IP Library Granted Patent US 9,074,061
Granted Patent B2
US 9,074,061 · App. 13/605,577 · Granted Jul 7, 2015

EVA recycling method

Inventor: Sui-Chieh J. Yu (Portland, OR)
Assignee: NIKE, Inc.
C08J11/04C08L31/04A43B13/04B29B17/00C08J9/0061C08J9/06C08J2201/026C08J2203/02C08J2203/04C08J2300/30C08J2323/08C08J2400/30C08J2423/08B29K2023/083B29K2105/04C08K3/0033
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Quick Facts
Patent No.
US 9,074,061
App. No.
13/605,577
Granted
Jul 7, 2015
Kind
B2
Abstract

A method of recycling scrap ethylene-vinyl acetate (EVA) foam involves foaming and crosslinking a blend containing virgin EVA resin and scrap EVA foam, as well as a crosslinking agent and blowing agent for the EVA resin. The blend further contains a compatibilizer, which is a hydrogenated petroleum resin.

Claims (32)

1. A foaming composition for making a foamed ethylene vinyl acetate copolymer article or articles incorporating recycled ethylene vinyl acetate foam, the composition consisting essentially of:

ethylene vinyl acetate (EVA) copolymer having 15-60 mole percent vinyl acetate;

scrap, at least partially crosslinked ethylene-vinyl acetate foam product;

peroxide crosslinking agent;

blowing agent for the vinyl acetate copolymer;

a compatibilizer comprising a hydrocarbon resin or a hydrogenated petroleum resin, and

optionally, a member selected from the group consisting of foam auxiliaries, foaming inhibitors, fillers, pigments, fire retardants, lubricants, activators, and combinations thereof.

2. A composition according to claim 1 , wherein the compatibilizer comprises a resin produced by polymerizing a C5 cut obtained as a byproduct of petroleum cracking.

3. A composition according to claim 1 , wherein the compatibilizer comprises a resin produced by polymerizing a C9 cut obtained as a byproduct of petroleum cracking.

4. A composition according to claim 1 comprising 1-19 percent by weight of the scrap foam product.

5. A composition according to claim 1 , wherein the peroxide crosslinking agent comprises dicumyl peroxide.

6. A composition according to claim 1 , wherein the blowing agent comprises a diazocarbamide.

7. A composition according to claim 1 , comprising a filler selected from the group consisting of magnesium carbonate, magnesium silicate, and calcium carbonate.

8. A composition according to claim 1 , comprising 1-4 parts of the compatibilizer based on 100 parts of the EVA copolymer.

9. A composition according to claim 1 , comprising 1-19 percent by weight of the scrap foam product and 1-4 parts of the compatibilizer based on 100 parts of the EVA copolymer.

10. A foaming composition for making a foamed ethylene vinyl acetate copolymer article, the mixture comprising:

virgin resin consisting essentially of ethylene vinyl acetate (EVA) copolymer having 15-60 mole percent vinyl acetate;

scrap, at least partially crosslinked ethylene-vinyl acetate foam product;

peroxide crosslinking agent;

blowing agent for the vinyl acetate copolymer; and

a compatibilizer comprising a hydrocarbon resin or a hydrogenated petroleum resin.

11. A composition according to claim 10 , comprising 1-19 percent by weight of the scrap foam product and 1-4 parts of the compatibilizer based on 100 parts of the EVA copolymer.

12. A composition according to claim 10 , comprising from 1 to 30 parts by weight of scrap ethylene-vinyl acetate foam product based on 100 parts by weight of virgin ethylene vinyl acetate (EVA) copolymer and comprising an amount of the compatibilizer that increases tear strength of a foamed article molded from the composition.

13. A composition according to claim 10 , wherein the mixture comprises a single copolymer component consisting essentially of the virgin resin and the scrap ethylene-vinyl acetate foam product.

14. A foamed ethylene vinyl acetate copolymer article comprising:

a crosslinked reaction product of a mixture comprising

ethylene vinyl acetate (EVA) copolymer having 15-60 mole percent vinyl acetate;

scrap, at least partially crosslinked ethylene-vinyl acetate foam product;

peroxide crosslinking agent;

blowing agent for the vinyl acetate copolymer; and

a compatibilizer comprising a hydrocarbon resin or a hydrogenated petroleum resin;

wherein the copolymer article has increased split tear strength, reduced shrinkage, or both as compared to a foamed ethylene vinyl acetate copolymer article that is a crosslinked reaction product of a mixture that is substantially the same but without the compatibilizer.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 14, 2015
From: NIKE, INC.
To: NIKE INTERNATIONAL LTD.
Reel/Frame 034705/0483 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2012
From: YU, SUI-CHIEH J.; SHEN, XIAO
To: NIKE, INC.
Reel/Frame 029501/0557 →
Continuity (1)
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