 μm.
12. The method of claim 11 wherein the lower average particle size is about 60 μm to about 80 μm and the upper average particle size is about 20 μm to about 35 μm.
13. The method of claim 11 wherein the lower average particle size is about 65 μm to about 75 μm and the upper average particle size is about 25 μm to about 35 μm.
14. The method of claim 11 wherein the lower average particle size is about 68 μm to about 72 μm and the upper average particle size is about 28 μm to about 32 μm.
15. The method of claim 11 wherein the substrate includes a cemented carbide substrate.
16. The method of claim 11 wherein subjecting the cell assembly to a high-pressure/high-temperature process to form a polycrystalline diamond table integrally with the substrate from the combination includes infiltrating at least the lower region with a metal-solvent catalyst from the substrate.
17. The method of claim 16 , further comprising at least partially removing the metal-solvent catalyst from at least a portion of the polycrystalline diamond table.
18. A rotary drill bit, comprising:
a bit body including a leading end structure configured to facilitate drilling a subterranean formation; and
a plurality of cutting elements mounted to the bit body, at least one of the plurality of cutting elements including:
a polycrystalline diamond table including:
a single lower region including a plurality of bonded diamond grains exhibiting a lower region average grain size; and
at least an upper region directly bonded to the single lower region, the upper region at least partially defining at least one upper exterior surface of the polycrystalline diamond table, the upper region including a plurality of bonded diamond grains exhibiting an upper region average grain size of less than about 40 μm, the lower region average grain size being about two times to about 3.5 times greater than that of the upper region average grain size and at least about 60 μm; and
a substrate including an interfacial surface that is directly bonded to the single lower region of the polycrystalline diamond table, the substrate being separated from the upper region by the single lower region.
19. A polycrystalline diamond compact, comprising:
a polycrystalline diamond table including:
a single lower region including a plurality of bonded diamond grains exhibiting a lower region average grain size of about 60 μm to about 80 μm; and
at least an upper region directly bonded to the single lower region, the upper region including an upper surface at least partially defining at least one upper exterior surface of the polycrystalline diamond table, the upper region including a plurality of bonded diamond grains exhibiting an upper region average grain size of about 15 μm to about 35 μm; and
a substrate including an interfacial surface that is bonded directly to the single lower region of the polycrystalline diamond table, the substrate being separated from the upper region by the single lower region.
20. The polycrystalline diamond compact of claim 19 wherein the lower region average grain size is about 65 μm to about 75 μm and the upper region average grain size is about 25 μm to about 35 μm.
21. The polycrystalline diamond compact of claim 19 wherein the lower region average grain size is about 68 μm to about 72 μm and the upper region average grain size is about 28 μm to about 32 μm.
22. The polycrystalline diamond compact of claim 19 wherein the lower region average grain size is about 2.5 to about 3.5 times the upper region average grain size.
23. The polycrystalline diamond compact of claim 19 wherein the polycrystalline diamond table exhibits a G ratio , as determined by a ratio of the volume of a workpiece cut to the volume of the polycrystalline diamond table worn in a vertical lathe test, of at least about 2×10 6 .
24. The polycrystalline diamond compact of claim 23 wherein the G ratio is at least about 4×10 6 .
25. The polycrystalline diamond compact of claim 19 wherein the polycrystalline diamond table in integrally formed with the substrate.
26. The polycrystalline diamond compact of claim 19 wherein the substrate includes a cemented carbide substrate.
27. The polycrystalline diamond compact of claim 19 wherein the polycrystalline diamond table comprises a leached region extending inwardly from the at least one upper exterior surface into at least the upper region.