Method for manufacturing a rubber composition
View Patent ↗Process for the manufacture of a rubber composition comprising various constituents, such as base elastomers, reinforcing fillers, additives and a vulcanization system, during which the following stages are carried out: A—using a continuous mixing device, a starting rubber composition comprising the reinforcing fillers and optionally other components, with the exception of the crosslinking system, is produced, the operating parameters for the continuous mixing device being chosen so that: a—the residence time of the elastomer in the mixing chamber is between 20 and 60 seconds, b—the specific energy conferred on the rubber composition is between 2000 joules/gram and 5000 joules/gram, B—at the outlet for the starting rubber composition from the mixing chamber, the temperature of the said starting rubber composition is lowered to a temperature of less than 140° C. in less than 5 minutes.
1. A process for the manufacture of a rubber composition comprising as base elastomers, reinforcing fillers, additives and a vulcanization system, comprising the following stages:
A—using a continuous mixing device comprising a mixing chamber comprising at least one rotor rotating in a stator and extending between an upstream end and a downstream end, between which the material gradually advances, and comprising appliances for metering and forced introduction of the base elastomer or elastomers, driving back the base elastomers through a pipeline emerging upstream of the mixing chamber, a starting rubber composition comprising reinforcing fillers is produced, wherein said produced starting rubber composition does not include the vulcanization system, the operating parameters for the continuous mixing device being chosen so that:
a—the residence time of the elastomer in the mixing chamber is between 20 and 60 seconds,
b—the specific energy conferred on the rubber composition is between 2000 joules/gram and 5000 joules/gram,
B—at the outlet for the starting rubber composition from the mixing chamber, the temperature of the said starting rubber composition is lowered to a temperature of less than 140° C. in less than 5 minutes.
2. The process according to claim 1 , wherein, during stage A, additives are also incorporated.
3. The process according to claim 1 , wherein, during stage A, the rotational speed of the rotor is between 50 and 500 rev/min.
4. The process according to claim 1 , wherein, during stage A, the rotational speed of the rotor is between 200 and 400 rev/min.
5. The process according to claim 1 , wherein, during stage A, the maximum theoretical shear rate ({dot over (γ)}) of the rubber composition in the mixing chamber is between 15 000 s−1 and 40 000 s−1.
6. The process according to claim 1 , wherein, during stage A, the degree of filling of the mixing chamber is between 5% and 40%.
7. The process according to claim 1 , wherein, on conclusion of stage B, a final rubber composition is produced using one or more continuous or batchwise mixing means of internal and/or external mixer type, a predetermined volume of the starting rubber composition, the vulcanization system and also any remaining elastomer, fillers and additives being incorporated, the operating parameters for the continuous or batchwise mixing means being chosen so that the additional specific energy conferred on the rubber composition during this stage is between 500 joules/gram and 1800 joules/gram.