IP Library Granted Patent US 9,670,064
Granted Patent B1
US 9,670,064 · App. 13/628,186 · Granted Jun 6, 2017

Production of heavy water

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Quick Facts
Patent No.
US 9,670,064
App. No.
13/628,186
Granted
Jun 6, 2017
Kind
B1
Abstract

Disclosed are methods and apparatuses for producing heavy water. In one embodiment, a catalyst is treated with high purity air or a mixture of gaseous nitrogen and oxygen with gaseous deuterium all together flowing over the catalyst to produce the heavy water. In an alternate embodiment, the deuterium is combusted to form the heavy water. In an alternate embodiment, gaseous deuterium and gaseous oxygen is flowed into a fuel cell to produce the heavy water. In various embodiments, the deuterium may be produced by a thermal decomposition and distillation process that involves heating solid lithium deuteride to form liquid lithium deuteride and then extracting the gaseous deuterium from the liquid lithium deuteride.

Claims (18)

1. A method of producing heavy water comprising:

heating solid lithium deuteride to form liquid lithium deuteride;

extracting gaseous deuterium from the liquid lithium deuteride;

combusting the extracted gaseous deuterium with gaseous oxygen to produce gaseous heavy water; and

condensing the gaseous heavy water to produce liquid or solid heavy water.

2. A method of producing heavy water comprising:

heating solid lithium deuteride to form liquid lithium deuteride;

extracting gaseous deuterium from the liquid lithium deuteride;

flowing the extracted gaseous deuterium into a fuel cell with gaseous oxygen; and

extracting liquid heavy water from the fuel cell.

3. A method of producing heavy water comprising:

heating solid lithium deuteride to form liquid lithium deuteride;

extracting gaseous deuterium from the liquid lithium deuteride;

treating a catalyst with inert gas and gaseous oxygen to produce an oxygenated catalyst;

flowing the extracted gaseous deuterium over the oxygenated catalyst to produce gaseous heavy water; and

condensing the gaseous heavy water to produce liquid or solid heavy water.

4. The method of claim 3 wherein the inert gas is nitrogen.

5. The method of claim 3 wherein the flowing step further includes flowing inert gas over the oxygenated catalyst.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2014
From: BABCOCK & WILCOX TECHNICAL SERVICES Y-12, LLC
To: CONSOLIDATED NUCLEAR SECURITY, LLC
Reel/Frame 033756/0649 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 27, 2012
From: PHILLIPS, MICHAEL R.; SPENCER, LARRY S.; BROWN, SAM W.
To: BABCOCK & WILCOX TECHNICAL SERVICES Y-12, LLC
Reel/Frame 029035/0524 →